UA99321C2 - Способ непрерывного получения циклогексанона и химическая установка - Google Patents
Способ непрерывного получения циклогексанона и химическая установкаInfo
- Publication number
- UA99321C2 UA99321C2 UAA201009006A UAA201009006A UA99321C2 UA 99321 C2 UA99321 C2 UA 99321C2 UA A201009006 A UAA201009006 A UA A201009006A UA A201009006 A UAA201009006 A UA A201009006A UA 99321 C2 UA99321 C2 UA 99321C2
- Authority
- UA
- Ukraine
- Prior art keywords
- fraction
- phenol
- cyclohexanone
- distillation
- trays
- Prior art date
Links
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 title abstract 10
- 238000000034 method Methods 0.000 title abstract 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 8
- 238000004821 distillation Methods 0.000 abstract 4
- 239000000047 product Substances 0.000 abstract 3
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 2
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 238000012856 packing Methods 0.000 abstract 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 abstract 2
- 239000006227 byproduct Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 229910052763 palladium Inorganic materials 0.000 abstract 1
- 229910052697 platinum Inorganic materials 0.000 abstract 1
- 238000005292 vacuum distillation Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/48—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups
- C07C29/50—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups with molecular oxygen only
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/006—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrogenation of aromatic hydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP07024764 | 2007-12-20 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UA99321C2 true UA99321C2 (ru) | 2012-08-10 |
Family
ID=39420745
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UAA201009006A UA99321C2 (ru) | 2007-12-20 | 2008-12-16 | Способ непрерывного получения циклогексанона и химическая установка |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US8618334B2 (ru) |
| EP (1) | EP2234952A1 (ru) |
| JP (1) | JP2011506547A (ru) |
| KR (1) | KR20100099310A (ru) |
| CN (1) | CN101945845B (ru) |
| EA (1) | EA201001033A1 (ru) |
| TW (1) | TWI434825B (ru) |
| UA (1) | UA99321C2 (ru) |
| WO (1) | WO2009080621A1 (ru) |
Families Citing this family (34)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009080618A1 (en) * | 2007-12-20 | 2009-07-02 | Dsm Ip Assets B.V. | Cyclohexanone production process with impurities removal |
| PL2231577T3 (pl) * | 2007-12-20 | 2012-07-31 | Dsm Ip Assets Bv | Proces produkcji cykloheksanonu za pomocą wielokrotnej destylacji następczej |
| US9689615B2 (en) | 2012-08-21 | 2017-06-27 | Uop Llc | Steady state high temperature reactor |
| US9205398B2 (en) | 2012-08-21 | 2015-12-08 | Uop Llc | Production of butanediol from a methane conversion process |
| US9707530B2 (en) | 2012-08-21 | 2017-07-18 | Uop Llc | Methane conversion apparatus and process using a supersonic flow reactor |
| US8933275B2 (en) | 2012-08-21 | 2015-01-13 | Uop Llc | Production of oxygenates from a methane conversion process |
| US8937186B2 (en) | 2012-08-21 | 2015-01-20 | Uop Llc | Acids removal and methane conversion process using a supersonic flow reactor |
| US9656229B2 (en) | 2012-08-21 | 2017-05-23 | Uop Llc | Methane conversion apparatus and process using a supersonic flow reactor |
| US9327265B2 (en) | 2012-08-21 | 2016-05-03 | Uop Llc | Production of aromatics from a methane conversion process |
| US9370757B2 (en) | 2012-08-21 | 2016-06-21 | Uop Llc | Pyrolytic reactor |
| US8927769B2 (en) | 2012-08-21 | 2015-01-06 | Uop Llc | Production of acrylic acid from a methane conversion process |
| US9308513B2 (en) | 2012-08-21 | 2016-04-12 | Uop Llc | Production of vinyl chloride from a methane conversion process |
| US9434663B2 (en) | 2012-08-21 | 2016-09-06 | Uop Llc | Glycols removal and methane conversion process using a supersonic flow reactor |
| US9023255B2 (en) | 2012-08-21 | 2015-05-05 | Uop Llc | Production of nitrogen compounds from a methane conversion process |
| CN103265418A (zh) * | 2013-06-08 | 2013-08-28 | 南京德力菲技术咨询有限公司 | 一种水合环己烯法环己醇制己内酰胺原料环己酮的方法 |
| EP3180303B1 (en) * | 2014-08-15 | 2018-07-18 | ExxonMobil Chemical Patents Inc. | Process and system for making cyclohexanone |
| US9902676B2 (en) * | 2014-08-15 | 2018-02-27 | Exxonmobil Chemical Patents Inc. | Process for making cyclohexanone |
| SG11201700415UA (en) | 2014-08-15 | 2017-02-27 | Exxonmobil Chemical Patents Inc | Process and system for making cyclohexanone |
| EP3180302B1 (en) | 2014-08-15 | 2019-01-30 | ExxonMobil Chemical Patents Inc. | Process for producing cyclohexanone |
| WO2016025214A1 (en) | 2014-08-15 | 2016-02-18 | Exxonmobil Chemical Patents Inc. | Process and system for making cyclohexanone |
| WO2016053583A1 (en) | 2014-09-30 | 2016-04-07 | Exxonmobil Chemical Patents Inc. | Process for making cyclohexanone |
| US10301243B2 (en) | 2014-11-10 | 2019-05-28 | Cap Iii B.V. | Process for the production of cyclohexanone from phenol |
| TWI691480B (zh) * | 2014-12-15 | 2020-04-21 | 荷蘭商卡普三世責任有限公司 | 用來建構用於生產環己酮之設備的方法 |
| ES2737174T3 (es) * | 2015-05-22 | 2020-01-10 | Cap Iii Bv | Proceso para la preparación de una mezcla que contiene ciclohexanona y ciclohexanol |
| ES2713679T3 (es) * | 2015-07-06 | 2019-05-23 | Cap Iii Bv | Un proceso para la producción de una mezcla que comprende ciclohexanol y ciclohexanona |
| EP3115353A1 (en) * | 2015-07-10 | 2017-01-11 | GFBiochemicals Ltd. | Process for the isolation of levulinic acid |
| US10259765B2 (en) | 2015-07-31 | 2019-04-16 | Exxonmobil Chemical Patents Inc. | Process for making cyclohexanone |
| US10252968B2 (en) | 2015-07-31 | 2019-04-09 | Exxonmobil Chemical Patents Inc. | Process for making cyclohexanone |
| CN105967984B (zh) * | 2016-06-02 | 2018-04-17 | 中国化学赛鼎宁波工程有限公司 | 苯酚生产环己酮的方法及系统 |
| WO2019005274A1 (en) | 2017-06-28 | 2019-01-03 | Exxonmobil Chemical Patents Inc. | PROCESS FOR PRODUCTION OF CYCLOHEXANONE |
| WO2019005273A1 (en) | 2017-06-28 | 2019-01-03 | Exxonmobil Chemical Patents Inc. | PRODUCTS CONTAINING CYCLOHEXANONE AND METHODS OF MAKING THE SAME |
| US10745336B2 (en) | 2017-06-28 | 2020-08-18 | Exxonmobil Chemical Patents Inc. | Cyclohexanone-containing products and processes for making the same |
| WO2020031765A1 (ja) * | 2018-08-09 | 2020-02-13 | 日本曹達株式会社 | 電解酸化によるトリキノイル及び／又はその水和物の製造方法 |
| CN111662160B (zh) * | 2019-03-06 | 2024-04-12 | 中国石油化工股份有限公司 | 一种提高环己醇脱氢装置产能的方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2829166A (en) * | 1933-04-04 | 1958-04-01 | Allied Chem & Dye Corp | Hydrogenation of phenol |
| US3305586A (en) | 1959-05-15 | 1967-02-21 | Stamicarbon | Process for preparing cyclohexanone |
| US4272326A (en) | 1980-01-24 | 1981-06-09 | Allied Chemical Corporation | Enhanced distillation of cyclohexanol from phenol with additional cyclohexanone feed |
| US4306944A (en) * | 1980-07-03 | 1981-12-22 | Allied Corporation | Cyclohexanone distillation process |
| NL8102280A (nl) * | 1981-05-09 | 1982-12-01 | Stamicarbon | Werkwijze voor het zuiveren van epsilon-caprolactam. |
| US5131984A (en) * | 1991-09-23 | 1992-07-21 | Allied-Signal Inc. | High quality phenol rectification with energy recovery |
| DE4205633A1 (de) * | 1992-02-25 | 1993-08-26 | Bayer Antwerpen Nv | Verfahren zur reinigung von cyclohexanon |
| WO2000011113A1 (en) * | 1998-08-21 | 2000-03-02 | Schumann-Sasol (South Africa) (Proprietary) Limited | Process for distilling fischer-tropsch derived paraffinic hydrocarbons |
| EP1433774A1 (en) | 2002-12-27 | 2004-06-30 | Koninklijke DSM N.V. | Process for reducing the aldehyde concentration in a mixture comprising cyclohexanone and one or more aldehydes |
| TW200738602A (en) * | 2006-02-01 | 2007-10-16 | Asahi Kasei Chemicals Corp | Industrial process for producing high-purity diol |
| WO2009080618A1 (en) * | 2007-12-20 | 2009-07-02 | Dsm Ip Assets B.V. | Cyclohexanone production process with impurities removal |
| PL2231577T3 (pl) * | 2007-12-20 | 2012-07-31 | Dsm Ip Assets Bv | Proces produkcji cykloheksanonu za pomocą wielokrotnej destylacji następczej |
-
2008
- 2008-12-16 WO PCT/EP2008/067635 patent/WO2009080621A1/en not_active Ceased
- 2008-12-16 UA UAA201009006A patent/UA99321C2/ru unknown
- 2008-12-16 EA EA201001033A patent/EA201001033A1/ru unknown
- 2008-12-16 US US12/809,257 patent/US8618334B2/en active Active
- 2008-12-16 CN CN2008801272010A patent/CN101945845B/zh active Active
- 2008-12-16 EP EP08864701A patent/EP2234952A1/en not_active Withdrawn
- 2008-12-16 KR KR1020107016105A patent/KR20100099310A/ko not_active Withdrawn
- 2008-12-16 JP JP2010538654A patent/JP2011506547A/ja active Pending
- 2008-12-19 TW TW097149687A patent/TWI434825B/zh active
Also Published As
| Publication number | Publication date |
|---|---|
| EA201001033A1 (ru) | 2010-12-30 |
| CN101945845A (zh) | 2011-01-12 |
| TWI434825B (zh) | 2014-04-21 |
| US20110054142A1 (en) | 2011-03-03 |
| WO2009080621A1 (en) | 2009-07-02 |
| EP2234952A1 (en) | 2010-10-06 |
| JP2011506547A (ja) | 2011-03-03 |
| TW200936554A (en) | 2009-09-01 |
| US8618334B2 (en) | 2013-12-31 |
| CN101945845B (zh) | 2013-09-18 |
| KR20100099310A (ko) | 2010-09-10 |
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