TWI432412B - 用於回收對苯二甲酸之經改良的方法 - Google Patents

用於回收對苯二甲酸之經改良的方法 Download PDF

Info

Publication number: TWI432412B
Authority: TW; Taiwan
Prior art keywords: temperature; hot; acid; control system; pressure
Prior art date: 2007-05-31

Application number

TW097120219A

Other languages

English (en)

Chinese (zh)

Other versions

TW200909407A (en

Inventor

Alessandro Baldelli

Carlo Cattaneo

Giovanni Cocco

Andrea Gnagnetti

Marzio Monagheddu

Luciano Piras

Original Assignee

Dow Italia S R L

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2007-05-31

Filing date

2008-05-30

Publication date

2014-04-01

2008-05-30 Application filed by Dow Italia S R L filed Critical Dow Italia S R L

2009-03-01 Publication of TW200909407A publication Critical patent/TW200909407A/zh

2014-04-01 Application granted granted Critical

2014-04-01 Publication of TWI432412B publication Critical patent/TWI432412B/zh

Links

KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 title claims description 53
238000000034 method Methods 0.000 title claims description 21
238000011084 recovery Methods 0.000 title description 3
239000002002 slurry Substances 0.000 claims description 18
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
239000007788 liquid Substances 0.000 claims description 14
239000007789 gas Substances 0.000 claims description 13
QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 claims description 12
ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 claims description 12
239000007787 solid Substances 0.000 claims description 11
238000001914 filtration Methods 0.000 claims description 9
239000012535 impurity Substances 0.000 claims description 8
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 6
238000010438 heat treatment Methods 0.000 claims description 6
150000001732 carboxylic acid derivatives Chemical class 0.000 claims description 4
239000011261 inert gas Substances 0.000 claims description 3
229910052757 nitrogen Inorganic materials 0.000 claims description 3
238000007254 oxidation reaction Methods 0.000 claims description 2
239000012530 fluid Substances 0.000 claims 2
150000002762 monocarboxylic acid derivatives Chemical class 0.000 claims 1
230000003647 oxidation Effects 0.000 claims 1
238000005502 peroxidation Methods 0.000 claims 1
LPNBBFKOUUSUDB-UHFFFAOYSA-N p-toluic acid Chemical compound CC1=CC=C(C(O)=O)C=C1 LPNBBFKOUUSUDB-UHFFFAOYSA-N 0.000 description 18
GOUHYARYYWKXHS-UHFFFAOYSA-N 4-formylbenzoic acid Chemical compound OC(=O)C1=CC=C(C=O)C=C1 GOUHYARYYWKXHS-UHFFFAOYSA-N 0.000 description 10
239000012065 filter cake Substances 0.000 description 9
239000013078 crystal Substances 0.000 description 8
238000004519 manufacturing process Methods 0.000 description 5
239000000047 product Substances 0.000 description 5
239000011343 solid material Substances 0.000 description 4
239000002253 acid Substances 0.000 description 3
238000004140 cleaning Methods 0.000 description 3
238000002425 crystallisation Methods 0.000 description 3
230000008025 crystallization Effects 0.000 description 3
239000000203 mixture Substances 0.000 description 3
229920000139 polyethylene terephthalate Polymers 0.000 description 3
239000005020 polyethylene terephthalate Substances 0.000 description 3
239000012265 solid product Substances 0.000 description 3
239000000243 solution Substances 0.000 description 3
238000005406 washing Methods 0.000 description 3
URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
230000001276 controlling effect Effects 0.000 description 2
230000000694 effects Effects 0.000 description 2
230000004907 flux Effects 0.000 description 2
238000005984 hydrogenation reaction Methods 0.000 description 2
239000000463 material Substances 0.000 description 2
XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
-1 polyethylene terephthalate Polymers 0.000 description 2
239000007864 aqueous solution Substances 0.000 description 1
238000007664 blowing Methods 0.000 description 1
238000005119 centrifugation Methods 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
238000009833 condensation Methods 0.000 description 1
230000005494 condensation Effects 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
238000006073 displacement reaction Methods 0.000 description 1
238000001035 drying Methods 0.000 description 1
238000010981 drying operation Methods 0.000 description 1
238000005886 esterification reaction Methods 0.000 description 1
239000004744 fabric Substances 0.000 description 1
238000004128 high performance liquid chromatography Methods 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
238000005191 phase separation Methods 0.000 description 1
XNGIFLGASWRNHJ-UHFFFAOYSA-L phthalate(2-) Chemical compound [O-]C(=O)C1=CC=CC=C1C([O-])=O XNGIFLGASWRNHJ-UHFFFAOYSA-L 0.000 description 1
229920000642 polymer Polymers 0.000 description 1
229920005862 polyol Polymers 0.000 description 1
150000003077 polyols Chemical class 0.000 description 1
238000011085 pressure filtration Methods 0.000 description 1
238000000746 purification Methods 0.000 description 1
238000004064 recycling Methods 0.000 description 1
230000001105 regulatory effect Effects 0.000 description 1
238000005201 scrubbing Methods 0.000 description 1
239000007790 solid phase Substances 0.000 description 1
238000003860 storage Methods 0.000 description 1
239000002699 waste material Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
- C07C63/14—Monocyclic dicarboxylic acids
- C07C63/15—Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
- C07C63/24—1,3 - Benzenedicarboxylic acid
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
- C07C63/14—Monocyclic dicarboxylic acids
- C07C63/15—Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
- C07C63/26—1,4 - Benzenedicarboxylic acid
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
- C07C63/307—Monocyclic tricarboxylic acids

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Oil, Petroleum & Natural Gas (AREA)
Crystallography & Structural Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Physical Or Chemical Processes And Apparatus (AREA)

TW097120219A 2007-05-31 2008-05-30 用於回收對苯二甲酸之經改良的方法 TWI432412B (zh)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
US93244707P	2007-05-31	2007-05-31

Publications (2)

Publication Number	Publication Date
TW200909407A TW200909407A (en)	2009-03-01
TWI432412B true TWI432412B (zh)	2014-04-01

Family

ID=40378756

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
TW097120219A TWI432412B (zh)	2007-05-31	2008-05-30	用於回收對苯二甲酸之經改良的方法

Country Status (8)

Country	Link
EP (1)	EP2155649A2 (de)
JP (2)	JP2010528100A (de)
KR (2)	KR101827229B1 (de)
CN (1)	CN101679185B (de)
BR (1)	BRPI0811380A2 (de)
RU (1)	RU2009149616A (de)
TW (1)	TWI432412B (de)
WO (1)	WO2009024872A2 (de)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CN101624342B (zh) *	2009-08-13	2012-10-31	中国纺织工业设计院	精对苯二甲酸制备中cta分离过滤的方法及系统
GB201008412D0 (en) *	2010-05-20	2010-07-07	Davy Process Techn Ltd	Process and system
CN102933539A (zh) *	2010-06-28	2013-02-13	戴维加工技术有限公司	从浆中分离羧酸(比如对苯二酸)的方法和系统
CN102992999B (zh) *	2011-09-17	2014-08-27	中国石油化工股份有限公司	精间苯二甲酸装置氧化单元粗间苯二甲酸“过滤、洗涤”套洗方法
US9663307B2 (en)	2012-07-12	2017-05-30	Ineos Europe Ag	Process for operating hot particle rotary valves

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS56134154A (en) *	1980-03-25	1981-10-20	Hitachi Seiki Co Ltd	Preventing device for temperature-rise in rotary valve
JP2595657B2 (ja) *	1988-05-27	1997-04-02	三井石油化学工業株式会社	スラリーから結晶を回収する方法
US5175355A (en) *	1991-04-12	1992-12-29	Amoco Corporation	Improved process for recovery of purified terephthalic acid
GB9310070D0 (en) *	1992-05-29	1993-06-30	Ici Plc	Process for the production of purified terephthalic acid
GB9400570D0 (en) *	1994-01-13	1994-03-09	Ici Plc	Handling of materials at elevated pressure
JPH11179115A (ja) *	1997-12-24	1999-07-06	Mitsui Chem Inc	スラリーからの結晶回収方法および装置
JP2000159348A (ja) *	1998-11-25	2000-06-13	Hokuetsu Giken Kogyo:Kk	小型ロ―タリ―バルブ
WO2000071226A1 (en) *	1999-05-24	2000-11-30	Baker Hughes Incorporated	Pressure filtration device and method employing a depressurizing chamber and material transport
BR0016947A (pt) *	1999-12-29	2002-09-10	Inca Internat S P A	Processo para recuperar ácido tereftálico (tpa) purificado
JP2003002452A (ja) *	2001-06-22	2003-01-08	Kawasaki Steel Corp	ロータリ・バルブ
JP3985507B2 (ja) *	2001-11-22	2007-10-03	株式会社豊田自動織機	斜板型圧縮機

2008
- 2008-05-16 WO PCT/IB2008/003093 patent/WO2009024872A2/en not_active Ceased
- 2008-05-16 CN CN2008800181141A patent/CN101679185B/zh active Active
- 2008-05-16 JP JP2010509918A patent/JP2010528100A/ja active Pending
- 2008-05-16 KR KR1020177004565A patent/KR101827229B1/ko active Active
- 2008-05-16 KR KR1020097024808A patent/KR20100019462A/ko not_active Ceased
- 2008-05-16 EP EP08827920A patent/EP2155649A2/de not_active Withdrawn
- 2008-05-16 BR BRPI0811380-7A2A patent/BRPI0811380A2/pt not_active Application Discontinuation
- 2008-05-16 RU RU2009149616/04A patent/RU2009149616A/ru unknown
- 2008-05-30 TW TW097120219A patent/TWI432412B/zh active
2014
- 2014-07-03 JP JP2014137642A patent/JP2014221791A/ja active Pending

Also Published As

Publication number	Publication date
KR20170026634A (ko)	2017-03-08
TW200909407A (en)	2009-03-01
JP2010528100A (ja)	2010-08-19
RU2009149616A (ru)	2011-07-10
CN101679185A (zh)	2010-03-24
KR101827229B1 (ko)	2018-02-07
EP2155649A2 (de)	2010-02-24
BRPI0811380A2 (pt)	2014-12-09
WO2009024872A2 (en)	2009-02-26
CN101679185B (zh)	2013-07-10
JP2014221791A (ja)	2014-11-27
WO2009024872A3 (en)	2009-05-07
KR20100019462A (ko)	2010-02-18

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US5705682A (en)	1998-01-06	Process for producing highly pure terephthalic acid
KR101004211B1 (ko)	2010-12-24	조질 카복실산 슬러리의 정제 방법
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