PL441429A1 - Method of conducting the process of collective co-precipitation of fluorine and other components from solutions obtained after a unit, single-stage or two-stage acidic leaching process of battery masses resulting from the processing of used, incomplete and/or waste lithium-ion (Li-ion) cells - Google Patents
Method of conducting the process of collective co-precipitation of fluorine and other components from solutions obtained after a unit, single-stage or two-stage acidic leaching process of battery masses resulting from the processing of used, incomplete and/or waste lithium-ion (Li-ion) cellsInfo
- Publication number
- PL441429A1 PL441429A1 PL441429A PL44142922A PL441429A1 PL 441429 A1 PL441429 A1 PL 441429A1 PL 441429 A PL441429 A PL 441429A PL 44142922 A PL44142922 A PL 44142922A PL 441429 A1 PL441429 A1 PL 441429A1
- Authority
- PL
- Poland
- Prior art keywords
- ion
- stage
- collective
- incomplete
- precipitation
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 9
- 229910001416 lithium ion Inorganic materials 0.000 title abstract 6
- 230000002378 acidificating effect Effects 0.000 title abstract 3
- 238000000975 co-precipitation Methods 0.000 title abstract 3
- 239000011737 fluorine Substances 0.000 title abstract 3
- 229910052731 fluorine Inorganic materials 0.000 title abstract 3
- 238000002386 leaching Methods 0.000 title abstract 3
- 239000002699 waste material Substances 0.000 title abstract 3
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 title abstract 2
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 title 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 abstract 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 2
- 229910052782 aluminium Inorganic materials 0.000 abstract 2
- 229910052802 copper Inorganic materials 0.000 abstract 2
- 239000010949 copper Substances 0.000 abstract 2
- 229910052742 iron Inorganic materials 0.000 abstract 2
- 239000011574 phosphorus Substances 0.000 abstract 2
- 229910052698 phosphorus Inorganic materials 0.000 abstract 2
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 abstract 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 1
- 238000004458 analytical method Methods 0.000 abstract 1
- 238000001636 atomic emission spectroscopy Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
- B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
- B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/006—Wet processes
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/54—Reclaiming serviceable parts of waste accumulators
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
Przedmiotem zgłoszenia jest sposób prowadzenia procesu kolektywnego współstrącania fluoru z roztworów otrzymanych po jednostkowym procesie kwaśnego jednostopniowego lub dwustopniowego ługowania mas bateryjnych powstałych z przerobu zużytych, niekompletnych i/lub odpadowych ogniw litowo-jonowych (Li-ion) charakteryzujący się tym, że wykorzystuje się roztwór wodorotlenku sodu(I) o stężeniu od 1,0 M do 2,0 M, przy czym fluor usuwany jest w zakresie od 94% do 98% wagowych, obliczonych na podstawie analizy chemicznej ilościowo-jakościowej wykonanej przy użyciu optycznej spektrometrii emisyjnej (ICP-OS). Ponadto, przedmiotem zgłoszenia jest sposób prowadzenia procesu kolektywnego współstrącania składników tj. fosforu, aluminium, żelaza i miedzi z roztworów otrzymanych po jednostkowym procesie kwaśnego jednostopniowego lub dwustopniowego ługowania mas bateryjnych powstałych z przerobu zużytych, niekompletnych i/lub odpadowych ogniw litowo-jonowych (Li-ion) charakteryzujący się tym, że wykorzystuje się roztwór wodorotlenku sodu(I) o stężeniu od 1,0 M do 2,0 M, przy czym fosfor usuwany jest w zakresie od 72% do 100% wagowych, aluminium od 97% do 100% wagowych, żelazo od 98% do 99% wagowych i miedź od 98% do 100% wagowych.The subject of the application is a method of conducting the process of collective co-precipitation of fluorine from solutions obtained after a single acidic one-stage or two-stage leaching process of battery masses resulting from the processing of used, incomplete and/or waste lithium-ion (Li-ion) cells, characterized by the use of a hydroxide solution sodium(I) with a concentration of 1.0 M to 2.0 M, with fluorine removed in the range of 94% to 98% by weight, calculated on the basis of quantitative and qualitative chemical analysis performed using optical emission spectrometry (ICP-OS ). Moreover, the subject of the application is a method of conducting the process of collective co-precipitation of components, i.e. phosphorus, aluminum, iron and copper from solutions obtained after a single process of acidic one-stage or two-stage leaching of battery masses resulting from the processing of used, incomplete and/or waste lithium-ion cells (Li- ion) characterized by the use of a sodium(I) hydroxide solution with a concentration of 1.0 M to 2.0 M, with phosphorus being removed in the range from 72% to 100% by weight, aluminum from 97% to 100% by weight, iron from 98% to 99% by weight and copper from 98% to 100% by weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL441429A PL441429A1 (en) | 2022-06-09 | 2022-06-09 | Method of conducting the process of collective co-precipitation of fluorine and other components from solutions obtained after a unit, single-stage or two-stage acidic leaching process of battery masses resulting from the processing of used, incomplete and/or waste lithium-ion (Li-ion) cells |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL441429A PL441429A1 (en) | 2022-06-09 | 2022-06-09 | Method of conducting the process of collective co-precipitation of fluorine and other components from solutions obtained after a unit, single-stage or two-stage acidic leaching process of battery masses resulting from the processing of used, incomplete and/or waste lithium-ion (Li-ion) cells |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL441429A1 true PL441429A1 (en) | 2023-12-11 |
Family
ID=89123597
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL441429A PL441429A1 (en) | 2022-06-09 | 2022-06-09 | Method of conducting the process of collective co-precipitation of fluorine and other components from solutions obtained after a unit, single-stage or two-stage acidic leaching process of battery masses resulting from the processing of used, incomplete and/or waste lithium-ion (Li-ion) cells |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL441429A1 (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104241724A (en) * | 2014-09-02 | 2014-12-24 | 湖南邦普循环科技有限公司 | Method for preparing battery-grade lithium carbonate from recycled lithium ion battery material |
| CN109593963A (en) * | 2018-10-31 | 2019-04-09 | 天齐锂业资源循环技术研发(江苏)有限公司 | A kind of new method of the selective recovery valuable metal from waste lithium cell |
| CN111471864A (en) * | 2020-04-24 | 2020-07-31 | 广东邦普循环科技有限公司 | Method for recovering copper, aluminum and iron from waste lithium ion battery leachate |
| CN113957254A (en) * | 2021-09-28 | 2022-01-21 | 广东邦普循环科技有限公司 | Method for efficiently removing fluorine from waste lithium battery |
-
2022
- 2022-06-09 PL PL441429A patent/PL441429A1/en unknown
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104241724A (en) * | 2014-09-02 | 2014-12-24 | 湖南邦普循环科技有限公司 | Method for preparing battery-grade lithium carbonate from recycled lithium ion battery material |
| CN109593963A (en) * | 2018-10-31 | 2019-04-09 | 天齐锂业资源循环技术研发(江苏)有限公司 | A kind of new method of the selective recovery valuable metal from waste lithium cell |
| CN111471864A (en) * | 2020-04-24 | 2020-07-31 | 广东邦普循环科技有限公司 | Method for recovering copper, aluminum and iron from waste lithium ion battery leachate |
| CN113957254A (en) * | 2021-09-28 | 2022-01-21 | 广东邦普循环科技有限公司 | Method for efficiently removing fluorine from waste lithium battery |
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