SU157695A1 - - Google Patents

Info

Publication number

SU157695A1

SU157695A1 SU787867A SU787867A SU157695A1 SU 157695 A1 SU157695 A1 SU 157695A1 SU 787867 A SU787867 A SU 787867A SU 787867 A SU787867 A SU 787867A SU 157695 A1 SU157695 A1 SU 157695A1

Authority

SU

USSR - Soviet Union

Prior art keywords

chloromethyl

carboxylic acid

furan

water

methyl ester

Prior art date

Links

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• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
• 239000004342 Benzoyl peroxide Substances 0.000 description 3
• OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 description 3
• WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 3
• 235000019400 benzoyl peroxide Nutrition 0.000 description 3
• GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 3
• 229910052794 bromium Inorganic materials 0.000 description 3
• CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
• OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
• PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
• 229910052799 carbon Inorganic materials 0.000 description 2
• 238000001816 cooling Methods 0.000 description 2
• 238000000034 method Methods 0.000 description 2
• PNOSOFQVIWIJFF-UHFFFAOYSA-N methyl 5-(bromomethyl)-4-(chloromethyl)furan-2-carboxylate Chemical compound COC(=O)C1=CC(CCl)=C(CBr)O1 PNOSOFQVIWIJFF-UHFFFAOYSA-N 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• 239000000126 substance Substances 0.000 description 2
• VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
• GCIKIBLIUGZSNR-UHFFFAOYSA-N CC1=C(C(O)=O)OC(C)=C1CCl Chemical compound CC1=C(C(O)=O)OC(C)=C1CCl GCIKIBLIUGZSNR-UHFFFAOYSA-N 0.000 description 1
• UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
• KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
• 239000002253 acid Substances 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 239000003610 charcoal Substances 0.000 description 1
• 239000000460 chlorine Substances 0.000 description 1
• 229910052801 chlorine Inorganic materials 0.000 description 1
• 239000012043 crude product Substances 0.000 description 1
• 230000008034 disappearance Effects 0.000 description 1
• 238000001035 drying Methods 0.000 description 1
• 239000011521 glass Substances 0.000 description 1
• 239000001257 hydrogen Substances 0.000 description 1
• 229910052739 hydrogen Inorganic materials 0.000 description 1
• -1 methyl 4-chloromethyl-5-bromomethyl-furan-2-carboxylic acid Chemical compound 0.000 description 1
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
• 239000003960 organic solvent Substances 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 230000002265 prevention Effects 0.000 description 1
• 238000000746 purification Methods 0.000 description 1
• 229910052938 sodium sulfate Inorganic materials 0.000 description 1
• 235000011152 sodium sulphate Nutrition 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 230000001629 suppression Effects 0.000 description 1