PL444164A1 - Procedura oznaczania całkowitej zawartości osadu - Google Patents

Procedura oznaczania całkowitej zawartości osadu

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Publication number
PL444164A1
PL444164A1 PL444164A PL44416423A PL444164A1 PL 444164 A1 PL444164 A1 PL 444164A1 PL 444164 A PL444164 A PL 444164A PL 44416423 A PL44416423 A PL 44416423A PL 444164 A1 PL444164 A1 PL 444164A1
Authority
PL
Poland
Prior art keywords
sub
mass
filter
determining
fraction
Prior art date
Application number
PL444164A
Other languages
English (en)
Other versions
PL244487B1 (pl
Inventor
Dominik Schlehöfer
Aleš Vráblik
Radek Černý
Original Assignee
ORLEN UniCRE, a.s.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ORLEN UniCRE, a.s. filed Critical ORLEN UniCRE, a.s.
Publication of PL444164A1 publication Critical patent/PL444164A1/pl
Publication of PL244487B1 publication Critical patent/PL244487B1/pl

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26Oils; Viscous liquids; Paints; Inks
    • G01N33/28Oils, i.e. hydrocarbon liquids
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/38Diluting, dispersing or mixing samples
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G99/00Subject matter not provided for in other groups of this subclass
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L1/00Liquid carbonaceous fuels
    • C10L1/10Liquid carbonaceous fuels containing additives
    • C10L1/14Organic compounds
    • C10L1/18Organic compounds containing oxygen
    • C10L1/19Esters ester radical containing compounds; ester ethers; carbonic acid esters
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44Sample treatment involving radiation, e.g. heat
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/22Fuels; Explosives
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26Oils; Viscous liquids; Paints; Inks
    • G01N33/28Oils, i.e. hydrocarbon liquids
    • G01N33/2805Oils, i.e. hydrocarbon liquids investigating the resistance to heat or oxidation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26Oils; Viscous liquids; Paints; Inks
    • G01N33/28Oils, i.e. hydrocarbon liquids
    • G01N33/2835Specific substances contained in the oils or fuels
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
    • G01N5/04Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder
    • GPHYSICS
    • G06COMPUTING OR CALCULATING; COUNTING
    • G06TIMAGE DATA PROCESSING OR GENERATION, IN GENERAL
    • G06T7/00Image analysis
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20Characteristics of the feedstock or the products
    • C10G2300/30Physical properties of feedstocks or products
    • C10G2300/302Viscosity
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/80Additives
    • C10G2300/802Diluents
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N2001/2893Preparing calibration standards

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Emergency Medicine (AREA)
  • Computer Vision & Pattern Recognition (AREA)
  • Theoretical Computer Science (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)
  • Fats And Perfumes (AREA)
  • Paper (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

Przedmiotem zgłoszenia jest procedura oznaczania całkowitej zawartości osadu, jako wskaźnika stabilności frakcji resztkowych o lepkości przekraczającej 55 mm<sup>2</sup>/s w temperaturze 100°C charakteryzująca się tym, że frakcję resztkową rozcieńcza się dodając do 50% wag. estrów metylowych kwasów tłuszczowych i homogenizuje, następnie kroplę homogenizowanej mieszaniny umieszcza się na papierowym filtrze, który ogrzewa się do 100°C przez jedną godzinę, wówczas na filtrze tworzy się plama, po czym wykonuje się fotografię cyfrową plamy, która jest przekształcana przez oprogramowanie komputerowe do trybu plastycznego skanu 3D w skali odcieni szarości, gdzie przeprowadzana jest analiza obrazu w celu obliczenia reprezentacji procentowej frakcji o dużej lepkości, przy jednoczesnym określeniu odpowiedniego stosunku mieszania frakcji resztkowej i estrów metylowych kwasów tłuszczowych oraz wyznaczeniu całkowitej zawartości osadu zgodnie ze wzorem S<sub>(TS)</sub>=(m<sub>5</sub>-m<sub>4</sub>)-(m<sub>3</sub>-m<sub>2</sub>)•100/m<sub>1</sub>•w<sub>z</sub>, w którym S = osad w procentach masowych - indywidualne oznaczenia równoległe, z których oblicza się parametr TS, jako średnią arytmetyczną; TS = całkowita zawartość osadu (Total Sediment); m<sub>1</sub> = masa przygotowanej mieszaniny wylanej na filtr; m<sub>2</sub> = masa dolnego filtra (B) przed filtracją, m<sub>3</sub> = masa dolnego filtra (B) po filtracji; m<sub>4</sub> = masa górnego filtra (A) przed filtracją; m<sub>5</sub> = masa górnego filtra (A) po filtracji; w<sub>z</sub> = udział masowy reprezentowanej frakcji resztkowej w mieszaninie z estrami metylowymi kwasów tłuszczowych.
PL444164A 2022-04-21 2023-03-22 Procedura oznaczania całkowitej zawartości osadu PL244487B1 (pl)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CZ2022-163A CZ310012B6 (cs) 2022-04-21 2022-04-21 Postup stanovení celkového obsahu sedimentu
CZPV2022-163 2022-04-21

Publications (2)

Publication Number Publication Date
PL444164A1 true PL444164A1 (pl) 2023-10-23
PL244487B1 PL244487B1 (pl) 2024-01-29

Family

ID=88469739

Family Applications (1)

Application Number Title Priority Date Filing Date
PL444164A PL244487B1 (pl) 2022-04-21 2023-03-22 Procedura oznaczania całkowitej zawartości osadu

Country Status (2)

Country Link
CZ (1) CZ310012B6 (pl)
PL (1) PL244487B1 (pl)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CZ306562B6 (cs) * 2015-10-26 2017-03-08 Unipetrol Výzkumně Vzdělávací Centrum, A. S. Postup hodnocení stability topného oleje
CZ30254U1 (cs) * 2016-12-16 2017-01-10 Unipetrol výzkumně vzdělávací centrum, a.s. Zředěná zbytková frakce
EP4162012A1 (en) * 2020-06-09 2023-04-12 ExxonMobil Technology and Engineering Company Marine fuel compositions

Also Published As

Publication number Publication date
CZ310012B6 (cs) 2024-05-08
PL244487B1 (pl) 2024-01-29
CZ2022163A3 (cs) 2023-11-01

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