RU2543177C2 - Способ концентрирования водного раствора пероксида водорода - Google Patents

Способ концентрирования водного раствора пероксида водорода Download PDF

Info

Publication number: RU2543177C2
Authority: RU; Russia
Prior art keywords: distillation column; hydrogen peroxide; preliminary; secondary steam; concentrated
Prior art date: 2010-08-25

Application number

RU2013112789/05A

Other languages

English (en)

Russian (ru)

Other versions

RU2013112789A (ru

Inventor

Хубертус АЙКХОФФ

Флориан ЛОДЕ

Эдуардо АРЕВАЛО

Марк БРЕНДЕЛЬ

Клаудиа ВАЛЛЕРТ

Original Assignee

Эвоник Дегусса Гмбх

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2010-08-25

Filing date

2011-07-29

Publication date

2015-02-27

Family has litigation

First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=44509295&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=RU2543177(C2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.

2011-07-29 Application filed by Эвоник Дегусса Гмбх filed Critical Эвоник Дегусса Гмбх

2014-09-27 Publication of RU2013112789A publication Critical patent/RU2013112789A/ru

2015-02-27 Application granted granted Critical

2015-02-27 Publication of RU2543177C2 publication Critical patent/RU2543177C2/ru

Links

MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title claims abstract description 148
238000000034 method Methods 0.000 title claims abstract description 41
238000004821 distillation Methods 0.000 claims abstract description 84
238000001704 evaporation Methods 0.000 claims abstract description 44
230000008020 evaporation Effects 0.000 claims abstract description 38
239000007864 aqueous solution Substances 0.000 claims abstract description 15
239000007788 liquid Substances 0.000 claims abstract description 12
239000007789 gas Substances 0.000 claims description 6
238000011068 loading method Methods 0.000 claims description 3
229910052751 metal Inorganic materials 0.000 claims description 3
239000002184 metal Substances 0.000 claims description 3
239000000126 substance Substances 0.000 abstract 1
239000000047 product Substances 0.000 description 17
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
238000005265 energy consumption Methods 0.000 description 5
229910052783 alkali metal Inorganic materials 0.000 description 4
PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 description 4
150000004056 anthraquinones Chemical class 0.000 description 4
239000000243 solution Substances 0.000 description 4
239000003381 stabilizer Substances 0.000 description 4
230000003321 amplification Effects 0.000 description 3
238000005516 engineering process Methods 0.000 description 3
238000003199 nucleic acid amplification method Methods 0.000 description 3
238000000746 purification Methods 0.000 description 3
238000010992 reflux Methods 0.000 description 3
150000001340 alkali metals Chemical class 0.000 description 2
238000009833 condensation Methods 0.000 description 2
230000005494 condensation Effects 0.000 description 2
238000000605 extraction Methods 0.000 description 2
239000012535 impurity Substances 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
239000011734 sodium Substances 0.000 description 2
159000000000 sodium salts Chemical class 0.000 description 2
BAERPNBPLZWCES-UHFFFAOYSA-N (2-hydroxy-1-phosphonoethyl)phosphonic acid Chemical compound OCC(P(O)(O)=O)P(O)(O)=O BAERPNBPLZWCES-UHFFFAOYSA-N 0.000 description 1
KXDHJXZQYSOELW-UHFFFAOYSA-N Carbamic acid Chemical class NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 description 1
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical class OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 1
229920000388 Polyphosphate Polymers 0.000 description 1
YDONNITUKPKTIG-UHFFFAOYSA-N [Nitrilotris(methylene)]trisphosphonic acid Chemical compound OP(O)(=O)CN(CP(O)(O)=O)CP(O)(O)=O YDONNITUKPKTIG-UHFFFAOYSA-N 0.000 description 1
-1 alkali metal salts Chemical class 0.000 description 1
BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical class OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
229910010293 ceramic material Inorganic materials 0.000 description 1
239000008139 complexing agent Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
239000000356 contaminant Substances 0.000 description 1
239000012043 crude product Substances 0.000 description 1
238000000354 decomposition reaction Methods 0.000 description 1
235000011180 diphosphates Nutrition 0.000 description 1
TVQLLNFANZSCGY-UHFFFAOYSA-N disodium;dioxido(oxo)tin Chemical compound [Na+].[Na+].[O-][Sn]([O-])=O TVQLLNFANZSCGY-UHFFFAOYSA-N 0.000 description 1
239000011552 falling film Substances 0.000 description 1
238000010438 heat treatment Methods 0.000 description 1
238000012856 packing Methods 0.000 description 1
ZJAOAACCNHFJAH-UHFFFAOYSA-N phosphonoformic acid Chemical class OC(=O)P(O)(O)=O ZJAOAACCNHFJAH-UHFFFAOYSA-N 0.000 description 1
PTMHPRAIXMAOOB-UHFFFAOYSA-N phosphoramidic acid Chemical class NP(O)(O)=O PTMHPRAIXMAOOB-UHFFFAOYSA-N 0.000 description 1
239000004033 plastic Substances 0.000 description 1
239000001205 polyphosphate Substances 0.000 description 1
235000011176 polyphosphates Nutrition 0.000 description 1
238000010926 purge Methods 0.000 description 1
238000000926 separation method Methods 0.000 description 1
229940079864 sodium stannate Drugs 0.000 description 1
239000012224 working solution Substances 0.000 description 1

Images

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/013—Separation; Purification; Concentration
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/28—Evaporating with vapour compression
- B01D1/2803—Special features relating to the vapour to be compressed
- B01D1/2806—The vapour is divided in at least two streams and only a part of the vapour is compressed
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/28—Evaporating with vapour compression
- B01D1/284—Special features relating to the compressed vapour
- B01D1/2856—The compressed vapour is used for heating a reboiler or a heat exchanger outside an evaporator
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/28—Evaporating with vapour compression
- B01D1/289—Compressor features (e.g. constructions, details, cooling, lubrication, driving systems)
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/148—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/037—Stabilisation by additives
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/19—Sidestream

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Inorganic Chemistry (AREA)
Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

RU2013112789/05A 2010-08-25 2011-07-29 Способ концентрирования водного раствора пероксида водорода RU2543177C2 (ru)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
DE102010039748.2		2010-08-25
DE102010039748A DE102010039748A1 (de)	2010-08-25	2010-08-25	Verfahren zum Konzentrieren von wässriger Wasserstoffperoxidlösung
PCT/EP2011/063069 WO2012025333A1 (de)	2010-08-25	2011-07-29	Verfahren zum konzentrieren von wässriger wasserstoffperoxidlösung

Publications (2)

Publication Number	Publication Date
RU2013112789A RU2013112789A (ru)	2014-09-27
RU2543177C2 true RU2543177C2 (ru)	2015-02-27

Family

ID=44509295

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
RU2013112789/05A RU2543177C2 (ru)	2010-08-25	2011-07-29	Способ концентрирования водного раствора пероксида водорода

Country Status (17)

Country	Link
US (1)	US9206047B2 (pl)
EP (1)	EP2609032B1 (pl)
KR (1)	KR101477938B1 (pl)
CN (1)	CN103068725B (pl)
AR (1)	AR082538A1 (pl)
CA (1)	CA2809323C (pl)
DE (1)	DE102010039748A1 (pl)
ES (1)	ES2525086T3 (pl)
MY (1)	MY157400A (pl)
PL (1)	PL2609032T3 (pl)
PT (1)	PT2609032E (pl)
RU (1)	RU2543177C2 (pl)
SG (1)	SG187884A1 (pl)
SI (1)	SI2609032T1 (pl)
TW (1)	TWI461353B (pl)
UY (1)	UY33573A (pl)
WO (1)	WO2012025333A1 (pl)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN103204476A (zh) *	2013-04-08	2013-07-17	安徽晋煤中能化工股份有限公司	一种27.5%过氧化氢稀品溶液浓缩为50%过氧化氢浓品溶液的浓缩精馏优化生产系统及其方法
PL403721A1 (pl)	2013-04-30	2014-11-10	Instytut Lotnictwa	Sposób otrzymywania nadtlenku wodoru, zwłaszcza klasy HTP do zastosowań napędowych i układ do destylacji próżniowej
PL233084B1 (pl)	2015-07-14	2019-08-30	Inst Lotnictwa	Jednostopniowy sposób otrzymywania nadtlenku wodoru klasy HTP ( High Test Peroxide) do zastosowań napędowych i układ do jego otrzymywania
CN109019521B (zh) *	2018-10-31	2023-07-25	湖南百利工程科技股份有限公司	一种双氧水浓缩提纯装置及其在双氧水浓缩提纯中的应用
CN109589624A (zh) *	2019-01-31	2019-04-09	滨化集团股份有限公司	一种过氧化氢浓缩一体化蒸发器
CL2021001192A1 (es)	2020-05-28	2021-11-19	Evonik Operations Gmbh	Dispositivo y proceso para producir peróxido de hidrógeno mediante un proceso de antraquinona
EP4063355A1 (en)	2021-03-22	2022-09-28	Evonik Operations GmbH	Integrated process and plant for making styrene and propene oxide
HUE071346T2 (hu)	2021-05-10	2025-08-28	Evonik Operations Gmbh	Integrált berendezés és integrált eljárás propén-oxid elõállítására
AU2022274987A1 (en) *	2021-05-10	2023-12-21	Evonik Operations Gmbh	Optimized steam network for the ao process
CN113289364B (zh) *	2021-05-18	2023-04-11	重庆宏大化工科技有限公司	一种用于双氧水生产的浓缩装置及其使用方法
CN117602584A (zh) *	2023-10-18	2024-02-27	兴国兴氟化工有限公司	一种双氧水及双氧水的纯化方法
PL447380A1 (pl)	2023-12-29	2025-06-30	Jakusz Spacetech Spółka Z Ograniczoną Odpowiedzialnością	Sposób wytwarzania wysoko stężonego nadtlenku wodoru

Citations (4)

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Publication number	Priority date	Publication date	Assignee	Title
DE1084249B (de) *	1958-03-15	1960-06-30	Herbert Schmidt Dipl Phys	Verfahren zur Verwertung der Kondensationswaerme aus Wasserstoff-peroxyd-Destillieranlagen
GB907421A (en) *	1960-04-12	1962-10-03	Kali Chemie Ag	Improvements in or relating to the concentration of dilute aqueous solutions of hydrogen peroxide
US5171407A (en) *	1989-09-22	1992-12-15	Sulzer Brothers Limited	Distillation plant for producing hydrogen peroxide
RU2237614C1 (ru) *	2000-08-11	2004-10-10	Полимери Эуропа С.П.А.	Способ получения пероксида водорода

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US2701233A (en)	1952-04-09	1955-02-01	Eastman Kodak Co	Azeotropic distillation
NL176744B (nl) *	1952-04-24		Helopharm Petrik Co Kg	Werkwijze voor de bereiding van tegen orthostatische dysregulatie werkzame preparaten.
BE756015A (fr) *	1969-09-10	1971-02-15	Degussa	Procede pour la preparation de peroxyde d'hydrogene (e)
US4566947A (en) *	1984-09-27	1986-01-28	Hidemasa Tsuruta	Method of separating a mixed liquid into light and heavy fractions by distillation
CN85103225B (zh)	1985-04-01	1988-09-28	化学工业部黎明化工研究院	过氧化氢的精制浓缩
JP3328854B2 (ja) *	1993-09-13	2002-09-30	三菱瓦斯化学株式会社	過酸化水素の濃縮精製方法
US5670028A (en) *	1994-11-22	1997-09-23	Ube Industries, Ltd.	Process for preparing high purity hydrogen peroxide aqueous solution
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EP1090663A1 (en) *	1999-10-05	2001-04-11	SOLVAY (Société Anonyme)	Process for the manufacture of concentrated solutions

2010
- 2010-08-25 DE DE102010039748A patent/DE102010039748A1/de not_active Withdrawn
2011
- 2011-07-29 PL PL11748326T patent/PL2609032T3/pl unknown
- 2011-07-29 CA CA2809323A patent/CA2809323C/en active Active
- 2011-07-29 SG SG2013011895A patent/SG187884A1/en unknown
- 2011-07-29 CN CN201180040752.5A patent/CN103068725B/zh active Active
- 2011-07-29 US US13/817,797 patent/US9206047B2/en active Active
- 2011-07-29 PT PT117483263T patent/PT2609032E/pt unknown
- 2011-07-29 SI SI201130332T patent/SI2609032T1/sl unknown
- 2011-07-29 KR KR1020137007247A patent/KR101477938B1/ko active Active
- 2011-07-29 EP EP11748326.3A patent/EP2609032B1/de active Active
- 2011-07-29 ES ES11748326.3T patent/ES2525086T3/es active Active
- 2011-07-29 RU RU2013112789/05A patent/RU2543177C2/ru active
- 2011-07-29 MY MYPI2013000508A patent/MY157400A/en unknown
- 2011-07-29 WO PCT/EP2011/063069 patent/WO2012025333A1/de not_active Ceased
- 2011-08-22 TW TW100129947A patent/TWI461353B/zh not_active IP Right Cessation
- 2011-08-24 AR ARP110103073A patent/AR082538A1/es not_active Application Discontinuation
- 2011-08-24 UY UY0001033573A patent/UY33573A/es not_active Application Discontinuation

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE1084249B (de) *	1958-03-15	1960-06-30	Herbert Schmidt Dipl Phys	Verfahren zur Verwertung der Kondensationswaerme aus Wasserstoff-peroxyd-Destillieranlagen
GB907421A (en) *	1960-04-12	1962-10-03	Kali Chemie Ag	Improvements in or relating to the concentration of dilute aqueous solutions of hydrogen peroxide
US5171407A (en) *	1989-09-22	1992-12-15	Sulzer Brothers Limited	Distillation plant for producing hydrogen peroxide
RU2237614C1 (ru) *	2000-08-11	2004-10-10	Полимери Эуропа С.П.А.	Способ получения пероксида водорода

Also Published As

Publication number	Publication date
ES2525086T3 (es)	2014-12-17
CN103068725A (zh)	2013-04-24
TWI461353B (zh)	2014-11-21
SG187884A1 (en)	2013-03-28
KR101477938B1 (ko)	2014-12-30
WO2012025333A1 (de)	2012-03-01
AR082538A1 (es)	2012-12-12
CN103068725B (zh)	2015-06-17
MY157400A (en)	2016-06-15
UY33573A (es)	2012-03-30
CA2809323C (en)	2017-05-16
US20130146438A1 (en)	2013-06-13
TW201223857A (en)	2012-06-16
KR20130081698A (ko)	2013-07-17
US9206047B2 (en)	2015-12-08
EP2609032A1 (de)	2013-07-03
EP2609032B1 (de)	2014-10-01
DE102010039748A1 (de)	2012-03-01
CA2809323A1 (en)	2012-03-01
PL2609032T3 (pl)	2015-03-31
PT2609032E (pt)	2014-12-05
SI2609032T1 (sl)	2015-01-30
RU2013112789A (ru)	2014-09-27

Legal Events

Date	Code	Title	Description
2020-04-23	PD4A	Correction of name of patent owner

Publication	Publication Date	Title
RU2543177C2 (ru)	2015-02-27	Способ концентрирования водного раствора пероксида водорода
US3294650A (en)	1966-12-27	Process for concentrating sulfuric acid in a quartz rectifying column
JP4575459B2 (ja)	2010-11-04	メタノールの回収方法
WO2011027787A1 (ja)	2011-03-10	含水有機物の無水化方法
CN102757019A (zh)	2012-10-31	一种双氧水的浓缩与提纯系统及方法
KR102948542B1 (ko)	2026-04-06	산업적 규모의 ε-카프로락탐 및 황산암모늄의 제조를 위한 방법 및 플랜트
JP2018008986A (ja)	2018-01-18	ニトロベンゼンの製造のための方法およびプラント
NO125466B (pl)	1972-09-11
US2741584A (en)	1956-04-10	Process and apparatus for concentrating hydrogen peroxide
KR101380032B1 (ko)	2014-04-01	1,2-디클로로에탄 정제 및 연관된 수산화나트륨액 증발농축을 위한 증류탑 가동 방법
JP7607663B2 (ja)	2024-12-27	復水を処理するための分離塔及びその方法
CN101084176B (zh)	2012-12-05	回收甲醇的方法
FI97538C (fi)	1997-01-10	Menetelmä vetyperoksidin oleellisesti puhtaan vesiliuoksen valmistamiseksi
US2169128A (en)	1939-08-08	Method of producing hydrogen peroxide from solutions
KR20050091706A (ko)	2005-09-15	하이드록실아민 수용액의 제조방법
RU2353575C1 (ru)	2009-04-27	Двухстадийный способ выделения 40-60% водного раствора пероксида водорода
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KR100307728B1 (ko)	2004-08-25	붕산의 분리방법
SU709522A1 (ru)	1980-01-15	Способ получени бромистоводородной кислоты
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KR20130134894A (ko)	2013-12-10	알칸올의 제조 장치
UA54428C2 (uk)	2003-03-17	Спосіб виділення циклогексану