PL445628A1 - Method of producing halloysite-carbon material for isolating naproxen from the aqueous phase by solid-phase extraction - Google Patents

Method of producing halloysite-carbon material for isolating naproxen from the aqueous phase by solid-phase extraction

Info

Publication number
PL445628A1
PL445628A1 PL445628A PL44562823A PL445628A1 PL 445628 A1 PL445628 A1 PL 445628A1 PL 445628 A PL445628 A PL 445628A PL 44562823 A PL44562823 A PL 44562823A PL 445628 A1 PL445628 A1 PL 445628A1
Authority
PL
Poland
Prior art keywords
halloysite
weight
naproxen
isolating
solid
Prior art date
Application number
PL445628A
Other languages
Polish (pl)
Other versions
PL247286B1 (en
Inventor
Piotr M. Słomkiewicz
Dariusz Wideł
Original Assignee
Uniwersytet Jana Kochanowskiego W Kielcach
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Uniwersytet Jana Kochanowskiego W Kielcach filed Critical Uniwersytet Jana Kochanowskiego W Kielcach
Priority to PL445628A priority Critical patent/PL247286B1/en
Publication of PL445628A1 publication Critical patent/PL445628A1/en
Publication of PL247286B1 publication Critical patent/PL247286B1/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/56—Use in the form of a bed

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)

Abstract

Przedmiotem zgłoszenia jest sposób wytwarzania materiału haloizytowo-węglowego do izolacji naproksenu z fazy wodnej metodą ekstrakcji do fazy stałej, w którym stosuje się sorbent na bazie odżelazionej zwietrzeliny haloizytowej i z prekursora węglowego otrzymanego sacharozy oraz ditioninu sodu polega na dodawaniu 5 części wagowych otrzymanego po trawieniu technicznym kwasem siarkowym(VI) o stężeniu 20% wagowych produktu haloizytowego do 20 części wagowych wodnego roztworu o stężeniu 18% wagowych sacharozy i 10% wagowych ditioninu sodu i mieszaniu całości przez 4 godziny, po odsączeniu i suszeniu przez 10 godzin temperaturze 343 K, produktu haloizytowego, sacharozy i ditioninu sodu, karbonizowaniu w atmosferze azotu z narostem temperatury 6 K/min, w zakresie temperatur 343 - 473 K i w izotermie 973 K przez 4 godziny.The subject of the application is a method of producing halloysite-carbon material for isolating naproxen from the water phase by the solid-phase extraction method, in which a sorbent based on deferrized halloysite weathering and a carbon precursor obtained from sucrose and sodium dithionite is used, which consists in adding 5 parts by weight of the halloysite product obtained after digestion with technical sulfuric acid (VI) with a concentration of 20% by weight to 20 parts by weight of an aqueous solution with a concentration of 18% by weight of sucrose and 10% by weight of sodium dithionite and mixing the whole for 4 hours, after filtering and drying for 10 hours at a temperature of 343 K, the halloysite product, sucrose and sodium dithionite, carbonizing in a nitrogen atmosphere with a temperature increase of 6 K/min, in the temperature range of 343 - 473 K and in the isotherm 973K for 4 hours.

PL445628A 2023-07-18 2023-07-18 Method of producing halloysite-carbon material for isolating naproxen from the aqueous phase by solid-phase extraction PL247286B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL445628A PL247286B1 (en) 2023-07-18 2023-07-18 Method of producing halloysite-carbon material for isolating naproxen from the aqueous phase by solid-phase extraction

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL445628A PL247286B1 (en) 2023-07-18 2023-07-18 Method of producing halloysite-carbon material for isolating naproxen from the aqueous phase by solid-phase extraction

Publications (2)

Publication Number Publication Date
PL445628A1 true PL445628A1 (en) 2024-11-18
PL247286B1 PL247286B1 (en) 2025-06-09

Family

ID=93522771

Family Applications (1)

Application Number Title Priority Date Filing Date
PL445628A PL247286B1 (en) 2023-07-18 2023-07-18 Method of producing halloysite-carbon material for isolating naproxen from the aqueous phase by solid-phase extraction

Country Status (1)

Country Link
PL (1) PL247286B1 (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107597062A (en) * 2017-11-03 2018-01-19 长沙理工大学 A kind of preparation method of galapectite multistage hydridization gas adsorption material
PL234357B1 (en) * 2017-11-09 2020-02-28 Univ Jana Kochanowskiego W Kielcach Method for producing carbonified halloysite adsorbent for adsorption of paracetamol from water phase
WO2023272363A1 (en) * 2021-07-02 2023-01-05 Natural Nanotech Pty Ltd Halloysite-kaolin derivatised nanoporous carbon materials and preparation and uses thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107597062A (en) * 2017-11-03 2018-01-19 长沙理工大学 A kind of preparation method of galapectite multistage hydridization gas adsorption material
PL234357B1 (en) * 2017-11-09 2020-02-28 Univ Jana Kochanowskiego W Kielcach Method for producing carbonified halloysite adsorbent for adsorption of paracetamol from water phase
WO2023272363A1 (en) * 2021-07-02 2023-01-05 Natural Nanotech Pty Ltd Halloysite-kaolin derivatised nanoporous carbon materials and preparation and uses thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
SZCZEPANIK B, RĘDZIA N, FRYDEL L, SŁOMKIEWICZ P, KOŁBUS A, STYSZKO K, DZIOK T, SAMOJEDEN B.: "Materials (Basel). 2019 Nov 14;12(22):3754. doi: 10.3390/ma12223754.", SYNTHESIS AND CHARACTERIZATION OF HALLOYSITE/CARBON NANOCOMPOSITES FOR ENHANCED NSAIDS ADSORPTION FROM WATER. *

Also Published As

Publication number Publication date
PL247286B1 (en) 2025-06-09

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