TWI342789B - - Google Patents

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Publication number: TWI342789B
Authority: TW; Taiwan
Prior art keywords: acid solution; waste; acid; waste acid; curing
Prior art date: 2007-01-26

Application number

TW96103041A

Other languages

English (en)

Chinese (zh)

Other versions

TW200831154A (en

Inventor

Ching Tsuen Huang

Ching Tu Chang

Original Assignee

Inst Nuclear Energy Res Aec

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2007-01-26

Filing date

2007-01-26

Publication date

2011-06-01

2007-01-26 Application filed by Inst Nuclear Energy Res Aec filed Critical Inst Nuclear Energy Res Aec

2007-01-26 Priority to TW96103041A priority Critical patent/TW200831154A/zh

2008-08-01 Publication of TW200831154A publication Critical patent/TW200831154A/zh

2011-06-01 Application granted granted Critical

2011-06-01 Publication of TWI342789B publication Critical patent/TWI342789B/zh

Links

239000002253 acid Substances 0.000 claims description 203
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 140
239000002699 waste material Substances 0.000 claims description 137
238000001723 curing Methods 0.000 claims description 82
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 70
239000003795 chemical substances by application Substances 0.000 claims description 57
238000000034 method Methods 0.000 claims description 42
239000007788 liquid Substances 0.000 claims description 39
239000010812 mixed waste Substances 0.000 claims description 36
RILZRCJGXSFXNE-UHFFFAOYSA-N 2-[4-(trifluoromethoxy)phenyl]ethanol Chemical compound OCCC1=CC=C(OC(F)(F)F)C=C1 RILZRCJGXSFXNE-UHFFFAOYSA-N 0.000 claims description 22
230000000087 stabilizing effect Effects 0.000 claims description 20
239000008187 granular material Substances 0.000 claims description 11
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 9
239000004568 cement Substances 0.000 claims description 8
238000002156 mixing Methods 0.000 claims description 8
239000000203 mixture Substances 0.000 claims description 8
MFGOFGRYDNHJTA-UHFFFAOYSA-N 2-amino-1-(2-fluorophenyl)ethanol Chemical compound NCC(O)C1=CC=CC=C1F MFGOFGRYDNHJTA-UHFFFAOYSA-N 0.000 claims description 7
RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical compound [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 claims description 7
229910001863 barium hydroxide Inorganic materials 0.000 claims description 7
HUCVOHYBFXVBRW-UHFFFAOYSA-M caesium hydroxide Inorganic materials [OH-].[Cs+] HUCVOHYBFXVBRW-UHFFFAOYSA-M 0.000 claims description 7
239000000843 powder Substances 0.000 claims description 6
238000003756 stirring Methods 0.000 claims description 6
239000010881 fly ash Substances 0.000 claims description 4
229910052739 hydrogen Inorganic materials 0.000 claims description 4
239000001257 hydrogen Substances 0.000 claims description 4
UNJPQTDTZAKTFK-UHFFFAOYSA-K cerium(iii) hydroxide Chemical compound [OH-].[OH-].[OH-].[Ce+3] UNJPQTDTZAKTFK-UHFFFAOYSA-K 0.000 claims description 3
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
230000002378 acidificating effect Effects 0.000 claims 2
150000004712 monophosphates Chemical class 0.000 claims 2
238000013006 addition curing Methods 0.000 claims 1
239000007789 gas Substances 0.000 claims 1
239000001117 sulphuric acid Substances 0.000 claims 1
235000011149 sulphuric acid Nutrition 0.000 claims 1
239000000243 solution Substances 0.000 description 129
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 9
238000006243 chemical reaction Methods 0.000 description 9
238000005202 decontamination Methods 0.000 description 9
238000012360 testing method Methods 0.000 description 9
230000003588 decontaminative effect Effects 0.000 description 7
238000005469 granulation Methods 0.000 description 7
230000003179 granulation Effects 0.000 description 7
238000007711 solidification Methods 0.000 description 7
230000008023 solidification Effects 0.000 description 7
239000002901 radioactive waste Substances 0.000 description 6
230000000694 effects Effects 0.000 description 5
239000010814 metallic waste Substances 0.000 description 5
238000001556 precipitation Methods 0.000 description 5
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 4
238000010306 acid treatment Methods 0.000 description 4
238000007654 immersion Methods 0.000 description 4
230000003472 neutralizing effect Effects 0.000 description 4
229910017604 nitric acid Inorganic materials 0.000 description 4
YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 3
229910019142 PO4 Inorganic materials 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
239000011737 fluorine Substances 0.000 description 3
229910052731 fluorine Inorganic materials 0.000 description 3
238000010438 heat treatment Methods 0.000 description 3
229910052751 metal Inorganic materials 0.000 description 3
239000002184 metal Substances 0.000 description 3
229910021645 metal ion Inorganic materials 0.000 description 3
235000006408 oxalic acid Nutrition 0.000 description 3
239000002245 particle Substances 0.000 description 3
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 3
239000010452 phosphate Substances 0.000 description 3
230000002285 radioactive effect Effects 0.000 description 3
WOCIAKWEIIZHES-UHFFFAOYSA-N ruthenium(iv) oxide Chemical compound O=[Ru]=O WOCIAKWEIIZHES-UHFFFAOYSA-N 0.000 description 3
150000003839 salts Chemical class 0.000 description 3
239000002910 solid waste Substances 0.000 description 3
239000010935 stainless steel Substances 0.000 description 3
229910001220 stainless steel Inorganic materials 0.000 description 3
XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
238000010669 acid-base reaction Methods 0.000 description 2
239000002956 ash Substances 0.000 description 2
OYLGJCQECKOTOL-UHFFFAOYSA-L barium fluoride Chemical compound [F-].[F-].[Ba+2] OYLGJCQECKOTOL-UHFFFAOYSA-L 0.000 description 2
229910001632 barium fluoride Inorganic materials 0.000 description 2
AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 2
239000000920 calcium hydroxide Substances 0.000 description 2
229910001861 calcium hydroxide Inorganic materials 0.000 description 2
239000001506 calcium phosphate Substances 0.000 description 2
229910000389 calcium phosphate Inorganic materials 0.000 description 2
235000011010 calcium phosphates Nutrition 0.000 description 2
238000005341 cation exchange Methods 0.000 description 2
238000009390 chemical decontamination Methods 0.000 description 2
230000001186 cumulative effect Effects 0.000 description 2
230000020169 heat generation Effects 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
239000010808 liquid waste Substances 0.000 description 2
239000007787 solid Substances 0.000 description 2
QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 2
239000002351 wastewater Substances 0.000 description 2
XMBRQILOBNSQEG-KIYNQFGBSA-N (2S)-2-[[4-[(2-amino-4-oxo-3H-pteridin-6-yl)methylamino]benzoyl]amino]-4-fluoropentanedioic acid Chemical compound FC(C(=O)O)C[C@@H](C(=O)O)NC(=O)C1=CC=C(NCC2=CN=C3N=C(N)NC(=O)C3=N2)C=C1 XMBRQILOBNSQEG-KIYNQFGBSA-N 0.000 description 1
TUSDEZXZIZRFGC-UHFFFAOYSA-N 1-O-galloyl-3,6-(R)-HHDP-beta-D-glucose Natural products OC1C(O2)COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC1C(O)C2OC(=O)C1=CC(O)=C(O)C(O)=C1 TUSDEZXZIZRFGC-UHFFFAOYSA-N 0.000 description 1
229910000975 Carbon steel Inorganic materials 0.000 description 1
KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
235000008733 Citrus aurantifolia Nutrition 0.000 description 1
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
239000001263 FEMA 3042 Substances 0.000 description 1
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
LRBQNJMCXXYXIU-PPKXGCFTSA-N Penta-digallate-beta-D-glucose Natural products OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-PPKXGCFTSA-N 0.000 description 1
102220510219 Poly(A)-specific ribonuclease PNLDC1_S31G_mutation Human genes 0.000 description 1
206010036790 Productive cough Diseases 0.000 description 1
241000239226 Scorpiones Species 0.000 description 1
239000005864 Sulphur Substances 0.000 description 1
235000011941 Tilia x europaea Nutrition 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
229910052786 argon Inorganic materials 0.000 description 1
LYSTYSFIGYAXTG-UHFFFAOYSA-L barium(2+);hydrogen phosphate Chemical compound [Ba+2].OP([O-])([O-])=O LYSTYSFIGYAXTG-UHFFFAOYSA-L 0.000 description 1
238000003339 best practice Methods 0.000 description 1
229910052797 bismuth Inorganic materials 0.000 description 1
JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 1
229910000416 bismuth oxide Inorganic materials 0.000 description 1
210000000476 body water Anatomy 0.000 description 1
230000037396 body weight Effects 0.000 description 1
229910052791 calcium Inorganic materials 0.000 description 1
239000011575 calcium Substances 0.000 description 1
239000010962 carbon steel Substances 0.000 description 1
229910010293 ceramic material Inorganic materials 0.000 description 1
229910000420 cerium oxide Inorganic materials 0.000 description 1
ABSOMGPQFXJESQ-UHFFFAOYSA-M cesium;hydroxide;hydrate Chemical compound O.[OH-].[Cs+] ABSOMGPQFXJESQ-UHFFFAOYSA-M 0.000 description 1
239000013522 chelant Substances 0.000 description 1
239000013043 chemical agent Substances 0.000 description 1
239000012295 chemical reaction liquid Substances 0.000 description 1
239000012141 concentrate Substances 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
239000004035 construction material Substances 0.000 description 1
230000008602 contraction Effects 0.000 description 1
229910052802 copper Inorganic materials 0.000 description 1
239000010949 copper Substances 0.000 description 1
238000005336 cracking Methods 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
230000006378 damage Effects 0.000 description 1
230000007547 defect Effects 0.000 description 1
238000011161 development Methods 0.000 description 1
AAOVKJBEBIDNHE-UHFFFAOYSA-N diazepam Chemical compound N=1CC(=O)N(C)C2=CC=C(Cl)C=C2C=1C1=CC=CC=C1 AAOVKJBEBIDNHE-UHFFFAOYSA-N 0.000 description 1
229960003529 diazepam Drugs 0.000 description 1
TYIXMATWDRGMPF-UHFFFAOYSA-N dibismuth;oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Bi+3].[Bi+3] TYIXMATWDRGMPF-UHFFFAOYSA-N 0.000 description 1
GFAUEQXLYWIWRU-UHFFFAOYSA-L dicesium hydrogen phosphate Chemical compound [Cs+].[Cs+].OP([O-])([O-])=O GFAUEQXLYWIWRU-UHFFFAOYSA-L 0.000 description 1
238000011038 discontinuous diafiltration by volume reduction Methods 0.000 description 1
238000004043 dyeing Methods 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
229910001653 ettringite Inorganic materials 0.000 description 1
238000011049 filling Methods 0.000 description 1
239000012530 fluid Substances 0.000 description 1
-1 fluoroboron bismuth Chemical compound 0.000 description 1
230000005484 gravity Effects 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
239000004571 lime Substances 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000000463 material Substances 0.000 description 1
238000009392 mechanical decontamination Methods 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
239000011259 mixed solution Substances 0.000 description 1
238000012986 modification Methods 0.000 description 1
230000004048 modification Effects 0.000 description 1
210000003205 muscle Anatomy 0.000 description 1
238000006386 neutralization reaction Methods 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 description 1
238000012545 processing Methods 0.000 description 1
230000000750 progressive effect Effects 0.000 description 1
238000011084 recovery Methods 0.000 description 1
238000011160 research Methods 0.000 description 1
239000011347 resin Substances 0.000 description 1
229920005989 resin Polymers 0.000 description 1
229910001925 ruthenium oxide Inorganic materials 0.000 description 1
238000000926 separation method Methods 0.000 description 1
239000008281 solid sol Substances 0.000 description 1
210000003802 sputum Anatomy 0.000 description 1
208000024794 sputum Diseases 0.000 description 1
230000006641 stabilisation Effects 0.000 description 1
238000011105 stabilization Methods 0.000 description 1
239000004575 stone Substances 0.000 description 1
UUCCCPNEFXQJEL-UHFFFAOYSA-L strontium dihydroxide Chemical compound [OH-].[OH-].[Sr+2] UUCCCPNEFXQJEL-UHFFFAOYSA-L 0.000 description 1
229910001866 strontium hydroxide Inorganic materials 0.000 description 1
229910052717 sulfur Inorganic materials 0.000 description 1
239000011593 sulfur Substances 0.000 description 1
LRBQNJMCXXYXIU-NRMVVENXSA-N tannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-NRMVVENXSA-N 0.000 description 1
229940033123 tannic acid Drugs 0.000 description 1
235000015523 tannic acid Nutrition 0.000 description 1
229920002258 tannic acid Polymers 0.000 description 1
238000005406 washing Methods 0.000 description 1

Landscapes

Processing Of Solid Wastes (AREA)

TW96103041A 2007-01-26 2007-01-26 Method of solidification and stabilization of waste acid solution TW200831154A (en)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
TW96103041A TW200831154A (en)	2007-01-26	2007-01-26	Method of solidification and stabilization of waste acid solution

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
TW96103041A TW200831154A (en)	2007-01-26	2007-01-26	Method of solidification and stabilization of waste acid solution

Publications (2)

Publication Number	Publication Date
TW200831154A TW200831154A (en)	2008-08-01
TWI342789B true TWI342789B (de)	2011-06-01

Family

ID=44818489

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
TW96103041A TW200831154A (en)	2007-01-26	2007-01-26	Method of solidification and stabilization of waste acid solution

Country Status (1)

Country	Link
TW (1)	TW200831154A (de)

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JP6549372B2 (ja) *	2014-12-16	2019-07-24	吉田　英夫	トリチウム水による汚染土壌および汚染水の除染方法および除染システム
TWI741802B (zh) *	2020-09-21	2021-10-01	黃慶村	硼酸鹽廢液的處理方法
CN114242293A (zh) *	2021-11-18	2022-03-25	中国辐射防护研究院	一种放射性减容处理废液固化处理方法

2007
- 2007-01-26 TW TW96103041A patent/TW200831154A/zh not_active IP Right Cessation

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Publication number	Publication date
TW200831154A (en)	2008-08-01

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Date	Code	Title	Description
2022-03-01	MM4A	Annulment or lapse of patent due to non-payment of fees

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