RO84437B1 - Process for preparing e-7-dodecene-1-ol acetate - Google Patents
Process for preparing e-7-dodecene-1-ol acetateInfo
- Publication number
- RO84437B1 RO84437B1 RO107620A RO10762082A RO84437B1 RO 84437 B1 RO84437 B1 RO 84437B1 RO 107620 A RO107620 A RO 107620A RO 10762082 A RO10762082 A RO 10762082A RO 84437 B1 RO84437 B1 RO 84437B1
- Authority
- RO
- Romania
- Prior art keywords
- dodecene
- acetate
- preparing
- tert
- dodecin
- Prior art date
Links
- MUZGQHWTRUVFLG-VOTSOKGWSA-N 7E-Dodecenyl acetate Chemical compound CCCC\C=C\CCCCCCOC(C)=O MUZGQHWTRUVFLG-VOTSOKGWSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- WPSSULGSNPSWLU-CMDGGOBGSA-N (e)-12-[(2-methylpropan-2-yl)oxy]dodec-5-ene Chemical compound CCCC\C=C\CCCCCCOC(C)(C)C WPSSULGSNPSWLU-CMDGGOBGSA-N 0.000 abstract 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 abstract 1
- WETWJCDKMRHUPV-UHFFFAOYSA-N acetyl chloride Chemical compound CC(Cl)=O WETWJCDKMRHUPV-UHFFFAOYSA-N 0.000 abstract 1
- 239000012346 acetyl chloride Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Inventia se refera la un procedeu de preparare a acetatului de E-7-dodecen-1-01, prin reducerea cu sodiu metalic în amoniac lichid a 7-dodecin-1-olului protejat, conform caruia se supune reducerii 1-tert-butoxi-7-dodecina, 1-tert-butoxi-E-7-dodecena astfel obtinuta fiind apoi acetilata cu un amestec de clorura de acetil; acid acetic 1:10.The invention relates to a process for the preparation of E-7-dodecen-1-ol acetate by reduction with sodium metal in liquid ammonia of protected 7-dodecin-1-ol, according to which the 1-tert- 7-dodecene, 1-tert-butoxy-E-7-dodecene thus obtained is then acetylated with a mixture of acetyl chloride; acetic acid 1:10.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO107620A RO84437B1 (en) | 1982-05-21 | 1982-05-21 | Process for preparing e-7-dodecene-1-ol acetate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO107620A RO84437B1 (en) | 1982-05-21 | 1982-05-21 | Process for preparing e-7-dodecene-1-ol acetate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RO84437A2 RO84437A2 (en) | 1984-06-21 |
| RO84437B1 true RO84437B1 (en) | 1984-08-30 |
Family
ID=20111565
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RO107620A RO84437B1 (en) | 1982-05-21 | 1982-05-21 | Process for preparing e-7-dodecene-1-ol acetate |
Country Status (1)
| Country | Link |
|---|---|
| RO (1) | RO84437B1 (en) |
-
1982
- 1982-05-21 RO RO107620A patent/RO84437B1/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| RO84437A2 (en) | 1984-06-21 |
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