SU421174A3 - Способ получения перекиси водорода - Google Patents
Способ получения перекиси водородаInfo
- Publication number
- SU421174A3 SU421174A3 SU1641013A SU1641013A SU421174A3 SU 421174 A3 SU421174 A3 SU 421174A3 SU 1641013 A SU1641013 A SU 1641013A SU 1641013 A SU1641013 A SU 1641013A SU 421174 A3 SU421174 A3 SU 421174A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- carbon atoms
- hydrogen peroxide
- quinone
- alkyl
- substituted
- Prior art date
Links
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title claims description 33
- 238000000034 method Methods 0.000 title claims description 14
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 claims description 28
- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 claims description 22
- 125000004432 carbon atom Chemical group C* 0.000 claims description 13
- 239000002904 solvent Substances 0.000 claims description 13
- 235000013877 carbamide Nutrition 0.000 claims description 11
- 150000003672 ureas Chemical class 0.000 claims description 11
- 229910052760 oxygen Inorganic materials 0.000 claims description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 7
- 239000007789 gas Substances 0.000 claims description 7
- 239000001301 oxygen Substances 0.000 claims description 7
- AVQQQNCBBIEMEU-UHFFFAOYSA-N 1,1,3,3-tetramethylurea Chemical compound CN(C)C(=O)N(C)C AVQQQNCBBIEMEU-UHFFFAOYSA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- QPUYECUOLPXSFR-UHFFFAOYSA-N 1-methylnaphthalene Chemical compound C1=CC=C2C(C)=CC=CC2=C1 QPUYECUOLPXSFR-UHFFFAOYSA-N 0.000 claims description 4
- 125000000217 alkyl group Chemical group 0.000 claims description 4
- 229930195733 hydrocarbon Natural products 0.000 claims description 4
- 150000002430 hydrocarbons Chemical class 0.000 claims description 4
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 229910052717 sulfur Inorganic materials 0.000 claims description 3
- 150000004996 alkyl benzenes Chemical class 0.000 claims description 2
- 125000003118 aryl group Chemical group 0.000 claims description 2
- 238000009903 catalytic hydrogenation reaction Methods 0.000 claims description 2
- 125000005842 heteroatom Chemical group 0.000 claims description 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 claims 1
- 125000000753 cycloalkyl group Chemical group 0.000 claims 1
- 229910052740 iodine Inorganic materials 0.000 claims 1
- 239000011630 iodine Substances 0.000 claims 1
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 229910052757 nitrogen Inorganic materials 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 229910052739 hydrogen Inorganic materials 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 239000001257 hydrogen Substances 0.000 description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 5
- 239000012224 working solution Substances 0.000 description 5
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 4
- -1 alkyl radicals Chemical class 0.000 description 4
- 239000004202 carbamide Substances 0.000 description 4
- 238000004821 distillation Methods 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 description 3
- 150000004056 anthraquinones Chemical class 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 238000005984 hydrogenation reaction Methods 0.000 description 3
- 230000001590 oxidative effect Effects 0.000 description 3
- 229910052700 potassium Inorganic materials 0.000 description 3
- FYGHSUNMUKGBRK-UHFFFAOYSA-N 1,2,3-trimethylbenzene Chemical compound CC1=CC=CC(C)=C1C FYGHSUNMUKGBRK-UHFFFAOYSA-N 0.000 description 2
- SJEBAWHUJDUKQK-UHFFFAOYSA-N 2-ethylanthraquinone Chemical compound C1=CC=C2C(=O)C3=CC(CC)=CC=C3C(=O)C2=C1 SJEBAWHUJDUKQK-UHFFFAOYSA-N 0.000 description 2
- 229910052763 palladium Inorganic materials 0.000 description 2
- 150000003254 radicals Chemical class 0.000 description 2
- 239000011877 solvent mixture Substances 0.000 description 2
- YEVQZPWSVWZAOB-UHFFFAOYSA-N 2-(bromomethyl)-1-iodo-4-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=CC=C(I)C(CBr)=C1 YEVQZPWSVWZAOB-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 229910021398 atomic carbon Inorganic materials 0.000 description 1
- 150000001555 benzenes Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- CBPYOHALYYGNOE-UHFFFAOYSA-M potassium;3,5-dinitrobenzoate Chemical compound [K+].[O-]C(=O)C1=CC([N+]([O-])=O)=CC([N+]([O-])=O)=C1 CBPYOHALYYGNOE-UHFFFAOYSA-M 0.000 description 1
- 229940090181 propyl acetate Drugs 0.000 description 1
- WMOVHXAZOJBABW-UHFFFAOYSA-N tert-butyl acetate Chemical compound CC(=O)OC(C)(C)C WMOVHXAZOJBABW-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/022—Preparation from organic compounds
- C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2018686A DE2018686C3 (de) | 1970-04-18 | 1970-04-18 | Verfahren zur Herstellung von Was serstoffperoxid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU421174A3 true SU421174A3 (ru) | 1974-03-25 |
Family
ID=5768445
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1641013A SU421174A3 (ru) | 1970-04-18 | 1971-04-02 | Способ получения перекиси водорода |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3767778A (fr) |
| JP (1) | JPS5023678B1 (fr) |
| AT (1) | AT327861B (fr) |
| BE (1) | BE765912A (fr) |
| CA (1) | CA954671A (fr) |
| FR (1) | FR2086166B1 (fr) |
| GB (2) | GB1354031A (fr) |
| NL (1) | NL170124C (fr) |
| SE (2) | SE388415B (fr) |
| SU (1) | SU421174A3 (fr) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2687449C1 (ru) * | 2018-05-07 | 2019-05-13 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Иркутский государственный университет" (ФГБОУ ВО "ИГУ") | Способ получения перекиси водорода |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3027253C2 (de) * | 1980-07-18 | 1982-11-04 | Degussa Ag, 6000 Frankfurt | Verfahren zur Herstellung von Wasserstoffperoxid |
| US4566998A (en) * | 1981-09-28 | 1986-01-28 | Foret S.A. | Production of hydrogen peroxide |
| US4394369A (en) * | 1982-05-24 | 1983-07-19 | Fmc Corporation | Hydrogen peroxide process |
| US4564514A (en) * | 1982-07-07 | 1986-01-14 | Degussa Aktiengesellschaft | Process for the production of water-free organic hydrogen peroxide solution |
| SE459919C (sv) * | 1987-03-27 | 1991-03-25 | Eka Nobel Ab | Foerfarande foer framstaellning av vaeteperoxid genom reduktion och oxidation av en antrakinon |
| US5674450A (en) * | 1994-04-28 | 1997-10-07 | Johnson & Johnson Medical, Inc. | Vapor sterilization using a non-aqueous source of hydrogen peroxide |
| US6180804B1 (en) | 1998-09-10 | 2001-01-30 | Fmc Corporation | Reversion of expoxide in the production of Hydrogen peroxide |
| EP3543208A1 (fr) | 2018-03-19 | 2019-09-25 | Solvay Sa | Procédé de fabrication d'une solution aqueuse de peroxyde d'hydrogène |
| FR3131292B1 (fr) | 2021-12-23 | 2025-10-31 | Arkema France | Procédé de production de peroxyde d’hydrogène |
| FR3141158B1 (fr) | 2022-10-25 | 2024-10-04 | Arkema France | Procédé de production de peroxyde d’hydrogène |
-
1971
- 1971-03-03 NL NLAANVRAGE7102820,A patent/NL170124C/xx not_active IP Right Cessation
- 1971-03-30 FR FR7111193A patent/FR2086166B1/fr not_active Expired
- 1971-04-02 SU SU1641013A patent/SU421174A3/ru active
- 1971-04-12 US US00133390A patent/US3767778A/en not_active Expired - Lifetime
- 1971-04-16 SE SE7405765A patent/SE388415B/xx not_active IP Right Cessation
- 1971-04-16 CA CA110,561A patent/CA954671A/en not_active Expired
- 1971-04-16 AT AT324771A patent/AT327861B/de not_active IP Right Cessation
- 1971-04-16 SE SE7104983A patent/SE377794B/xx unknown
- 1971-04-16 BE BE765912A patent/BE765912A/fr not_active IP Right Cessation
- 1971-04-19 JP JP46025216A patent/JPS5023678B1/ja active Pending
- 1971-04-19 GB GB2689671*A patent/GB1354031A/en not_active Expired
- 1971-04-19 GB GB4078573A patent/GB1354032A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2687449C1 (ru) * | 2018-05-07 | 2019-05-13 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Иркутский государственный университет" (ФГБОУ ВО "ИГУ") | Способ получения перекиси водорода |
Also Published As
| Publication number | Publication date |
|---|---|
| US3767778A (en) | 1973-10-23 |
| SE377794B (fr) | 1975-07-28 |
| FR2086166B1 (fr) | 1974-03-08 |
| JPS5023678B1 (fr) | 1975-08-09 |
| BE765912A (fr) | 1971-09-16 |
| NL170124B (nl) | 1982-05-03 |
| ATA324771A (de) | 1975-05-15 |
| CA954671A (en) | 1974-09-17 |
| AT327861B (de) | 1976-02-25 |
| GB1354031A (en) | 1974-06-05 |
| GB1354032A (en) | 1974-06-05 |
| NL7102820A (fr) | 1971-10-20 |
| NL170124C (nl) | 1982-10-01 |
| FR2086166A1 (fr) | 1971-12-31 |
| SE388415B (sv) | 1976-10-04 |
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