PL91974B1 - - Google Patents

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Publication number: PL91974B1
Authority: PL; Poland
Prior art keywords: amount; sulfuric acid; reaction mixture; sulphate; propylene
Prior art date: 1973-03-31

Application number

PL16163173A

Other languages

English (en)

Polish (pl)

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1973-03-31

Filing date

1973-03-31

Publication date

1977-03-31

1973-03-31 Application filed filed Critical

1973-03-31 Priority to PL16163173A priority Critical patent/PL91974B1/pl

1977-03-31 Publication of PL91974B1 publication Critical patent/PL91974B1/pl

Links

QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 29
HWBLTYHIEYOAOL-UHFFFAOYSA-N Diisopropyl sulfate Chemical compound CC(C)OS(=O)(=O)OC(C)C HWBLTYHIEYOAOL-UHFFFAOYSA-N 0.000 claims description 23
239000011541 reaction mixture Substances 0.000 claims description 18
QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 13
125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 13
238000000034 method Methods 0.000 claims description 9
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 8
239000012074 organic phase Substances 0.000 claims description 7
239000002253 acid Substances 0.000 claims description 6
239000003513 alkali Substances 0.000 claims description 6
239000007864 aqueous solution Substances 0.000 claims description 6
JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 claims description 6
239000000203 mixture Substances 0.000 claims description 6
239000008346 aqueous phase Substances 0.000 claims description 5
150000004649 carbonic acid derivatives Chemical class 0.000 claims description 5
150000001875 compounds Chemical class 0.000 claims description 4
-1 isopropylamine ions Chemical class 0.000 claims description 4
239000003960 organic solvent Substances 0.000 claims description 4
238000007086 side reaction Methods 0.000 claims description 4
239000000243 solution Substances 0.000 claims description 4
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims description 3
150000002191 fatty alcohols Chemical class 0.000 claims description 3
150000004679 hydroxides Chemical class 0.000 claims description 3
239000002736 nonionic surfactant Substances 0.000 claims description 3
229910021653 sulphate ion Inorganic materials 0.000 claims description 3
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 2
230000002401 inhibitory effect Effects 0.000 claims 2
LWIHDJKSTIGBAC-UHFFFAOYSA-K tripotassium phosphate Chemical compound [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 description 9
239000000126 substance Substances 0.000 description 6
150000002894 organic compounds Chemical class 0.000 description 5
229910000160 potassium phosphate Inorganic materials 0.000 description 5
235000011009 potassium phosphates Nutrition 0.000 description 5
IVNFTPCOZIGNAE-UHFFFAOYSA-N propan-2-yl hydrogen sulfate Chemical compound CC(C)OS(O)(=O)=O IVNFTPCOZIGNAE-UHFFFAOYSA-N 0.000 description 5
238000000926 separation method Methods 0.000 description 5
230000015572 biosynthetic process Effects 0.000 description 4
238000006243 chemical reaction Methods 0.000 description 4
BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 4
230000000694 effects Effects 0.000 description 3
238000000605 extraction Methods 0.000 description 3
239000012451 post-reaction mixture Substances 0.000 description 3
239000011734 sodium Substances 0.000 description 3
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
229910052802 copper Inorganic materials 0.000 description 2
239000010949 copper Substances 0.000 description 2
ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 description 2
239000000839 emulsion Substances 0.000 description 2
239000011790 ferrous sulphate Substances 0.000 description 2
235000003891 ferrous sulphate Nutrition 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
229940085991 phosphate ion Drugs 0.000 description 2
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
229910000027 potassium carbonate Inorganic materials 0.000 description 2
239000001103 potassium chloride Substances 0.000 description 2
WCUXLLCKKVVCTQ-UHFFFAOYSA-M potassium chloride Inorganic materials [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
235000011164 potassium chloride Nutrition 0.000 description 2
229910052939 potassium sulfate Inorganic materials 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
229910052938 sodium sulfate Inorganic materials 0.000 description 2
235000011152 sodium sulphate Nutrition 0.000 description 2
239000002904 solvent Substances 0.000 description 2
238000003786 synthesis reaction Methods 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
239000007832 Na2SO4 Substances 0.000 description 1
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
239000013543 active substance Substances 0.000 description 1
239000002168 alkylating agent Substances 0.000 description 1
229940100198 alkylating agent Drugs 0.000 description 1
150000001450 anions Chemical class 0.000 description 1
239000001273 butane Substances 0.000 description 1
239000000356 contaminant Substances 0.000 description 1
ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 1
229910000366 copper(II) sulfate Inorganic materials 0.000 description 1
GQDHEYWVLBJKBA-UHFFFAOYSA-H copper(ii) phosphate Chemical compound [Cu+2].[Cu+2].[Cu+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O GQDHEYWVLBJKBA-UHFFFAOYSA-H 0.000 description 1
229960003280 cupric chloride Drugs 0.000 description 1
238000004821 distillation Methods 0.000 description 1
239000008187 granular material Substances 0.000 description 1
230000007062 hydrolysis Effects 0.000 description 1
238000006460 hydrolysis reaction Methods 0.000 description 1
BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 description 1
229910000359 iron(II) sulfate Inorganic materials 0.000 description 1
239000003350 kerosene Substances 0.000 description 1
239000007788 liquid Substances 0.000 description 1
QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
229910052753 mercury Inorganic materials 0.000 description 1
IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
238000006386 neutralization reaction Methods 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
238000005191 phase separation Methods 0.000 description 1
239000011574 phosphorus Substances 0.000 description 1
229910052698 phosphorus Inorganic materials 0.000 description 1
229910052697 platinum Inorganic materials 0.000 description 1
UZTIGBMIZLASSJ-UHFFFAOYSA-M potassium propan-2-yl sulfate Chemical compound S(=O)(=O)(OC(C)C)[O-].[K+] UZTIGBMIZLASSJ-UHFFFAOYSA-M 0.000 description 1
OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 description 1
239000001120 potassium sulphate Substances 0.000 description 1
235000011151 potassium sulphates Nutrition 0.000 description 1
239000001294 propane Substances 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
229930195734 saturated hydrocarbon Natural products 0.000 description 1
229910052709 silver Inorganic materials 0.000 description 1
239000004332 silver Substances 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
239000011780 sodium chloride Substances 0.000 description 1
FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Inorganic materials [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
239000001488 sodium phosphate Substances 0.000 description 1
229910000162 sodium phosphate Inorganic materials 0.000 description 1
238000006277 sulfonation reaction Methods 0.000 description 1

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Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

PL16163173A 1973-03-31 1973-03-31 PL91974B1 (pt)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
PL16163173A PL91974B1 (pt)	1973-03-31	1973-03-31

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
PL16163173A PL91974B1 (pt)	1973-03-31	1973-03-31

Publications (1)

Publication Number	Publication Date
PL91974B1 true PL91974B1 (pt)	1977-03-31

Family

ID=19962076

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
PL16163173A PL91974B1 (pt)	1973-03-31	1973-03-31

Country Status (1)

Country	Link
PL (1)	PL91974B1 (pt)

1973
- 1973-03-31 PL PL16163173A patent/PL91974B1/pl unknown

Publication	Publication Date	Title
DE68906975T2 (de)	1993-10-14	Verfahren zur Herstellung von Sulfonaten von internen Olefinen.
US3617546A (en)	1971-11-02	Removal of organic compounds by liquid membrane
US4091014A (en)	1978-05-23	Process for making ether sulfonates
US4147638A (en)	1979-04-03	Sulfonation of crude oils to produce petroleum sulfonates
US3931339A (en)	1976-01-06	Removal and neutralisation of acid catalyst from products of cumene hydroperoxide cleavage
US2715646A (en)	1955-08-16	Manufacture of dhsopropylbenzene hydroperoxides
US3966594A (en)	1976-06-29	Treatment of aqueous waste solution
DE1215695B (de)	1966-05-05	Verfahren zur Herstellung hellfarbiger Olefinsulfonierungsprodukte bzw. der entsprechenden Sulfonate
KR100891230B1 (ko)	2009-04-01	쿠멘 하이드로퍼옥사이드를 제조하는 방법 및 시스템
KR910001610B1 (ko)	1991-03-16	갈륨포함 수용액에서 갈륨회수방법 및 갈륨 착화합물
US2687420A (en)	1954-08-24	Process for the neutralization of sulfonated products suitable as detergents
DE69310007T2 (de)	1997-12-18	Herstellung eines organischen Salzes des seltenen Erdmetalls
US2806875A (en)	1957-09-17	Preparation of alkaryl sulfonic acids
JP7771765B2 (ja)	2025-11-18	フェノールの製造方法及びフェノール組成物
GB1585030A (en)	1981-02-18	Preparation of salts of secondary monoalkyl sulphuric acids
PL74243B1 (pt)	1974-10-31
US2820056A (en)	1958-01-14	Alkaryl sulfonates
US4241229A (en)	1980-12-23	Recovery of nitrated aromatic compounds from nitration wash liquors
US2843626A (en)	1958-07-15	Sulfonation process
US4175092A (en)	1979-11-20	Extraction process
US4087469A (en)	1978-05-02	Method of producing 2,2 '-methylenebis(4,6-dialkylphenols)
JP7683268B2 (ja)	2025-05-27	フェノールの製造方法
US4361520A (en)	1982-11-30	Refinement of sulfonated hydrocarbons
US2497152A (en)	1950-02-14	Purification of petroleum sulfonates
EP0009851B1 (de)	1982-01-20	Verfahren zur Herstellung von araliphatischen Dihydroperoxiden