TW202112726A - 來自氧化酯化之反應器輸出物的簡化後處理 - Google Patents

來自氧化酯化之反應器輸出物的簡化後處理 Download PDF

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Publication number
TW202112726A
TW202112726A TW109128884A TW109128884A TW202112726A TW 202112726 A TW202112726 A TW 202112726A TW 109128884 A TW109128884 A TW 109128884A TW 109128884 A TW109128884 A TW 109128884A TW 202112726 A TW202112726 A TW 202112726A
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TW
Taiwan
Prior art keywords
phase
reactor
methacrolein
mma
mal
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TW109128884A
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English (en)
Chinese (zh)
Inventor
史蒂芬 瑞爾
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德商羅伊姆公司
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Application filed by 德商羅伊姆公司 filed Critical 德商羅伊姆公司
Publication of TW202112726A publication Critical patent/TW202112726A/zh

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/39—Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/44—Preparation of carboxylic acid esters by oxidation-reduction of aldehydes, e.g. Tishchenko reaction
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/58—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
TW109128884A 2019-08-28 2020-08-25 來自氧化酯化之反應器輸出物的簡化後處理 TW202112726A (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP19193981.8A EP3786148A1 (fr) 2019-08-28 2019-08-28 Retraitement simplifié de la décharge du réacteur d'une estérification oxydative
EP19193981.8 2019-08-28

Publications (1)

Publication Number Publication Date
TW202112726A true TW202112726A (zh) 2021-04-01

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ID=67777131

Family Applications (1)

Application Number Title Priority Date Filing Date
TW109128884A TW202112726A (zh) 2019-08-28 2020-08-25 來自氧化酯化之反應器輸出物的簡化後處理

Country Status (6)

Country Link
US (1) US12297170B2 (fr)
EP (2) EP3786148A1 (fr)
JP (1) JP2022546076A (fr)
CN (1) CN114401941B (fr)
TW (1) TW202112726A (fr)
WO (1) WO2021037660A1 (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115246773B (zh) * 2021-04-26 2024-05-10 上海浦景化工技术股份有限公司 一种从羟醛缩合产物中分离mma的系统
US20240400492A1 (en) * 2021-10-08 2024-12-05 Rohm And Haas Company Process for methyl methacrylate production
MX2024004169A (es) * 2021-10-08 2024-04-23 Rohm & Haas Proceso para la produccion de metacrilato de alquilo.
WO2023059673A1 (fr) * 2021-10-08 2023-04-13 Rohm And Haas Company Procédé pour un réacteur d'estérification oxydative
CN121729404A (zh) 2023-08-22 2026-03-24 罗姆化学有限责任公司 (甲基)丙烯酸酯生产的脱碳

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE312723C (fr) 1919-03-15
US2848499A (en) 1956-05-09 1958-08-19 Celanese Corp Preparation of unsaturated aldehydes
DE3106557A1 (de) 1981-02-21 1982-09-16 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von (alpha)-alkylacroleinen
DE3213681A1 (de) 1982-04-14 1983-10-27 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von (alpha)-alkylacroleinen
DE3508702A1 (de) 1985-03-12 1986-09-18 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von methacrylsaeure
DE3740293A1 (de) 1987-11-27 1989-06-01 Hoechst Ag Verfahren zur herstellung von alpha-alkylacroleinen
JP3069420B2 (ja) 1991-11-05 2000-07-24 ダイセル化学工業株式会社 反応器および反応方法
SG71815A1 (en) 1997-07-08 2000-04-18 Asahi Chemical Ind Method of producing methyl methacrylate
JP4076227B2 (ja) 2001-12-21 2008-04-16 旭化成ケミカルズ株式会社 酸化物触媒組成物
JP4173757B2 (ja) 2003-03-26 2008-10-29 ジヤトコ株式会社 ロックアップクラッチの寿命判定方法及びスリップロックアップ領域設定方法並びに寿命判定装置
US7141702B2 (en) 2004-03-26 2006-11-28 Council Of Scientific And Industrial Research Process for the synthesis of α-substituted acroleins
EP2986589B1 (fr) 2013-04-19 2018-03-14 Evonik Röhm GmbH Procédé destiné à la fabrication de méthylméthacrylate
EP2886528A1 (fr) 2013-12-20 2015-06-24 Evonik Industries AG Procédé de fabrication d'esters non saturés à partir d'aldéhydes par estérisation oxydative directe
EP2998284A1 (fr) 2014-09-18 2016-03-23 Evonik Röhm GmbH Procédé optimisé de fabrication de méthacroléine
EP3144291A1 (fr) 2015-09-16 2017-03-22 Evonik Röhm GmbH Synthese d'acide methacrylique a partir de methacrylate d'alkyle a base de methacroleine
TWI715627B (zh) 2015-09-16 2021-01-11 德商羅伊姆公司 含鈉鹽之mma-甲醇混合物的萃取後處理
KR102619749B1 (ko) 2017-05-09 2023-12-29 룀 게엠베하 알데히드의 카르복실산 에스테르로의 산화 에스테르화 방법
EP3450422A1 (fr) * 2017-08-29 2019-03-06 Evonik Röhm GmbH Procédé de fabrication des matières à mouler optiques
CN108440281B (zh) * 2018-03-16 2021-03-02 上海载正化工科技发展有限公司 化学反应装置及其应用
EP3587390A1 (fr) 2018-06-26 2020-01-01 Röhm GmbH Procédé de fabrication de mma en grandes quantités

Also Published As

Publication number Publication date
US20220363625A1 (en) 2022-11-17
WO2021037660A1 (fr) 2021-03-04
CN114401941A (zh) 2022-04-26
JP2022546076A (ja) 2022-11-02
CN114401941B (zh) 2024-10-29
US12297170B2 (en) 2025-05-13
EP3786148A1 (fr) 2021-03-03
EP4021882A1 (fr) 2022-07-06

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