SU586838A3 - Способ получени оксима циклогексанона - Google Patents
Способ получени оксима циклогексанонаInfo
- Publication number
- SU586838A3 SU586838A3 SU752126766A SU2126766A SU586838A3 SU 586838 A3 SU586838 A3 SU 586838A3 SU 752126766 A SU752126766 A SU 752126766A SU 2126766 A SU2126766 A SU 2126766A SU 586838 A3 SU586838 A3 SU 586838A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- liquid
- cyclohexanone oxime
- cyclohexanone
- nitrous gases
- pipeline
- Prior art date
Links
- VEZUQRBDRNJBJY-UHFFFAOYSA-N cyclohexanone oxime Chemical compound ON=C1CCCCC1 VEZUQRBDRNJBJY-UHFFFAOYSA-N 0.000 title description 24
- 238000000034 method Methods 0.000 title description 13
- 239000007789 gas Substances 0.000 description 23
- 239000007788 liquid Substances 0.000 description 23
- GQPLMRYTRLFLPF-UHFFFAOYSA-N nitrous oxide Inorganic materials [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 description 19
- 238000006243 chemical reaction Methods 0.000 description 18
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 14
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical class ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 description 10
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 10
- 239000003054 catalyst Substances 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 7
- 229910052799 carbon Inorganic materials 0.000 description 6
- -1 cyclohexane oxime Chemical class 0.000 description 6
- MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical compound O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- MGWGWNFMUOTEHG-UHFFFAOYSA-N 4-(3,5-dimethylphenyl)-1,3-thiazol-2-amine Chemical compound CC1=CC(C)=CC(C=2N=C(N)SC=2)=C1 MGWGWNFMUOTEHG-UHFFFAOYSA-N 0.000 description 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 4
- PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 description 4
- 229910017604 nitric acid Inorganic materials 0.000 description 4
- JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 4
- 229910052763 palladium Inorganic materials 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 229910002651 NO3 Inorganic materials 0.000 description 3
- 150000003863 ammonium salts Chemical class 0.000 description 3
- 239000000337 buffer salt Substances 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 150000002894 organic compounds Chemical class 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 150000001735 carboxylic acids Chemical class 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 239000012429 reaction media Substances 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000000872 buffer Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 150000002763 monocarboxylic acids Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 150000002923 oximes Chemical class 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
- 239000002918 waste heat Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7405630A NL7405630A (nl) | 1974-04-26 | 1974-04-26 | Kringloopproces voor de bereiding van cyclohexanonoxim. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU586838A3 true SU586838A3 (ru) | 1977-12-30 |
Family
ID=19821235
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU752126766A SU586838A3 (ru) | 1974-04-26 | 1975-04-24 | Способ получени оксима циклогексанона |
Country Status (15)
| Country | Link |
|---|---|
| JP (1) | JPS50154224A (it) |
| AR (1) | AR202611A1 (it) |
| BE (1) | BE828393A (it) |
| BR (1) | BR7502549A (it) |
| CH (1) | CH609335A5 (it) |
| CS (1) | CS199266B2 (it) |
| DE (1) | DE2518259A1 (it) |
| ES (1) | ES436961A1 (it) |
| FR (1) | FR2268794B1 (it) |
| GB (1) | GB1506437A (it) |
| IT (1) | IT1035465B (it) |
| NL (1) | NL7405630A (it) |
| PL (1) | PL94769B1 (it) |
| RO (1) | RO73094A (it) |
| SU (1) | SU586838A3 (it) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6844469B2 (en) | 2000-06-05 | 2005-01-18 | Dsm Ip Assets B.V. | Process for the production of cyclohexanone oxime |
| CN1200928C (zh) * | 2000-06-05 | 2005-05-11 | Dsmip财产有限公司 | 制备环己酮肟的方法 |
| AU2002347664A1 (en) * | 2001-12-04 | 2003-06-17 | Dsm Ip Assets B.V. | Process for treating an aqueous medium containing phosphate salt and organic compounds |
-
1974
- 1974-04-26 NL NL7405630A patent/NL7405630A/xx not_active Application Discontinuation
-
1975
- 1975-04-22 GB GB1666/75A patent/GB1506437A/en not_active Expired
- 1975-04-24 DE DE19752518259 patent/DE2518259A1/de active Pending
- 1975-04-24 CS CS752884A patent/CS199266B2/cs unknown
- 1975-04-24 SU SU752126766A patent/SU586838A3/ru active
- 1975-04-24 FR FR7512794A patent/FR2268794B1/fr not_active Expired
- 1975-04-24 JP JP50050167A patent/JPS50154224A/ja active Pending
- 1975-04-24 IT IT49299/75A patent/IT1035465B/it active
- 1975-04-25 BE BE155775A patent/BE828393A/xx unknown
- 1975-04-25 RO RO7582088A patent/RO73094A/ro unknown
- 1975-04-25 ES ES436961A patent/ES436961A1/es not_active Expired
- 1975-04-25 PL PL1975179927A patent/PL94769B1/pl unknown
- 1975-04-25 CH CH530775A patent/CH609335A5/xx not_active IP Right Cessation
- 1975-04-25 BR BR3233/75A patent/BR7502549A/pt unknown
- 1975-04-28 AR AR258525A patent/AR202611A1/es active
Also Published As
| Publication number | Publication date |
|---|---|
| ES436961A1 (es) | 1976-12-01 |
| BR7502549A (pt) | 1976-03-03 |
| FR2268794A1 (it) | 1975-11-21 |
| NL7405630A (nl) | 1975-10-28 |
| GB1506437A (en) | 1978-04-05 |
| JPS50154224A (it) | 1975-12-12 |
| BE828393A (nl) | 1975-10-27 |
| DE2518259A1 (de) | 1975-11-06 |
| CS199266B2 (en) | 1980-07-31 |
| IT1035465B (it) | 1979-10-20 |
| CH609335A5 (en) | 1979-02-28 |
| FR2268794B1 (it) | 1979-10-05 |
| RO73094A (ro) | 1982-02-26 |
| PL94769B1 (pl) | 1977-08-31 |
| AR202611A1 (es) | 1975-06-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Brown et al. | Purifying hydrogen by selective oxidation of carbon monoxide | |
| JPS6041056B2 (ja) | シクロヘキサンの酸化法 | |
| US4623668A (en) | Preparation of methanol | |
| US3997607A (en) | Recycling process for the preparation of cyclohexanone oxime | |
| US3914389A (en) | Lanthanum oxidation catalyst and method for utilizing the same | |
| US3451776A (en) | Halogen production | |
| US4032548A (en) | Process for preparing 1,4-naphthoquinone | |
| US4246250A (en) | Process for the preparation of a hydroxylamine salt | |
| US6322766B1 (en) | Preparation of oxides of nitrogen having a low degree of oxidation | |
| US4201872A (en) | Process for preparing purified terephthalic acid | |
| US20040116745A1 (en) | Process for the preparation of cyclohexanone oxime | |
| US4010198A (en) | Process for the preparation of allyl acetate | |
| EP1301468B1 (en) | Process for the production of cyclohexanone oxime | |
| US4045540A (en) | Process for the synthesis of ammonium nitrite | |
| US2291345A (en) | Hydrocarbon nitration | |
| US2772947A (en) | Process for converting nickel sulfide to nickel sulfate | |
| US4328198A (en) | Cyclic process for the preparation and processing of a hydroxylammonium salt solution | |
| US4122153A (en) | Recycling method for the preparation and processing of a hydroxyl ammonium salt solution | |
| GB215789A (en) | Improvements in the process of making ammonia by catalysis | |
| US1338417A (en) | Manufacture of concentrated nitric acid | |
| US3615192A (en) | Oxidation of hydrogen cyanide to cyanogen in a liquid medium utilizing a copper catalyst | |
| IE66031B1 (en) | Continous industrial manufacturing process for an aqueous solution of glyoxylic acid | |
| US6300507B2 (en) | Process of manufacturing ethylene oxide | |
| US3769388A (en) | Oxidation of hydrogen cyanide to cyanogen in a liquid medium containing a soluble nitrate salt or nitric acid | |
| SU751321A3 (ru) | Способ получени фталатов щелочных металлов |