TW197444B - Method of synthesizing N-phosphorous methyl carboxyglycine - Google Patents
Method of synthesizing N-phosphorous methyl carboxyglycineInfo
- Publication number
- TW197444B TW197444B TW81104365A TW81104365A TW197444B TW 197444 B TW197444 B TW 197444B TW 81104365 A TW81104365 A TW 81104365A TW 81104365 A TW81104365 A TW 81104365A TW 197444 B TW197444 B TW 197444B
- Authority
- TW
- Taiwan
- Prior art keywords
- carboxyglycine
- synthesizing
- alcohol
- iminodimethyl
- reacting
- Prior art date
Links
- YSVHIKSKCCPTGF-UHFFFAOYSA-N 2-[carboxy(methyl)amino]acetic acid Chemical compound OC(=O)N(C)CC(O)=O YSVHIKSKCCPTGF-UHFFFAOYSA-N 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 230000002194 synthesizing effect Effects 0.000 title abstract 2
- -1 iminodimethyl alcohol Chemical compound 0.000 abstract 2
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 abstract 1
- 229930040373 Paraformaldehyde Natural products 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 239000003518 caustics Substances 0.000 abstract 1
- FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical compound OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 1
- 239000011707 mineral Substances 0.000 abstract 1
- 229920002866 paraformaldehyde Polymers 0.000 abstract 1
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 abstract 1
- 239000000376 reactant Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
Abstract
A method of synthesizing N-phosphorous methyl carboxyglycine comprising: C1-C4 alkyl alcohol as solvent; NH3 and paraformaldehyde as reactants to produce iminodimethyl alcohol; trialkyl phosphite reacting with iminodimethyl alcohol below 50讈 in the presence of an alkaline compound; then reacting with mono-chloracetic acid; stirring the above reaction below 50讈, heating the product with mineral acid, treating the product with caustic alkali to obtain white crystal.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| TW81104365A TW197444B (en) | 1992-06-03 | 1992-06-03 | Method of synthesizing N-phosphorous methyl carboxyglycine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| TW81104365A TW197444B (en) | 1992-06-03 | 1992-06-03 | Method of synthesizing N-phosphorous methyl carboxyglycine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TW197444B true TW197444B (en) | 1993-01-01 |
Family
ID=51356397
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW81104365A TW197444B (en) | 1992-06-03 | 1992-06-03 | Method of synthesizing N-phosphorous methyl carboxyglycine |
Country Status (1)
| Country | Link |
|---|---|
| TW (1) | TW197444B (en) |
-
1992
- 1992-06-03 TW TW81104365A patent/TW197444B/en active
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