SE511722C2 - Förfarande vid ingjutning av oorganiska substanser i amorfa provkroppar för analys samt användning av provkropparna vid analys - Google Patents
Förfarande vid ingjutning av oorganiska substanser i amorfa provkroppar för analys samt användning av provkropparna vid analysInfo
- Publication number
- SE511722C2 SE511722C2 SE9202405A SE9202405A SE511722C2 SE 511722 C2 SE511722 C2 SE 511722C2 SE 9202405 A SE9202405 A SE 9202405A SE 9202405 A SE9202405 A SE 9202405A SE 511722 C2 SE511722 C2 SE 511722C2
- Authority
- SE
- Sweden
- Prior art keywords
- process according
- sample
- analysis
- amount
- oxygen
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 22
- 238000004458 analytical method Methods 0.000 title claims abstract description 8
- 239000000126 substance Substances 0.000 title description 3
- 238000002347 injection Methods 0.000 title 1
- 239000007924 injection Substances 0.000 title 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 21
- 239000001301 oxygen Substances 0.000 claims abstract description 21
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 15
- 230000003647 oxidation Effects 0.000 claims abstract description 14
- 238000002844 melting Methods 0.000 claims abstract description 9
- 230000008018 melting Effects 0.000 claims abstract description 9
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 8
- 230000004907 flux Effects 0.000 claims abstract description 8
- 238000004519 manufacturing process Methods 0.000 claims abstract description 6
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims abstract 7
- 238000004442 gravimetric analysis Methods 0.000 claims abstract 3
- 239000005447 environmental material Substances 0.000 claims abstract 2
- 239000000463 material Substances 0.000 claims abstract 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 9
- 230000001590 oxidative effect Effects 0.000 claims description 7
- 239000007800 oxidant agent Substances 0.000 claims description 6
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 229910001854 alkali hydroxide Inorganic materials 0.000 claims description 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims 2
- 229910005793 GeO 2 Inorganic materials 0.000 claims 1
- 229910013553 LiNO Inorganic materials 0.000 claims 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims 1
- 238000007496 glass forming Methods 0.000 claims 1
- 150000007529 inorganic bases Chemical class 0.000 claims 1
- 239000000395 magnesium oxide Substances 0.000 claims 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims 1
- 229910052697 platinum Inorganic materials 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- RIUWBIIVUYSTCN-UHFFFAOYSA-N trilithium borate Chemical class [Li+].[Li+].[Li+].[O-]B([O-])[O-] RIUWBIIVUYSTCN-UHFFFAOYSA-N 0.000 claims 1
- 238000005303 weighing Methods 0.000 claims 1
- YBMRDBCBODYGJE-UHFFFAOYSA-N germanium dioxide Chemical compound O=[Ge]=O YBMRDBCBODYGJE-UHFFFAOYSA-N 0.000 abstract description 6
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 abstract 2
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- 239000011521 glass Substances 0.000 description 8
- IIPYXGDZVMZOAP-UHFFFAOYSA-N lithium nitrate Chemical compound [Li+].[O-][N+]([O-])=O IIPYXGDZVMZOAP-UHFFFAOYSA-N 0.000 description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 229910052717 sulfur Inorganic materials 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 229940119177 germanium dioxide Drugs 0.000 description 2
- 229910044991 metal oxide Inorganic materials 0.000 description 2
- 150000004706 metal oxides Chemical class 0.000 description 2
- 150000003568 thioethers Chemical class 0.000 description 2
- 239000003039 volatile agent Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- -1 compound lithium sulfate Chemical class 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- INHCSSUBVCNVSK-UHFFFAOYSA-L lithium sulfate Inorganic materials [Li+].[Li+].[O-]S([O-])(=O)=O INHCSSUBVCNVSK-UHFFFAOYSA-L 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052752 metalloid Inorganic materials 0.000 description 1
- 150000002738 metalloids Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/38—Concrete; Lime; Mortar; Gypsum; Bricks; Ceramics; Glass
- G01N33/386—Glass
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/44—Sample treatment involving radiation, e.g. heat
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N5/00—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- General Physics & Mathematics (AREA)
- Pathology (AREA)
- Immunology (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Ceramic Engineering (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Glass Compositions (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE9202405A SE511722C2 (sv) | 1992-07-16 | 1992-07-16 | Förfarande vid ingjutning av oorganiska substanser i amorfa provkroppar för analys samt användning av provkropparna vid analys |
| ES93916368T ES2116460T3 (es) | 1992-07-16 | 1993-07-15 | Proceso de infusion de sustancias inorganicas en cuerpos amorfos para el analisis del contenido en oxigeno de las muestras perfundidas. |
| DE69317544T DE69317544T2 (de) | 1992-07-16 | 1993-07-15 | Einschmelzen von anorganischen substanzen in amorphe körper zur analyse ihres sauerstoffgehalts |
| AU45947/93A AU4594793A (en) | 1992-07-16 | 1993-07-15 | Infusing process of inorganic substances into amorphous bodies for analysis of the oxygen content of the infused samples |
| PCT/SE1993/000630 WO1994002827A1 (en) | 1992-07-16 | 1993-07-15 | Infusing process of inorganic substances into amorphous bodies for analysis of the oxygen content of the infused samples |
| AT93916368T ATE164226T1 (de) | 1992-07-16 | 1993-07-15 | Einschmelzen von anorganischen substanzen in amorphe körper zur analyse ihres sauerstoffgehalts |
| EP93916368A EP0612404B1 (de) | 1992-07-16 | 1993-07-15 | Einschmelzen von anorganischen substanzen in amorphe körper zur analyse ihres sauerstoffgehalts |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE9202405A SE511722C2 (sv) | 1992-07-16 | 1992-07-16 | Förfarande vid ingjutning av oorganiska substanser i amorfa provkroppar för analys samt användning av provkropparna vid analys |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| SE9202405D0 SE9202405D0 (sv) | 1992-07-16 |
| SE9202405L SE9202405L (sv) | 1994-01-17 |
| SE511722C2 true SE511722C2 (sv) | 1999-11-15 |
Family
ID=20386976
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SE9202405A SE511722C2 (sv) | 1992-07-16 | 1992-07-16 | Förfarande vid ingjutning av oorganiska substanser i amorfa provkroppar för analys samt användning av provkropparna vid analys |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP0612404B1 (de) |
| AT (1) | ATE164226T1 (de) |
| AU (1) | AU4594793A (de) |
| DE (1) | DE69317544T2 (de) |
| ES (1) | ES2116460T3 (de) |
| SE (1) | SE511722C2 (de) |
| WO (1) | WO1994002827A1 (de) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2849650B1 (fr) * | 2003-01-06 | 2006-12-08 | Gerard Lang | Verre de borate utilise comme fondant pour la realisation de perles destinees a l'analyse par fluorescence x, et procede de preparation du dit verre |
| JP7076835B2 (ja) * | 2020-09-11 | 2022-05-30 | 株式会社リガク | 蛍光x線分析装置用のガラスビードを作製する方法 |
| CN116359265B (zh) * | 2023-02-14 | 2026-04-21 | 包钢集团矿山研究院(有限责任公司) | 一种白云鄂博含铌矿物中铌含量的快速测定方法 |
-
1992
- 1992-07-16 SE SE9202405A patent/SE511722C2/sv not_active IP Right Cessation
-
1993
- 1993-07-15 AU AU45947/93A patent/AU4594793A/en not_active Abandoned
- 1993-07-15 EP EP93916368A patent/EP0612404B1/de not_active Expired - Lifetime
- 1993-07-15 DE DE69317544T patent/DE69317544T2/de not_active Expired - Fee Related
- 1993-07-15 AT AT93916368T patent/ATE164226T1/de not_active IP Right Cessation
- 1993-07-15 WO PCT/SE1993/000630 patent/WO1994002827A1/en not_active Ceased
- 1993-07-15 ES ES93916368T patent/ES2116460T3/es not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| SE9202405D0 (sv) | 1992-07-16 |
| AU4594793A (en) | 1994-02-14 |
| EP0612404B1 (de) | 1998-03-18 |
| DE69317544T2 (de) | 1998-08-06 |
| DE69317544D1 (de) | 1998-04-23 |
| SE9202405L (sv) | 1994-01-17 |
| ATE164226T1 (de) | 1998-04-15 |
| ES2116460T3 (es) | 1998-07-16 |
| WO1994002827A1 (en) | 1994-02-03 |
| EP0612404A1 (de) | 1994-08-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| NUG | Patent has lapsed |