PL420392A1 - Reactor for spectroscopic tests - Google Patents

Reactor for spectroscopic tests

Info

Publication number
PL420392A1
PL420392A1 PL420392A PL42039217A PL420392A1 PL 420392 A1 PL420392 A1 PL 420392A1 PL 420392 A PL420392 A PL 420392A PL 42039217 A PL42039217 A PL 42039217A PL 420392 A1 PL420392 A1 PL 420392A1
Authority
PL
Poland
Prior art keywords
reaction chamber
reactor
reaction
heating
coolant passage
Prior art date
Application number
PL420392A
Other languages
Polish (pl)
Other versions
PL232633B1 (en
Inventor
Karolina TARACH
Kinga GÓRA-MAREK
Janusz BUDZIOCH
Original Assignee
Uniwersytet Jagielloński
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Uniwersytet Jagielloński filed Critical Uniwersytet Jagielloński
Priority to PL420392A priority Critical patent/PL232633B1/en
Priority to PCT/PL2018/050003 priority patent/WO2018143832A1/en
Publication of PL420392A1 publication Critical patent/PL420392A1/en
Publication of PL232633B1 publication Critical patent/PL232633B1/en

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01—Arrangements or apparatus for facilitating the optical investigation
    • G01N21/03—Cuvette constructions
    • G01N21/0332—Cuvette constructions with temperature control
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01—Arrangements or apparatus for facilitating the optical investigation
    • G01N21/03—Cuvette constructions
    • G01N2021/0325—Cells for testing reactions, e.g. containing reagents
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01—Arrangements or apparatus for facilitating the optical investigation
    • G01N21/03—Cuvette constructions
    • G01N2021/0339—Holders for solids, powders

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Optical Measuring Cells (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
  • Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)

Abstract

Przedmiotem zgłoszenia jest reaktor do badań spektroskopowych, pracujący w modzie transmisyjnym, zawierający komorę reakcyjną (1), obejmującą cylindryczną rurę, z której rozciągają się prostopadle co najmniej dwa wyprowadzenia, doprowadzające gazowe medium robocze do obszaru reakcyjnego w komorze reakcyjnej (1), w którym umieszczona jest badana próbka (6), co najmniej dwa okna optyczne, rozmieszczone na końcach cylindrycznej rury komory reakcyjnej (1), dociśnięte do komory reakcyjnej (1) i uszczelnione z nią przez uszczelnienie okna, układ grzania i chłodzenia wsparty bezpośrednio na komorze reakcyjnej (1) oraz rozmieszczony zasadniczo wokół obszaru reakcyjnego, co najmniej dwa mocowania reaktora utrzymujące przeciwległe końce komory reakcyjnej (1), przy czym mocowanie reaktora obejmuje kanał cieczy chłodzącej, którego wewnętrzna powierzchnia stanowi powierzchnię zewnętrzną komory reakcyjnej (1), przy czym kanał cieczy chłodzącej uszczelniony jest od strony układu grzania i chłodzenia oraz od strony próżniowej uszczelnieniem cieczowym, będącym w bezpośrednim kontakcie z komorą reakcyjną (1).The subject of the application is a spectroscopic reactor, operating in transmission mode, containing a reaction chamber (1), comprising a cylindrical pipe from which at least two outlets extend perpendicularly, supplying a working gas medium to the reaction area in the reaction chamber (1), in which the test sample (6) is placed, at least two optical windows, arranged at the ends of the cylindrical reaction chamber tube (1), pressed against the reaction chamber (1) and sealed with it by window sealing, heating and cooling system supported directly on the reaction chamber ( 1) and disposed essentially around the reaction area, at least two reactor mounts holding opposite ends of the reaction chamber (1), wherein the reactor mount includes a coolant passage whose internal surface is the external surface of the reaction chamber (1), the coolant passage sealed thi t on the heating and cooling side and on the vacuum side with a liquid seal in direct contact with the reaction chamber (1).

PL420392A 2017-02-03 2017-02-03 Reactor for spectroscopic tests PL232633B1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
PL420392A PL232633B1 (en) 2017-02-03 2017-02-03 Reactor for spectroscopic tests
PCT/PL2018/050003 WO2018143832A1 (en) 2017-02-03 2018-02-04 Reactor for spectroscopic studies

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL420392A PL232633B1 (en) 2017-02-03 2017-02-03 Reactor for spectroscopic tests

Publications (2)

Publication Number Publication Date
PL420392A1 true PL420392A1 (en) 2018-08-13
PL232633B1 PL232633B1 (en) 2019-07-31

Family

ID=63039908

Family Applications (1)

Application Number Title Priority Date Filing Date
PL420392A PL232633B1 (en) 2017-02-03 2017-02-03 Reactor for spectroscopic tests

Country Status (2)

Country Link
PL (1) PL232633B1 (en)
WO (1) WO2018143832A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL443347A1 (en) * 2022-12-30 2024-07-01 Measline Spolka Z Ograniczona Odpowiedzialnoscia Reactor for spectroscopic research

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111272654B (en) * 2018-12-04 2021-02-26 中国科学院大连化学物理研究所 A temperature-controlled infrared in-situ reaction cell based on high vacuum conditions from low temperature to high temperature
CN110614067B (en) * 2019-09-27 2025-03-04 费勉仪器科技（上海）有限公司 In-situ high temperature and high pressure reaction device
CN112748073B (en) * 2019-10-31 2024-05-31 中国石油化工股份有限公司 Material in-situ characterization sample cell and use method thereof
CN112485198B (en) * 2020-11-25 2025-01-24 北京中研环科科技有限公司 A high and low temperature in-situ spectral reaction cell

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6031040A (en) * 1983-07-29 1985-02-16 Sagami Chem Res Center Infrared ray spectral cell
PL173291B1 (en) * 1994-08-12 1998-02-27 Akad Gorniczo Hutnicza High-temperature gas cuvette

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL443347A1 (en) * 2022-12-30 2024-07-01 Measline Spolka Z Ograniczona Odpowiedzialnoscia Reactor for spectroscopic research
PL246671B1 (en) * 2022-12-30 2025-02-24 Uniwersytet Jagielloński Reactor for spectroscopic research

Also Published As

Publication number Publication date
PL232633B1 (en) 2019-07-31
WO2018143832A1 (en) 2018-08-09

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