SE520970C2 - Förfarande vid utvinning av trimethylolpropantriallyleter eller -diallyleter - Google Patents

Förfarande vid utvinning av trimethylolpropantriallyleter eller -diallyleter

Info

Publication number: SE520970C2
Authority: SE; Sweden
Prior art keywords: trimethylolpropane; process according; mixture; ethers; ether
Prior art date: 1998-09-30

Application number

SE9803315A

Other languages

English (en)

Swedish (sv)

Other versions

SE9803315L (sv

SE9803315D0 (sv

Inventor

Nils Moellby

Aake Rasmuson

Oleg Pajalic

Original Assignee

Perstorp Ab

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1998-09-30

Filing date

1998-09-30

Publication date

2003-09-16

1998-09-30 Application filed by Perstorp Ab filed Critical Perstorp Ab

1998-09-30 Priority to SE9803315A priority Critical patent/SE520970C2/sv

1998-09-30 Publication of SE9803315D0 publication Critical patent/SE9803315D0/xx

1999-09-28 Priority to PCT/SE1999/001711 priority patent/WO2000018713A1/en

1999-09-28 Priority to AT99954565T priority patent/ATE245618T1/de

1999-09-28 Priority to AU10883/00A priority patent/AU1088300A/en

1999-09-28 Priority to JP2000572176A priority patent/JP3782304B2/ja

1999-09-28 Priority to DE69909809T priority patent/DE69909809T2/de

1999-09-28 Priority to EP99954565A priority patent/EP1119537B1/de

2000-03-31 Publication of SE9803315L publication Critical patent/SE9803315L/xx

2003-09-16 Publication of SE520970C2 publication Critical patent/SE520970C2/sv

Links

ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 title claims abstract description 31
238000000034 method Methods 0.000 title claims abstract description 21
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 title claims abstract description 18
ATVJXMYDOSMEPO-UHFFFAOYSA-N 3-prop-2-enoxyprop-1-ene Chemical compound C=CCOCC=C ATVJXMYDOSMEPO-UHFFFAOYSA-N 0.000 title abstract description 3
238000011084 recovery Methods 0.000 title abstract description 3
239000000203 mixture Substances 0.000 claims abstract description 29
238000004821 distillation Methods 0.000 claims abstract description 28
JQRRFDWXQOQICD-UHFFFAOYSA-N biphenylen-1-ylboronic acid Chemical compound C12=CC=CC=C2C2=C1C=CC=C2B(O)O JQRRFDWXQOQICD-UHFFFAOYSA-N 0.000 claims abstract description 5
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 3
150000002170 ethers Chemical class 0.000 claims description 19
-1 trimethylolpropane diallyl ethers Chemical class 0.000 claims description 18
DCAYPVUWAIABOU-UHFFFAOYSA-N hexadecane Chemical compound CCCCCCCCCCCCCCCC DCAYPVUWAIABOU-UHFFFAOYSA-N 0.000 claims description 8
239000006227 byproduct Substances 0.000 claims description 5
NDJKXXJCMXVBJW-UHFFFAOYSA-N heptadecane Chemical compound CCCCCCCCCCCCCCCCC NDJKXXJCMXVBJW-UHFFFAOYSA-N 0.000 claims description 4
RZJRJXONCZWCBN-UHFFFAOYSA-N octadecane Chemical compound CCCCCCCCCCCCCCCCCC RZJRJXONCZWCBN-UHFFFAOYSA-N 0.000 claims description 4
239000000126 substance Substances 0.000 claims description 3
KAOCEWTZJVIHHP-UHFFFAOYSA-N 4-hydroxy-2,2-bis(hydroxymethyl)-3-oxobutanal Chemical compound OCC(=O)C(CO)(CO)C=O KAOCEWTZJVIHHP-UHFFFAOYSA-N 0.000 claims description 2
238000000998 batch distillation Methods 0.000 claims description 2
125000004432 carbon atom Chemical group C* 0.000 claims description 2
238000001944 continuous distillation Methods 0.000 claims description 2
229940038384 octadecane Drugs 0.000 claims description 2
239000003795 chemical substances by application Substances 0.000 abstract 2
150000001338 aliphatic hydrocarbons Chemical class 0.000 abstract 1
150000001875 compounds Chemical class 0.000 description 7
238000000605 extraction Methods 0.000 description 6
150000001298 alcohols Chemical class 0.000 description 5
238000009835 boiling Methods 0.000 description 5
238000010992 reflux Methods 0.000 description 5
239000000539 dimer Substances 0.000 description 4
229920000642 polymer Polymers 0.000 description 4
239000013638 trimer Substances 0.000 description 4
238000001704 evaporation Methods 0.000 description 3
230000008020 evaporation Effects 0.000 description 3
239000005977 Ethylene Substances 0.000 description 2
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical class OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical class CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 2
GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 2
230000001476 alcoholic effect Effects 0.000 description 2
238000005937 allylation reaction Methods 0.000 description 2
229920000166 polytrimethylene carbonate Polymers 0.000 description 2
239000000047 product Substances 0.000 description 2
235000013772 propylene glycol Nutrition 0.000 description 2
238000000746 purification Methods 0.000 description 2
238000000926 separation method Methods 0.000 description 2
QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 2
PTBDIHRZYDMNKB-UHFFFAOYSA-N 2,2-Bis(hydroxymethyl)propionic acid Chemical compound OCC(C)(CO)C(O)=O PTBDIHRZYDMNKB-UHFFFAOYSA-N 0.000 description 1
FLTJDUOFAQWHDF-UHFFFAOYSA-N 2,2-dimethylhexane Chemical compound CCCCC(C)(C)C FLTJDUOFAQWHDF-UHFFFAOYSA-N 0.000 description 1
SZSSMFVYZRQGIM-UHFFFAOYSA-N 2-(hydroxymethyl)-2-propylpropane-1,3-diol Chemical compound CCCC(CO)(CO)CO SZSSMFVYZRQGIM-UHFFFAOYSA-N 0.000 description 1
XATIZWAWQAIMQJ-UHFFFAOYSA-N 3,3-diethylheptane Chemical compound CCCCC(CC)(CC)CC XATIZWAWQAIMQJ-UHFFFAOYSA-N 0.000 description 1
SLINHMUFWFWBMU-UHFFFAOYSA-N Triisopropanolamine Chemical compound CC(O)CN(CC(C)O)CC(C)O SLINHMUFWFWBMU-UHFFFAOYSA-N 0.000 description 1
150000001335 aliphatic alkanes Chemical class 0.000 description 1
150000001735 carboxylic acids Chemical class 0.000 description 1
LVTYICIALWPMFW-UHFFFAOYSA-N diisopropanolamine Chemical compound CC(O)CNCC(C)O LVTYICIALWPMFW-UHFFFAOYSA-N 0.000 description 1
150000002009 diols Chemical class 0.000 description 1
238000005194 fractionation Methods 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 1
238000005457 optimization Methods 0.000 description 1
238000012856 packing Methods 0.000 description 1
235000020030 perry Nutrition 0.000 description 1
229920005862 polyol Polymers 0.000 description 1
150000003077 polyols Chemical class 0.000 description 1
YPFDHNVEDLHUCE-UHFFFAOYSA-N propane-1,3-diol Chemical class OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 1
HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical class O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 description 1
125000003258 trimethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])[*:1] 0.000 description 1
150000004072 triols Chemical class 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
- C07C41/01—Preparation of ethers
- C07C41/34—Separation; Purification; Stabilisation; Use of additives
- C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
- C07C41/42—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation by distillation

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Crystallography & Structural Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

SE9803315A 1998-09-30 1998-09-30 Förfarande vid utvinning av trimethylolpropantriallyleter eller -diallyleter SE520970C2 (sv)

Priority Applications (7)

Application Number	Priority Date	Filing Date	Title
SE9803315A SE520970C2 (sv)	1998-09-30	1998-09-30	Förfarande vid utvinning av trimethylolpropantriallyleter eller -diallyleter
PCT/SE1999/001711 WO2000018713A1 (en)	1998-09-30	1999-09-28	Method in recovery of trimethylolpropane triallyl or diallyl ether
AT99954565T ATE245618T1 (de)	1998-09-30	1999-09-28	Verfahren zur rückgewinnung von trimethylolpropan-triallyl- oder -diallyl-ether
AU10883/00A AU1088300A (en)	1998-09-30	1999-09-28	Method in recovery of trimethylolpropane triallyl or diallyl ether
JP2000572176A JP3782304B2 (ja)	1998-09-30	1999-09-28	トリメチロールプロパントリアリルエーテルまたはトリメチロールプロパンジアリルエーテルの回収方法
DE69909809T DE69909809T2 (de)	1998-09-30	1999-09-28	Verfahren zur rückgewinnung von trimethylolpropan-triallyl- oder -diallyl-ether
EP99954565A EP1119537B1 (de)	1998-09-30	1999-09-28	Verfahren zur rückgewinnung von trimethylolpropan-triallyl- oder -diallyl-ether

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
SE9803315A SE520970C2 (sv)	1998-09-30	1998-09-30	Förfarande vid utvinning av trimethylolpropantriallyleter eller -diallyleter

Publications (3)

Publication Number	Publication Date
SE9803315D0 SE9803315D0 (sv)	1998-09-30
SE9803315L SE9803315L (sv)	2000-03-31
SE520970C2 true SE520970C2 (sv)	2003-09-16

Family

ID=20412771

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
SE9803315A SE520970C2 (sv)	1998-09-30	1998-09-30	Förfarande vid utvinning av trimethylolpropantriallyleter eller -diallyleter

Country Status (7)

Country	Link
EP (1)	EP1119537B1 (de)
JP (1)	JP3782304B2 (de)
AT (1)	ATE245618T1 (de)
AU (1)	AU1088300A (de)
DE (1)	DE69909809T2 (de)
SE (1)	SE520970C2 (de)
WO (1)	WO2000018713A1 (de)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
EP2755259A1 (de)	2013-01-10	2014-07-16	Belenos Clean Power Holding AG	Selbst zusammengestellter Verbundstoff aus Grafenoxid und H4V3O8
JP6210515B2 (ja) *	2014-06-16	2017-10-11	株式会社オメガ	有機物質含浸食塩の処理方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2437789C3 (de) *	1974-08-06	1980-03-20	Bayer Ag, 5090 Leverkusen	Verfahren zur kontinuierlichen Herstellung von Trimethylolalkanallyläthern

1998
- 1998-09-30 SE SE9803315A patent/SE520970C2/sv not_active IP Right Cessation
1999
- 1999-09-28 EP EP99954565A patent/EP1119537B1/de not_active Expired - Lifetime
- 1999-09-28 DE DE69909809T patent/DE69909809T2/de not_active Expired - Fee Related
- 1999-09-28 WO PCT/SE1999/001711 patent/WO2000018713A1/en not_active Ceased
- 1999-09-28 JP JP2000572176A patent/JP3782304B2/ja not_active Expired - Fee Related
- 1999-09-28 AU AU10883/00A patent/AU1088300A/en not_active Abandoned
- 1999-09-28 AT AT99954565T patent/ATE245618T1/de not_active IP Right Cessation

Also Published As

Publication number	Publication date
SE9803315L (sv)	2000-03-31
WO2000018713A1 (en)	2000-04-06
JP3782304B2 (ja)	2006-06-07
SE9803315D0 (sv)	1998-09-30
EP1119537B1 (de)	2003-07-23
AU1088300A (en)	2000-04-17
ATE245618T1 (de)	2003-08-15
DE69909809D1 (de)	2003-08-28
DE69909809T2 (de)	2004-06-17
EP1119537A1 (de)	2001-08-01
JP2002525343A (ja)	2002-08-13

Legal Events

Date	Code	Title	Description
2010-06-02	NUG	Patent has lapsed

Publication	Publication Date	Title
EP0453084B1 (de)	1995-06-07	Reinigung von niederem Alkylenoxid
US3578568A (en)	1971-05-11	Purification of low molecular weight epoxides by extractive distillation with a glycol or glycol ether
US2622060A (en)	1952-12-16	Purification of 1,2-propylene oxide
US9180384B2 (en)	2015-11-10	Apparatus and process for using olefin as an azeotropic entrainer for isolating 1,3-DICHLORO-2-propanol from a 2,2′-oxybis (1-chloropropane) waste stream
EP0535949A1 (de)	1993-04-07	Reinigung von Propylenoxid durch Extraktivdestillation
JP2001514258A (ja)	2001-09-11	反応混合物からのメタノールとプロピレンオキシドの分離
US2552412A (en)	1951-05-08	Purification of aliphatic alcohols by extractive distillation
US2575243A (en)	1951-11-13	Extractive distillation of alcohols
US4402794A (en)	1983-09-06	Purification of butylene oxides by extractive distillation with selected extractive distillation solvents
US5262017A (en)	1993-11-16	Plural stage purification of propylene oxide
EP1003701B1 (de)	2002-11-27	Reinigung von einem methanolstrom
EP0457421B1 (de)	1995-06-28	Reiningung von niederen Alkylenoxiden
US2305106A (en)	1942-12-15	Manufacture of acetonitrile
KR890003657A (ko)	1989-04-17	조 sec-부틸 알코올의 정제 증류방법
EP0645381B1 (de)	1997-11-12	Mehrstufiges Verfahren zum Trocknen und Reinigen von Propylenoxid
SE520970C2 (sv)	2003-09-16	Förfarande vid utvinning av trimethylolpropantriallyleter eller -diallyleter
US5154804A (en)	1992-10-13	Removal of water, acetone and methanol from propylene oxide by extractive distillation
US2635992A (en)	1953-04-21	Separation and purification of alcohols by extractive distillation
US3303108A (en)	1967-02-07	Purification of alkanols having three to five carbon atomas by distillation of the alkanol from a crude mxiture in a single column in the presence of water
US5958192A (en)	1999-09-28	Purification of propylene oxide using ethylene glycol monomethyl ether as an extractive distillation agent
EP0685472B1 (de)	1997-09-03	Extraktivdestillation von Propylenoxid
US5772854A (en)	1998-06-30	Use of paired reboilers in the purification of propylene oxide by extractive distillation
US4401516A (en)	1983-08-30	Process for separating acetamidoethylene from crude preparation products
US2561680A (en)	1951-07-24	Purification of methanol by azeotropic distillation
US3655524A (en)	1972-04-11	Glycidol isolation by azeotropic distillation with a lower-boiling entrainer