PL9524B1 - The method of obtaining active substances of the reproductive glands in a water-soluble form. - Google Patents
The method of obtaining active substances of the reproductive glands in a water-soluble form. Download PDFInfo
- Publication number
- PL9524B1 PL9524B1 PL9524A PL952427A PL9524B1 PL 9524 B1 PL9524 B1 PL 9524B1 PL 9524 A PL9524 A PL 9524A PL 952427 A PL952427 A PL 952427A PL 9524 B1 PL9524 B1 PL 9524B1
- Authority
- PL
- Poland
- Prior art keywords
- water
- soluble form
- active substances
- obtaining active
- reproductive glands
- Prior art date
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- 210000004907 gland Anatomy 0.000 title claims description 4
- 230000001850 reproductive effect Effects 0.000 title claims description 4
- 239000013543 active substance Substances 0.000 title claims description 3
- 238000000034 method Methods 0.000 title claims description 3
- 229940088597 hormone Drugs 0.000 claims description 6
- 239000005556 hormone Substances 0.000 claims description 6
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 8
- 239000007864 aqueous solution Substances 0.000 description 4
- 239000001569 carbon dioxide Substances 0.000 description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- UUCCCPNEFXQJEL-UHFFFAOYSA-L strontium dihydroxide Chemical compound [OH-].[OH-].[Sr+2] UUCCCPNEFXQJEL-UHFFFAOYSA-L 0.000 description 1
- 229910001866 strontium hydroxide Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Description
Przy otrzymywaniu czynnych skladni¬ ków gruczolów rozrodczych przez zwykla ekstrakcje odpowiednich narzadów, zmy- dlenie wyciagu, oddzielenie i oczyszczenie czesci niedajacej sie zmydlic i zawiera¬ jacej suihstaniqje czynne, otrzymuje sie materjaly oleiste.Wykryto, z£ czynne substancje gruczo¬ lów rozrodczych (hormony) mozna otrzy¬ mywac w postaci rozpuszczalnej w wo¬ dzie przez dzialanie ziem alkalicznych na oleisty produkt, otrzymany sposobem wy¬ zej wymienionym lub inlnym, Z otrzyma¬ nych przy tem przesaczów przez wprowa¬ dzanie dwutlenku wegla straca isie alkalja ziemne w postaci weglanów i oddziela te ostatnie. Pozostale roztwoiy wodne hor¬ monu steza sie.Przyklad L W 100 czesciach objeto* sciowych alkoholu rozpuszcza sie 3 czesci wagowe oleju hormonowego, otrzymanego wyzej wymienionym sposobem, poczem do roztworu, .silnie mieszajac, doprowadza sie ptowoli 500 czesci objetosciowych stezone¬ go goracego wodorotlenku barwnego, o- grzewa sie do Wrzenia i gotuje przez pe¬ wien czas. Nastepnie ido goracej cieczy wprowadza sie dwutlenek wegla i odsacza utworzony weglan baru. Wprowadzanie dwutlenku wegla powtarza sie, dopóki nie przestanie -wytwarzac sie zmetnienie. Po¬ zostaly wodny roztwór hormonu steza sie do odpowiedniej koncentracji.Przyklad IL 3 czesci wagowe oczy¬ szczonego oleijiu hormonowego rozpuszcza sie w 30 czesciach objetosciowych alkoho¬ lu i rozrabia z wodorotlenkiem wapnia na gesta papke, która sie nastepnie przez czas dluzszy gotuje z 500 czesciami objetoscio- wemi wody. Odsacza sie czesc nierozpu- szczona, straca dwutlenkiem wegla i odsa¬ cza od weglanu wapnia. Pozostaje przej¬ rzysty wodny roztwór hormonu, Przy uzyciu wodorotlenku strontu po¬ stepuje isie analogicznie, jak w przykla¬ dach poprzednich.Tak otrzymane wodne roztwory hor¬ monu isa wolne od soli. PL PLWhen the active ingredients of the reproductive glands are obtained by the simple extraction of the appropriate organs, the saponification of the extract, the separation and purification of the part that does not saponate and contains active substances, oily materials are obtained. ) can be obtained in water-soluble form by the action of alkaline earths on the oily product obtained by the above-mentioned method or otherwise. From the feeds obtained at the same time by introducing carbon dioxide, the earth alkali is lost in the form of carbonates and separates the latter. The remaining aqueous solutions of the hormone will become concentrated. , it is heated to boiling and boiled for some time. The carbon dioxide is then introduced into the hot liquid and the barium carbonate formed is filtered off. The carbon dioxide injection is repeated until the formation of turbidity ceases. The remaining aqueous solution of the hormone is concentrated to the appropriate concentration. Example IL 3 parts by weight of the purified hormone oil is dissolved in 30 parts by volume of alcohol and mixed with calcium hydroxide into a thick slurry, which is then cooked for a longer time with 500 parts. by volume of water. The undissolved part is drained off, lost with carbon dioxide and separated from the calcium carbonate. The clear aqueous solution of the hormone remains. With the use of strontium hydroxide, it is analogous to the previous examples. The aqueous solutions of the hormone thus obtained are salt-free. PL PL
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL9524B1 true PL9524B1 (en) | 1928-11-30 |
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