TW506970B - Process for removal of ammonia from solutions including lactam and ammonia - Google Patents

Process for removal of ammonia from solutions including lactam and ammonia Download PDF

Info

Publication number: TW506970B
Authority: TW; Taiwan
Prior art keywords: item; ammonia; patent application; solvent; scope
Prior art date: 2000-06-05

Application number

TW090113615A

Other languages

English (en)

Chinese (zh)

Inventor

Hermann Luyken

Frank Ohlbach

Stefan Maixner

Rolf-Hartmuth Fischer

Johann-Peter Melder

Original Assignee

Basf Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2000-06-05

Filing date

2001-06-05

Publication date

2002-10-21

Family has litigation

First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=26005932&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=TW506970(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.

2000-06-05 Priority claimed from DE2000127328 external-priority patent/DE10027328A1/de

2000-07-11 Priority claimed from DE2000133516 external-priority patent/DE10033516A1/de

2001-06-05 Application filed by Basf Ag filed Critical Basf Ag

2002-10-21 Application granted granted Critical

2002-10-21 Publication of TW506970B publication Critical patent/TW506970B/zh

Links

QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims abstract description 88
229910021529 ammonia Inorganic materials 0.000 title claims abstract description 43
238000000034 method Methods 0.000 title claims abstract description 34
150000003951 lactams Chemical class 0.000 title claims abstract description 10
238000004821 distillation Methods 0.000 claims abstract description 33
239000002904 solvent Substances 0.000 claims description 24
JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical group O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 claims description 18
239000007788 liquid Substances 0.000 claims description 12
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
238000010992 reflux Methods 0.000 claims description 8
238000001704 evaporation Methods 0.000 claims description 6
230000008020 evaporation Effects 0.000 claims description 6
230000006835 compression Effects 0.000 claims description 5
238000007906 compression Methods 0.000 claims description 5
238000001179 sorption measurement Methods 0.000 claims description 4
239000006096 absorbing agent Substances 0.000 claims description 3
238000009835 boiling Methods 0.000 claims description 2
238000010521 absorption reaction Methods 0.000 claims 1
150000001412 amines Chemical class 0.000 claims 1
125000003277 amino group Chemical group 0.000 claims 1
238000004519 manufacturing process Methods 0.000 claims 1
238000006243 chemical reaction Methods 0.000 description 7
125000005219 aminonitrile group Chemical group 0.000 description 4
239000000203 mixture Substances 0.000 description 3
238000010025 steaming Methods 0.000 description 3
239000000126 substance Substances 0.000 description 3
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
239000003054 catalyst Substances 0.000 description 2
230000000052 comparative effect Effects 0.000 description 2
238000001816 cooling Methods 0.000 description 2
239000007791 liquid phase Substances 0.000 description 2
239000012071 phase Substances 0.000 description 2
FHKPTEOFUHYQFY-UHFFFAOYSA-N 2-aminohexanenitrile Chemical compound CCCCC(N)C#N FHKPTEOFUHYQFY-UHFFFAOYSA-N 0.000 description 1
-1 4 -fluorenyl Chemical group 0.000 description 1
URKYFRSLKUNMFG-UHFFFAOYSA-N 5-aminopyrrolidin-2-one Chemical compound NC1CCC(=O)N1 URKYFRSLKUNMFG-UHFFFAOYSA-N 0.000 description 1
KBMSFJFLSXLIDJ-UHFFFAOYSA-N 6-aminohexanenitrile Chemical compound NCCCCCC#N KBMSFJFLSXLIDJ-UHFFFAOYSA-N 0.000 description 1
JVGZXCCKUMXEOU-UHFFFAOYSA-N 7-aminoazepan-2-one Chemical compound NC1CCCCC(=O)N1 JVGZXCCKUMXEOU-UHFFFAOYSA-N 0.000 description 1
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
150000001409 amidines Chemical class 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
229910052794 bromium Inorganic materials 0.000 description 1
VHRGRCVQAFMJIZ-UHFFFAOYSA-N cadaverine Chemical compound NCCCCCN VHRGRCVQAFMJIZ-UHFFFAOYSA-N 0.000 description 1
238000001311 chemical methods and process Methods 0.000 description 1
229910052801 chlorine Inorganic materials 0.000 description 1
239000000460 chlorine Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
239000000428 dust Substances 0.000 description 1
229910052731 fluorine Inorganic materials 0.000 description 1
239000011737 fluorine Substances 0.000 description 1
229910052736 halogen Inorganic materials 0.000 description 1
150000002367 halogens Chemical class 0.000 description 1
239000012528 membrane Substances 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
230000003647 oxidation Effects 0.000 description 1
238000007254 oxidation reaction Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
229910052704 radon Inorganic materials 0.000 description 1
SYUHGPGVQRZVTB-UHFFFAOYSA-N radon atom Chemical compound [Rn] SYUHGPGVQRZVTB-UHFFFAOYSA-N 0.000 description 1
238000000926 separation method Methods 0.000 description 1
239000007787 solid Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/10—Separation of ammonia from ammonia liquors, e.g. gas liquors
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/02—Preparation of lactams
- C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Analytical Chemistry (AREA)
Inorganic Chemistry (AREA)
Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Other In-Based Heterocyclic Compounds (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

TW090113615A 2000-06-05 2001-06-05 Process for removal of ammonia from solutions including lactam and ammonia TW506970B (en)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE2000127328 DE10027328A1 (de)	2000-06-05	2000-06-05	Verfahren zur Abtrennung von Ammoniak aus Lösungen, die Caprolactam und Ammoniak enthalten
DE2000133516 DE10033516A1 (de)	2000-07-11	2000-07-11	Verfahren und Abtrennung von Ammoniak aus Lösungen, die Caprolactam, ein oligomeres Amid oder ein polymeres Amid oder Ammoniak enthalten

Publications (1)

Publication Number	Publication Date
TW506970B true TW506970B (en)	2002-10-21

Family

ID=26005932

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
TW090113615A TW506970B (en)	2000-06-05	2001-06-05	Process for removal of ammonia from solutions including lactam and ammonia

Country Status (17)

Country	Link
US (1)	US6896772B2 (fr)
EP (1)	EP1286963B2 (fr)
JP (1)	JP2003535846A (fr)
KR (1)	KR20030016279A (fr)
CN (1)	CN1204119C (fr)
AR (1)	AR029261A1 (fr)
AT (1)	ATE256109T1 (fr)
AU (1)	AU2001262336A1 (fr)
BR (1)	BR0111320A (fr)
CA (1)	CA2409344C (fr)
DE (1)	DE50101150D1 (fr)
ES (1)	ES2212790T3 (fr)
IL (1)	IL152837A0 (fr)
MX (1)	MXPA02011275A (fr)
MY (1)	MY127068A (fr)
TW (1)	TW506970B (fr)
WO (1)	WO2001094308A1 (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP3667140B2 (ja) *	1999-03-04	2005-07-06	パイオニア株式会社	ディスクチェンジャ装置
DE10253095A1 (de) *	2002-11-13	2004-06-17	Basf Ag	Verfahren zur Reinigung von Caprolactam
DE10253094A1 (de) *	2002-11-13	2004-05-27	Basf Ag	Verfahren zur Reinigung von Caprolactam
DE102004027022A1 (de) *	2004-06-02	2006-01-05	Basf Ag	Verfahren zur Abtrennung von Ammoniak und Wasser aus Lactam-haltigen Gemischen
GB2608159B (en) *	2021-06-24	2026-03-25	Process Ltd	A system and method for recovering ammonia from an ammonia-containing liquid
CN119822997A (zh) *	2023-10-13	2025-04-15	中国石油化工股份有限公司	一种从己内酰胺合成氨基己腈的方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE4339648A1 (de)	1993-11-20	1995-05-24	Basf Ag	Verfahren zur Herstellung von Caprolactam
DE4443125A1 (de) *	1994-12-03	1996-06-05	Basf Ag	Verfahren zur Herstellung von Caprolactam
DE19500222A1 (de) *	1995-01-05	1996-07-11	Basf Ag	Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin
US5717090A (en)	1995-01-05	1998-02-10	Basf Aktiengesellschaft	Simultaneous preparation of caprolactam and hexamethylenediamine
DE19548289A1 (de) *	1995-12-22	1997-06-26	Basf Ag	Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin
FR2781476B1 (fr) *	1998-07-22	2000-09-22	Rhone Poulenc Fibres	Procede de distillation d'ammoniac contenu dans un melange comprenant du caprolactame

2001
- 2001-06-01 MY MYPI20012613 patent/MY127068A/en unknown
- 2001-06-02 MX MXPA02011275A patent/MXPA02011275A/es active IP Right Grant
- 2001-06-02 ES ES01936425T patent/ES2212790T3/es not_active Expired - Lifetime
- 2001-06-02 WO PCT/EP2001/006310 patent/WO2001094308A1/fr not_active Ceased
- 2001-06-02 IL IL15283701A patent/IL152837A0/xx unknown
- 2001-06-02 AT AT01936425T patent/ATE256109T1/de not_active IP Right Cessation
- 2001-06-02 KR KR1020027016519A patent/KR20030016279A/ko not_active Ceased
- 2001-06-02 EP EP01936425A patent/EP1286963B2/fr not_active Expired - Lifetime
- 2001-06-02 CN CNB018106358A patent/CN1204119C/zh not_active Expired - Fee Related
- 2001-06-02 US US10/297,051 patent/US6896772B2/en not_active Expired - Fee Related
- 2001-06-02 CA CA002409344A patent/CA2409344C/fr not_active Expired - Fee Related
- 2001-06-02 AU AU2001262336A patent/AU2001262336A1/en not_active Abandoned
- 2001-06-02 JP JP2002501824A patent/JP2003535846A/ja not_active Withdrawn
- 2001-06-02 DE DE50101150T patent/DE50101150D1/de not_active Expired - Lifetime
- 2001-06-02 BR BR0111320-8A patent/BR0111320A/pt not_active Application Discontinuation
- 2001-06-04 AR ARP010102661A patent/AR029261A1/es not_active Application Discontinuation
- 2001-06-05 TW TW090113615A patent/TW506970B/zh not_active IP Right Cessation

Also Published As

Publication number	Publication date
MXPA02011275A (es)	2003-04-25
KR20030016279A (ko)	2003-02-26
EP1286963A1 (fr)	2003-03-05
US6896772B2 (en)	2005-05-24
EP1286963B1 (fr)	2003-12-10
CA2409344C (fr)	2007-11-27
EP1286963B2 (fr)	2012-10-24
CA2409344A1 (fr)	2002-11-15
AU2001262336A1 (en)	2001-12-17
JP2003535846A (ja)	2003-12-02
US20030132098A1 (en)	2003-07-17
CN1431993A (zh)	2003-07-23
ES2212790T3 (es)	2004-08-01
ATE256109T1 (de)	2003-12-15
WO2001094308A1 (fr)	2001-12-13
IL152837A0 (en)	2003-06-24
BR0111320A (pt)	2003-06-10
CN1204119C (zh)	2005-06-01
MY127068A (en)	2006-11-30
DE50101150D1 (de)	2004-01-22
AR029261A1 (es)	2003-06-18

Legal Events

Date	Code	Title	Description
2003-03-03	GD4A	Issue of patent certificate for granted invention patent
2006-08-01	MM4A	Annulment or lapse of patent due to non-payment of fees

Publication	Publication Date	Title
US5427759A (en)	1995-06-27	Method of recovering ammonia and compounds from offgases contaminated with organic materials, carbon dioxide, and ammonia
TW200404761A (en)	2004-04-01	Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column
KR100551461B1 (ko)	2006-02-14	미정제 액상 비닐 아세테이트의 후처리방법
CA2409344C (fr)	2007-11-27	Methode permettant de separer l'ammoniac des solutions contenant du pentano-5-lactame et de l'ammoniac
KR100503982B1 (ko)	2005-07-27	락탐 처리 방법
JP2003080001A (ja)	2003-03-18	水分を含有する有機溶媒の精製方法。
JP3854069B2 (ja)	2006-12-06	アンモニア蒸留方法
JP4961208B2 (ja)	2012-06-27	カプロラクタムの製造方法
JP4961209B2 (ja)	2012-06-27	テトラヒドロアゼピンを含む不純な６−アミノカプロニトリルからカプロラクタムを製造する方法
RU2004131537A (ru)	2005-04-10	Способ и устройство для непрерывного получения полиамида 6,6 и его сополиамидов
NL8200905A (nl)	1983-10-03	Werkwijze voor het scheiden van ammoniak en kooldioxide uit mengsels van ammoniak, kooldioxide en water.
JP2785629B2 (ja)	1998-08-13	ピロリドン類の製造法
CN118103346A (zh)	2024-05-28	从组合物获得脂族胺
JP4251506B2 (ja)	2009-04-08	Ｃ▲下１▼−ｃ▲下３▼炭化水素および／またはイソブタンで汚染されている塩化メチルを浄化する方法
IE45825B1 (en)	1982-12-01	Process for preparing a urea solution from nh3 and co2
EA008698B1 (ru)	2007-06-29	Способ отделения nhот смеси, содержащей nh, coи ho
JP2004501135A (ja)	2004-01-15	アミノカプロニトリルの蒸留分離方法
JP3995431B2 (ja)	2007-10-24	トリメチルアミンの精製方法
WO1998002416A1 (fr)	1998-01-22	Procede de separation de la cetoxime ou de l'aldoxime d'un amide
JP2003221366A (ja)	2003-08-05	メチルアミン類の製造方法
TW318180B (fr)	1997-10-21
DE10027328A1 (de)	2001-12-06	Verfahren zur Abtrennung von Ammoniak aus Lösungen, die Caprolactam und Ammoniak enthalten
JP2003290601A (ja)	2003-10-14	アセトンの回収方法
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