PL450084A1 - Sposób otrzymywania sorpcyjnego tlenku manganu - Google Patents

Sposób otrzymywania sorpcyjnego tlenku manganu

Info

Publication number
PL450084A1
PL450084A1 PL450084A PL45008424A PL450084A1 PL 450084 A1 PL450084 A1 PL 450084A1 PL 450084 A PL450084 A PL 450084A PL 45008424 A PL45008424 A PL 45008424A PL 450084 A1 PL450084 A1 PL 450084A1
Authority
PL
Poland
Prior art keywords
rpm
temperature
period
manganese
manganese oxide
Prior art date
Application number
PL450084A
Other languages
English (en)
Inventor
Łukasz Gralewski
Andrzej Milewski
Agata Jakóbik-Kolon
Original Assignee
Politechnika Śląska W Gliwicach
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Śląska W Gliwicach filed Critical Politechnika Śląska W Gliwicach
Priority to PL450084A priority Critical patent/PL450084A1/pl
Publication of PL450084A1 publication Critical patent/PL450084A1/pl

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3071—Washing or leaching
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10—Obtaining alkali metals
    • C22B26/12—Obtaining lithium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Thermal Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

Przedmiotem zgłoszenia jest sposób otrzymywania sorpcyjnego tlenku manganu, który polega na tym, że na każdy 1 mol stałej soli manganu(II) dodaje się od 3 mol do 5 mol stałego monohydratu wodorotlenku litu, rozdrabnia, po czym wkrapla od 600 ml do 700 ml 60% roztworu nadtlenku wodoru na każdy 1 mol soli manganu(II) obecnej w mieszaninie, miesza z prędkością od 60 rpm do 200 rpm w czasie od 12 h do 72 h, osad sączy, przemywa wodą zdejonizowaną w ilości od 5 ml do 20 ml na każdy 1 g osadu i suszy w temperaturze od 40°C do 60°C w czasie od 24 h do 48 h, następnie spieka w temperaturze od 100°C do 150°C w czasie od 10 h do 15 h, proces prowadzi się kolejno od 400°C do 500°C w czasie od 5 h do 7 h, otrzymany prekursor umieszcza się w roztworze kwasu od 0,5 M do 1 M, miesza z szybkością od 60 rpm do 250 rpm w czasie od 4 h do 72 h w temperaturze od 20°C do 60°C, kolejno przemywa wodą zdejonizowaną od 500 ml do 1000 ml na każde 5 gram do osiągnięcia przez przesącz pH co najmniej 6, po czym suszy w temperaturze od 40°C do 60°C, przez od 4 h do 48 h.
PL450084A 2024-10-21 2024-10-21 Sposób otrzymywania sorpcyjnego tlenku manganu PL450084A1 (pl)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL450084A PL450084A1 (pl) 2024-10-21 2024-10-21 Sposób otrzymywania sorpcyjnego tlenku manganu

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL450084A PL450084A1 (pl) 2024-10-21 2024-10-21 Sposób otrzymywania sorpcyjnego tlenku manganu

Publications (1)

Publication Number Publication Date
PL450084A1 true PL450084A1 (pl) 2026-04-27

Family

ID=99547499

Family Applications (1)

Application Number Title Priority Date Filing Date
PL450084A PL450084A1 (pl) 2024-10-21 2024-10-21 Sposób otrzymywania sorpcyjnego tlenku manganu

Country Status (1)

Country Link
PL (1) PL450084A1 (pl)

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016207793A1 (en) * 2015-06-22 2016-12-29 Eramet & Comilog Chemicals Sprl Highly pure birnessite and method for the production thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016207793A1 (en) * 2015-06-22 2016-12-29 Eramet & Comilog Chemicals Sprl Highly pure birnessite and method for the production thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
QI FENG ET AL.:: "Journal of the Ceramic Society of Japan (1996) 104(9):897-989", SYNTHESIS OF BIRNESSITE-TYPE LITHIUM MANGANESE OXIDE *
RAMESH CHITRAKAR ET AL.: "Chemistry of Materials (2000) 12(10):3151-3157. DOI:10.1021/cm0000191", A NEW TYPE OF MANGANESE OXIDE MNO2•0.5H2O) DERIVED FROM LI1.6MN1.6O4 AND ITS LITHIUM ION-SIEVE PROPERTIES *
XIAOLING XIAO ET AL.: "Nano Res (2009) 2: 923 930. DOI 10.1007/s12274-009-9094-8", HYDROTHERMAL SYNTHESIS OF ORTHORHOMBIC LIMNO2 NANO-PARTICLES AND LIMNO2 NANORODS AND COMPARISON OF THEIR ELECTROCHEMICAL PERFORMANCES *

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