SE434123B - Forfarande for selektiv extrahering av metalljoner ur en vattenlosning - Google Patents

Forfarande for selektiv extrahering av metalljoner ur en vattenlosning

Info

Publication number: SE434123B
Authority: SE; Sweden
Prior art keywords: ions; process according; oxime; fatty acid; extractant
Prior art date: 1977-03-09

Application number

SE7802594A

Other languages

English (en)

Swedish (sv)

Other versions

SE7802594L (sv

Inventor

M Tels

J P Lotens

H P M Kivits

Original Assignee

Stamicarbon

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1977-03-09

Filing date

1978-03-07

Publication date

1984-07-09

1978-03-07 Application filed by Stamicarbon filed Critical Stamicarbon

1978-09-10 Publication of SE7802594L publication Critical patent/SE7802594L/xx

1984-07-09 Publication of SE434123B publication Critical patent/SE434123B/sv

Links

238000000605 extraction Methods 0.000 title claims description 28
238000000034 method Methods 0.000 title claims description 24
229910021645 metal ion Inorganic materials 0.000 title claims description 8
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title description 3
150000002500 ions Chemical class 0.000 claims description 36
239000012074 organic phase Substances 0.000 claims description 21
239000008346 aqueous phase Substances 0.000 claims description 20
235000014113 dietary fatty acids Nutrition 0.000 claims description 20
229930195729 fatty acid Natural products 0.000 claims description 20
239000000194 fatty acid Substances 0.000 claims description 20
150000004665 fatty acids Chemical class 0.000 claims description 20
239000000203 mixture Chemical group 0.000 claims description 19
229910052802 copper Inorganic materials 0.000 claims description 16
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims description 15
LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 15
QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 15
ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims description 15
239000005642 Oleic acid Substances 0.000 claims description 15
QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 15
229910052759 nickel Inorganic materials 0.000 claims description 15
ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 15
VEZUQRBDRNJBJY-UHFFFAOYSA-N cyclohexanone oxime Chemical compound ON=C1CCCCC1 VEZUQRBDRNJBJY-UHFFFAOYSA-N 0.000 claims description 14
239000007864 aqueous solution Substances 0.000 claims description 13
150000002923 oximes Chemical class 0.000 claims description 12
235000021122 unsaturated fatty acids Nutrition 0.000 claims description 5
150000004670 unsaturated fatty acids Chemical group 0.000 claims description 5
238000000926 separation method Methods 0.000 claims description 4
-1 aliphatic oxime Chemical class 0.000 claims description 3
238000002425 crystallisation Methods 0.000 claims description 3
230000008025 crystallization Effects 0.000 claims description 3
150000004671 saturated fatty acids Chemical class 0.000 claims description 3
235000003441 saturated fatty acids Nutrition 0.000 claims description 3
OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 claims description 2
DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 claims description 2
235000020661 alpha-linolenic acid Nutrition 0.000 claims description 2
235000020778 linoleic acid Nutrition 0.000 claims description 2
OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 claims description 2
229960004488 linolenic acid Drugs 0.000 claims description 2
KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 claims description 2
230000010349 pulsation Effects 0.000 claims description 2
238000000746 purification Methods 0.000 claims description 2
241000080590 Niso Species 0.000 claims 1
230000000737 periodic effect Effects 0.000 claims 1
PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 25
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 18
238000002474 experimental method Methods 0.000 description 14
229910052725 zinc Inorganic materials 0.000 description 9
229910052804 chromium Inorganic materials 0.000 description 8
239000000243 solution Substances 0.000 description 8
238000002156 mixing Methods 0.000 description 6
238000005192 partition Methods 0.000 description 6
239000012071 phase Substances 0.000 description 6
239000002253 acid Substances 0.000 description 5
239000002904 solvent Substances 0.000 description 4
238000010586 diagram Methods 0.000 description 3
230000000694 effects Effects 0.000 description 3
150000004679 hydroxides Chemical class 0.000 description 3
229910052742 iron Inorganic materials 0.000 description 3
239000003350 kerosene Substances 0.000 description 3
239000007788 liquid Substances 0.000 description 3
239000002184 metal Substances 0.000 description 3
229910052751 metal Inorganic materials 0.000 description 3
239000012454 non-polar solvent Substances 0.000 description 3
238000004062 sedimentation Methods 0.000 description 3
NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 2
UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 description 2
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
230000002378 acidificating effect Effects 0.000 description 2
238000009835 boiling Methods 0.000 description 2
239000013078 crystal Substances 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 2
NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 2
238000005191 phase separation Methods 0.000 description 2
150000003839 salts Chemical class 0.000 description 2
239000007787 solid Substances 0.000 description 2
239000011343 solid material Substances 0.000 description 2
WHXCGIRATPOBAY-VOTSOKGWSA-N (ne)-n-hexan-2-ylidenehydroxylamine Chemical compound CCCC\C(C)=N\O WHXCGIRATPOBAY-VOTSOKGWSA-N 0.000 description 1
QQZOPKMRPOGIEB-UHFFFAOYSA-N 2-Oxohexane Chemical compound CCCCC(C)=O QQZOPKMRPOGIEB-UHFFFAOYSA-N 0.000 description 1
VEQPNABPJHWNSG-UHFFFAOYSA-N Nickel(2+) Chemical compound [Ni+2] VEQPNABPJHWNSG-UHFFFAOYSA-N 0.000 description 1
CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
230000002411 adverse Effects 0.000 description 1
150000007933 aliphatic carboxylic acids Chemical class 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
239000000470 constituent Substances 0.000 description 1
ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 1
229910000366 copper(II) sulfate Inorganic materials 0.000 description 1
LSRPARCOXAUYNP-UHFFFAOYSA-N cyclohexylidene(oxido)oxidanium Chemical compound [O-][O+]=C1CCCCC1 LSRPARCOXAUYNP-UHFFFAOYSA-N 0.000 description 1
230000001419 dependent effect Effects 0.000 description 1
POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 1
238000011067 equilibration Methods 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 1
239000012535 impurity Substances 0.000 description 1
239000001282 iso-butane Substances 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
239000000479 mixture part Substances 0.000 description 1
229910001453 nickel ion Inorganic materials 0.000 description 1
230000020477 pH reduction Effects 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
239000000047 product Substances 0.000 description 1
238000004064 recycling Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1
229910021653 sulphate ion Inorganic materials 0.000 description 1
229950011008 tetrachloroethylene Drugs 0.000 description 1
TUNFSRHWOTWDNC-UHFFFAOYSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 description 1
230000001988 toxicity Effects 0.000 description 1
231100000419 toxicity Toxicity 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0446—Juxtaposition of mixers-settlers
- B01D11/0457—Juxtaposition of mixers-settlers comprising rotating mechanisms, e.g. mixers, mixing pumps
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/26—Treatment of water, waste water, or sewage by extraction
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/30—Oximes
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/32—Carboxylic acids
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/40—Mixtures
- C22B3/402—Mixtures of acyclic or carbocyclic compounds of different types
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/40—Mixtures
- C22B3/402—Mixtures of acyclic or carbocyclic compounds of different types
- C22B3/404—Mixtures of acyclic or carbocyclic compounds of different types of organic acids and oximes
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling

Landscapes

Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Environmental & Geological Engineering (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Materials Engineering (AREA)
Manufacturing & Machinery (AREA)
Geology (AREA)
Geochemistry & Mineralogy (AREA)
Mechanical Engineering (AREA)
Metallurgy (AREA)
General Life Sciences & Earth Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Hydrology & Water Resources (AREA)
Water Supply & Treatment (AREA)
Extraction Or Liquid Replacement (AREA)
Manufacture And Refinement Of Metals (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

SE7802594A 1977-03-09 1978-03-07 Forfarande for selektiv extrahering av metalljoner ur en vattenlosning SE434123B (sv)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
NLAANVRAGE7702517,A NL169958C (nl)	1977-03-09	1977-03-09	Werkwijze voor het selectief extraheren van metaalionen uit waterige oplossingen daarvan.

Publications (2)

Publication Number	Publication Date
SE7802594L SE7802594L (sv)	1978-09-10
SE434123B true SE434123B (sv)	1984-07-09

Family

ID=19828135

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
SE7802594A SE434123B (sv)	1977-03-09	1978-03-07	Forfarande for selektiv extrahering av metalljoner ur en vattenlosning

Country Status (12)

Country	Link
JP (1)	JPS53110971A (it)
AU (1)	AU513707B2 (it)
BE (1)	BE864341A (it)
CA (1)	CA1107975A (it)
DE (1)	DE2810281A1 (it)
FR (1)	FR2383126A1 (it)
GB (1)	GB1571172A (it)
IT (1)	IT1101836B (it)
NL (1)	NL169958C (it)
SE (1)	SE434123B (it)
ZA (1)	ZA781144B (it)
ZM (1)	ZM2878A1 (it)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP0045735A3 (de) *	1980-07-31	1982-06-30	Andritz Ruthner Industrieanlagen Aktiengesellschaft	Flüssig-Flüssig-Extraktion von wässerigen ionenhältigen Flüssigkeiten
ZW9882A1 (en) *	1981-11-03	1983-02-02	Mineral Tech Council	Selective solvent extraction using organophosphorus and carboxylic acids
FR2591505B1 (fr) *	1985-12-18	1988-02-26	Atochem	Procede d'extraction de composes organiques de leurs solutions ou suspensions aqueuses.
JPH0781173B2 (ja) *	1987-06-18	1995-08-30	旭化成工業株式会社	金属ルテニウムの回収方法
DE3841673A1 (de) *	1988-12-10	1990-06-13	Hoechst Ag	Verfahren zur abtrennung von kupfer aus basisch reagierenden, waessrigen loesungen
KR102820068B1 (ko) *	2018-09-27	2025-06-12	이고 리미티드	고순도 수화 황산 니켈의 제조 방법

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2761563A (en) *	1951-11-16	1956-09-04	John C Van Dijk	Method of treating water
US2740708A (en) *	1955-03-14	1956-04-03	Sherritt Gordon Mines Ltd	Method of producing metal powder from solutions
BE635283A (it) *	1961-09-14	1900-01-01
DE1258101B (de) *	1964-04-29	1968-01-04	Ministerul Ind Petrolului	Trennungs- und Extrahierungsverfahren fuer Metalle aus waessrigen Loesungen mit Alkali-Naphthenaten, in apolaren organischen Loesungsmitteln aufgeloest
US3558288A (en) *	1965-04-15	1971-01-26	Ashland Oil Inc	Extraction of metal ions from acidic aqueous solution using an amine and a carboxylic acid
US3655347A (en) *	1968-03-18	1972-04-11	Gen Mills Inc	Process of extracting copper with certain substituted 2-hydroxybenzophenoximes
GB1267586A (en) *	1969-06-30	1972-03-22	Shell Int Research	Process for the separation of metals
GB1451490A (en) *	1970-05-21	1976-10-06	Shell Int Research	Use of hydroxy-oximes in the extraction of metal values
FI54329C (fi) *	1972-07-03	1978-11-10	Outokumpu Oy	Extraktionsmedelskomposition
GB1474944A (en) *	1974-05-30	1977-05-25	Thorsen G	Process for extraction and separation of metals using liquid cation exchangers
GB1537828A (en) *	1975-03-26	1979-01-04	Shell Int Research	Extraction of copper values from aqueous solutions with hydroxy-oximes
IE44327B1 (en) *	1976-01-30	1981-10-21	Ici Ltd	Extracting metal values with o-hydroxyaryloximes

1977
- 1977-03-09 NL NLAANVRAGE7702517,A patent/NL169958C/xx not_active IP Right Cessation
1978
- 1978-02-27 GB GB7706/78A patent/GB1571172A/en not_active Expired
- 1978-02-27 BE BE185500A patent/BE864341A/xx not_active IP Right Cessation
- 1978-02-27 ZA ZA00781144A patent/ZA781144B/xx unknown
- 1978-03-01 AU AU33720/78A patent/AU513707B2/en not_active Expired
- 1978-03-06 ZM ZM7828A patent/ZM2878A1/xx unknown
- 1978-03-06 IT IT48311/78A patent/IT1101836B/it active
- 1978-03-07 JP JP2591778A patent/JPS53110971A/ja active Pending
- 1978-03-07 SE SE7802594A patent/SE434123B/sv unknown
- 1978-03-07 FR FR7806438A patent/FR2383126A1/fr not_active Withdrawn
- 1978-03-08 CA CA298,537A patent/CA1107975A/en not_active Expired
- 1978-03-09 DE DE19782810281 patent/DE2810281A1/de not_active Ceased

Also Published As

Publication number	Publication date
IT1101836B (it)	1985-10-07
NL169958B (nl)	1982-04-16
FR2383126A1 (fr)	1978-10-06
IT7848311A0 (it)	1978-03-06
ZM2878A1 (en)	1978-12-21
AU513707B2 (en)	1980-12-18
CA1107975A (en)	1981-09-01
ZA781144B (en)	1979-02-28
GB1571172A (en)	1980-07-09
DE2810281A1 (de)	1978-09-14
JPS53110971A (en)	1978-09-28
NL7702517A (nl)	1978-09-12
BE864341A (nl)	1978-08-28
AU3372078A (en)	1979-09-06
NL169958C (nl)	1982-09-16
SE7802594L (sv)	1978-09-10

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DE2612505A1 (de)	1976-10-14	Verfahren zum abtrennen von kupfer aus sauren waessrigen loesungen
DE69204360T2 (de)	1996-04-18	Verfahren zur Reinigung und Rückgewinnung von Orthophosphorsäure mittels Flüssig-Flüssig-Extraktion.
DE2744187A1 (de)	1978-04-06	Verfahren zur rueckgewinnung eines katalysators
US3294842A (en)	1966-12-27	Alpha-hydroxy oximes containing alkenyl radicals
Kumbasar et al.	2006	Selective separation of gallium from acidic leach solutions by emulsion liquid membranes
DE69006334T2 (de)	1994-05-19	Verfahren zur Gewinnung von Gallium aus basischen Lösungen.
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