RU2012123717A - MEANS FOR REGULATING THE REACTIVITY AND TIME OF GELATINIZATION OF THE RESIN MIXTURE CONTAINING ITS REACTIVE MIXTURE AND ITS APPLICATION - Google Patents

MEANS FOR REGULATING THE REACTIVITY AND TIME OF GELATINIZATION OF THE RESIN MIXTURE CONTAINING ITS REACTIVE MIXTURE AND ITS APPLICATION Download PDF

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RU2012123717A
RU2012123717A RU2012123717/04A RU2012123717A RU2012123717A RU 2012123717 A RU2012123717 A RU 2012123717A RU 2012123717/04 A RU2012123717/04 A RU 2012123717/04A RU 2012123717 A RU2012123717 A RU 2012123717A RU 2012123717 A RU2012123717 A RU 2012123717A
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Армин ПФАЙЛЬ
Йоханнес БРИНКХОРСТ
Дидье ЖИГМЕ
Лука ВАЛЬДЖИМИЛИ
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Хильти Акциенгезельшафт
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Abstract

1. Применение комбинации из соединения общей формулы (I)в которой Rи Rв каждом случае независимо друг от друга означают водород или неразветвленную или разветвленную алкильную группу с 1-20 атомами углерода, а X означает -ORили -NR , причем Rявляется неразветвленной или разветвленной алкильной группой с 1-20 атомами углерода, либо полиалкиленоксидной группой с 2-4 атомами углерода в алкиле, и соединения общей формулы (II)в которой R является водородом, неразветвленной или разветвленной алкильной группой с 1-18 атомами углерода или означает -ORили -NR , причем Rявляется разветвленной или неразветвленной алкильной группой с 1-20 атомами углерода, R' является водородом, неразветвленной или разветвленной алкильной группой с 1-18 атомами углерода, а R" является неразветвленной или разветвленной алкильной группой с 1-18 атомами углерода для регулирования реакционной способности и времени желатинизации смесей смол на основе радикально-отверждающихся соединений.2. Применение по п.1, причем Rи Rв формуле (I) независимо друг от друга означают водород или неразветвленную или разветвленную алкильную группу с 1-8 атомами углерода.3. Применение по п.2, причем Rи Rв формуле (I) независимо друг от друга означают водород или метил.4. Применение по п.3, причем соединением формулы (I) является 2-(диметиламино)пиримидин-5-ол, 2-(диметиламино)-4,6-диметилпиримидин-5-ол или 4,6-диметил-2-(октилокси)пиримидин-5-ол.5. Применение по п.1, причем соединением формулы (II) является 2,6-ди(трет.бутил)-4-метилфенол или 2,6-ди(трет.бутил)-4-гидроксианизол.6. Применение по п.5, причем комбинацией является комбинация (III-1) из 2-(диметиламино)пиримидин-5-ола с 2,6-ди(трет.бутил)-4-метилфенолом; комби1. The use of a combination of a compound of general formula (I) in which R and R in each case, independently of one another, means hydrogen or an unbranched or branched alkyl group with 1-20 carbon atoms, and X means —OR or —NR, wherein R is unbranched or branched alkyl a group with 1-20 carbon atoms, or a polyalkylene oxide group with 2-4 carbon atoms in the alkyl, and a compound of general formula (II) in which R is hydrogen, a straight or branched alkyl group with 1-18 carbon atoms or means —OR or —NR , P whereby R is a branched or unbranched alkyl group with 1-20 carbon atoms, R 'is hydrogen, a unbranched or branched alkyl group with 1-18 carbon atoms, and R "is a unbranched or branched alkyl group with 1-18 carbon atoms to control reactivity and the gelatinization time of the resin mixtures based on the radical curing compounds 2. The use according to claim 1, wherein R and R in the formula (I) independently from each other mean hydrogen or unbranched or branched alkyl groups with 1-8 carbon atoms. 3. The use according to claim 2, wherein R and R in the formula (I) are independently hydrogen or methyl. 4. The use according to claim 3, wherein the compound of formula (I) is 2- (dimethylamino) pyrimidin-5-ol, 2- (dimethylamino) -4,6-dimethylpyrimidin-5-ol or 4,6-dimethyl-2- (octyloxy ) pyrimidin-5-ol. 5. The use according to claim 1, wherein the compound of formula (II) is 2,6-di (tert.butyl) -4-methylphenol or 2,6-di (tert.butyl) -4-hydroxyanisole. The use according to claim 5, wherein the combination is a combination of (III-1) from 2- (dimethylamino) pyrimidin-5-ol with 2,6-di (tert.butyl) -4-methylphenol; combi

Claims (22)

1. Применение комбинации из соединения общей формулы (I)1. The use of a combination of a compound of general formula (I)
Figure 00000001
Figure 00000001
 в которой R1 и R2 в каждом случае независимо друг от друга означают водород или неразветвленную или разветвленную алкильную группу с 1-20 атомами углерода, а X означает -OR3 или -NR3 2, причем R3 является неразветвленной или разветвленной алкильной группой с 1-20 атомами углерода, либо полиалкиленоксидной группой с 2-4 атомами углерода в алкиле, и соединения общей формулы (II)in which R 1 and R 2 in each case, independently of one another, are hydrogen or an unbranched or branched alkyl group with 1-20 carbon atoms, and X is —OR 3 or —NR 3 2 , wherein R 3 is a unbranched or branched alkyl group with 1-20 carbon atoms, or a polyalkylene oxide group with 2-4 carbon atoms in alkyl, and the compounds of general formula (II)
Figure 00000002
Figure 00000002
 в которой R является водородом, неразветвленной или разветвленной алкильной группой с 1-18 атомами углерода или означает -OR3 или -NR3 2, причем R3 является разветвленной или неразветвленной алкильной группой с 1-20 атомами углерода, R' является водородом, неразветвленной или разветвленной алкильной группой с 1-18 атомами углерода, а R" является неразветвленной или разветвленной алкильной группой с 1-18 атомами углерода для регулирования реакционной способности и времени желатинизации смесей смол на основе радикально-отверждающихся соединений.in which R is hydrogen, an unbranched or branched alkyl group with 1-18 carbon atoms or means —OR 3 or —NR 3 2 , wherein R 3 is a branched or unbranched alkyl group with 1-20 carbon atoms, R 'is hydrogen, unbranched or a branched alkyl group with 1-18 carbon atoms, and R "is an unbranched or branched alkyl group with 1-18 carbon atoms to control the reactivity and gelation time of radical mixtures of resins based on radically-cured compounds. 2. Применение по п.1, причем R1 и R2 в формуле (I) независимо друг от друга означают водород или неразветвленную или разветвленную алкильную группу с 1-8 атомами углерода.2. The use according to claim 1, wherein R 1 and R 2 in the formula (I) independently from each other mean hydrogen or an unbranched or branched alkyl group with 1-8 carbon atoms. 3. Применение по п.2, причем R1 и R2 в формуле (I) независимо друг от друга означают водород или метил.3. The use according to claim 2, wherein R 1 and R 2 in the formula (I) are independently hydrogen or methyl. 4. Применение по п.3, причем соединением формулы (I) является 2-(диметиламино)пиримидин-5-ол, 2-(диметиламино)-4,6-диметилпиримидин-5-ол или 4,6-диметил-2-(октилокси)пиримидин-5-ол.4. The use according to claim 3, wherein the compound of formula (I) is 2- (dimethylamino) pyrimidin-5-ol, 2- (dimethylamino) -4,6-dimethylpyrimidin-5-ol or 4,6-dimethyl-2- (octyloxy) pyrimidin-5-ol. 5. Применение по п.1, причем соединением формулы (II) является 2,6-ди(трет.бутил)-4-метилфенол или 2,6-ди(трет.бутил)-4-гидроксианизол.5. The use according to claim 1, wherein the compound of formula (II) is 2,6-di (tert.butyl) -4-methylphenol or 2,6-di (tert.butyl) -4-hydroxyanisole. 6. Применение по п.5, причем комбинацией является комбинация (III-1) из 2-(диметиламино)пиримидин-5-ола с 2,6-ди(трет.бутил)-4-метилфенолом; комбинация (III-2) из 2-(диметиламино)-4,6-диметилпиримидин-5-ола с 2,6-ди(трет.бутил)-4-гидроксианизолом или комбинация (III-3) из 4,6-диметил-2-(октилокси)пиримидин-5-ола с 2,6-ди(трет.бутил)-4-метилфенолом.6. The use according to claim 5, wherein the combination is a combination of (III-1) of 2- (dimethylamino) pyrimidin-5-ol with 2,6-di (tert.butyl) -4-methylphenol; a combination of (III-2) from 2- (dimethylamino) -4,6-dimethylpyrimidin-5-ol with 2,6-di (tert.butyl) -4-hydroxyanisole or a combination of (III-3) from 4,6-dimethyl -2- (octyloxy) pyrimidin-5-ol with 2,6-di (tert.butyl) -4-methylphenol. 7. Применение по одному из пп.1-6, причем молярное отношение соединения формулы (I) к соединению формулы (II) составляет от 1:1 до 1:10.7. The use according to one of claims 1 to 6, wherein the molar ratio of the compound of formula (I) to the compound of formula (II) is from 1: 1 to 1:10. 8. Смесь смол, содержащая, по меньшей мере, одно радикально-полимеризующееся соединение, при необходимости, реакционно-способный разбавитель и средство для регулирования реакционной способности и времени желатинизации, причем средство для регулирования реакционной способности и времени желатинизации является комбинацией соединения общей формулы (I)8. A mixture of resins containing at least one radical polymerizable compound, if necessary, a reactive diluent and a means for controlling the reactivity and gelation time, and a means for regulating the reactivity and gelation time is a combination of a compound of the general formula (I )
Figure 00000001
Figure 00000001
 в которой R1 и R2 в каждом случае независимо друг от друга означают водород, неразветвленную или разветвленную алкильную группу с 1-20 атомами углерода, а X означает -OR3 или -NR3 2, причем R3 является неразветвленной или разветвленной алкильной группой с 1-20 атомами углерода, либо полиалкиленоксидной группой с 2-4 атомами углерода в алкиле, и соединения общей формулы (II)in which R 1 and R 2 in each case, independently of one another, are hydrogen, an unbranched or branched alkyl group with 1-20 carbon atoms, and X is —OR 3 or —NR 3 2 , wherein R 3 is a unbranched or branched alkyl group with 1-20 carbon atoms, or a polyalkylene oxide group with 2-4 carbon atoms in alkyl, and the compounds of general formula (II)
Figure 00000003
Figure 00000003
 в которой R является водородом, неразветвленной или разветвленной алкильной группой с 1-18 атомами углерода или означает -OR3 или -NR3 2, причем R3 является разветвленной или неразветвленной алкильной группой с 1-20 атомами углерода, R' является водородом, неразветвленной или разветвленной алкильной группой с 1-18 атомами углерода, а R" является неразветвленной или разветвленной алкильной группой с 1-18 атомами углерода.in which R is hydrogen, an unbranched or branched alkyl group with 1-18 carbon atoms or means —OR 3 or —NR 3 2 , wherein R 3 is a branched or unbranched alkyl group with 1-20 carbon atoms, R 'is hydrogen, unbranched or a branched alkyl group with 1-18 carbon atoms, and R "is an unbranched or branched alkyl group with 1-18 carbon atoms. 9. Смесь смол по п.8, причем R1 и R2 в формуле (I) независимо друг от друга означают водород, разветвленную или неразветвленную алкильную группу с 1-8 атомами углерода.9. The resin mixture of claim 8, wherein R 1 and R 2 in the formula (I) independently of one another are hydrogen, a branched or unbranched alkyl group with 1-8 carbon atoms. 10. Смесь смол по п.9, причем R1 и R2 в формуле (I) независимо друг от друга означают водород или метил.10. The mixture of resins according to claim 9, wherein R 1 and R 2 in the formula (I) are independently hydrogen or methyl. 11. Смесь смол по п.10, причем средством (с) для регулирования реакционной способности и времени желатинизации является 2-(диметиламино)пиримидин-5-ол, 2-(диметиламино)-4,6-диметилпири-мидин-5-ол или 4,6-диметил-2-(октилокси)пиримидин-5-ол.11. The resin mixture of claim 10, wherein the means (c) for controlling the reactivity and gelation time is 2- (dimethylamino) pyrimidin-5-ol, 2- (dimethylamino) -4,6-dimethylpyri-midin-5-ol or 4,6-dimethyl-2- (octyloxy) pyrimidin-5-ol. 12. Смесь смол по п.8, причем соединением формулы (II) является 2,6-ди(трет.бутил)-4-метилфенолом или 2,6-ди(трет.бутил)-4-гидроксианизолом.12. The resin mixture of claim 8, wherein the compound of formula (II) is 2,6-di (tert.butyl) -4-methylphenol or 2,6-di (tert.butyl) -4-hydroxyanisole. 13. Смесь смол по п.12, причем средством для регулирования времени желатинизации и реакционной способности являются комбинация (III-1) из 2-(диметиламино)пиримидин-5-ола с 2,6-ди(трет.бутил)-4-метилфенолом; комбинация (III-2) из 2-(диметиламино)-4,6-диметилпиримидин-5-ола с 2,6-ди(трет.бутил)-4-гидроксианизолом или комбинация (III-3) из 4,6-диметил-2-(октилокси)-пиримидин-5-ола с 2,6-ди(трет.бутил)-4-метилфенолом.13. The resin mixture of claim 12, wherein the combination of (III-1) of 2- (dimethylamino) pyrimidin-5-ol with 2,6-di (tert.butyl) -4- is a means for controlling the gelation time and reactivity methylphenol; a combination of (III-2) from 2- (dimethylamino) -4,6-dimethylpyrimidin-5-ol with 2,6-di (tert.butyl) -4-hydroxyanisole or a combination of (III-3) from 4,6-dimethyl -2- (octyloxy) pyrimidin-5-ol with 2,6-di (tert.butyl) -4-methylphenol. 14. Смесь смол по одному из пп.8-13, причем молярное отношение соединения формулы (I) к соединению формулы (II) составляет от 1:1 до 1:10.14. The resin mixture according to one of claims 8 to 13, wherein the molar ratio of the compound of formula (I) to the compound of formula (II) is from 1: 1 to 1:10. 15. Смесь смол по одному из пп.8-13, содержащая дополнительно ускоритель для средства отверждения.15. The resin mixture according to one of claims 8 to 13, further comprising an accelerator for the curing agent. 16. Реакционноспособный строительный раствор смол, содержащий смесь смол по одному из пп.8-15 и неорганические инертные добавки.16. A reactive resin mortar containing a mixture of resins according to one of claims 8 to 15 and inorganic inert additives. 17. Двухкомпонентная система строительного раствора, содержащая в качестве А-компонента реакционноспособный строительный раствор смол по пункту 16 и в качестве В-компонента находящийся отдельно отвердитель для ингибирования реакционной способности.17. A two-component mortar system containing, as an A-component, a reactive mortar of resins according to paragraph 16 and, as a B-component, a separate hardener for inhibiting reactivity. 18. Двухкомпонентная система строительного раствора по п.17, причем отвердитель содержит неорганический или органический пероксид в качестве средства для отверждения.18. A two-component mortar system according to claim 17, wherein the hardener contains inorganic or organic peroxide as a curing agent. 19. Двухкомпонентная система строительного раствора по п.17, причем отвердитель дополнительно содержит неорганические инертные наполнители.19. The two-component mortar system according to claim 17, wherein the hardener further comprises inorganic inert fillers. 20. Двухкомпонентная система строительного раствора по одному из пп.17-19, причем А-компонент помимо реакционно-способного строительного раствора смол дополнительно содержит гидравлически затвердевающее или поликонденсирующееся неорганическое соединение, а В-компонент средства для отверждения дополнительно содержит воду.20. A two-component mortar system according to one of claims 17-19, wherein the A component, in addition to the reactive mortar resins, further comprises a hydraulically settable or polycondensable inorganic compound, and the B component of the curing agent further comprises water. 21. Применение двухкомпонентной системы строительного раствора по одному из пп.17-20 для химического закрепления.21. The use of a two-component mortar system according to one of paragraphs.17-20 for chemical fixing. 22. Патрон, картуш или пленочный пакет, содержащие двухкомпонентную систему строительного раствора по одному из пп.17-20, включающие две или более отделенные друг от друга камеры, в которых находятся реакционноспособный строительный раствор смол или отвердитель. 22. A cartridge, cartridge, or film bag containing a two-component mortar system according to one of claims 17-20, including two or more chambers separated from each other, in which a reactive mortar resins or hardener are located.
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