US2071651A - Process and device for degumming ramie and other similar fibers - Google Patents
Process and device for degumming ramie and other similar fibers Download PDFInfo
- Publication number
- US2071651A US2071651A US4200235A US2071651A US 2071651 A US2071651 A US 2071651A US 4200235 A US4200235 A US 4200235A US 2071651 A US2071651 A US 2071651A
- Authority
- US
- United States
- Prior art keywords
- fibers
- fiber
- cage
- degumming
- ramie
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000835 fiber Substances 0.000 title description 46
- 238000000034 method Methods 0.000 title description 20
- 240000008564 Boehmeria nivea Species 0.000 title description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- 230000033001 locomotion Effects 0.000 description 9
- 239000000344 soap Substances 0.000 description 6
- 239000000126 substance Substances 0.000 description 5
- 238000004061 bleaching Methods 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 239000008234 soft water Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 241001648341 Orites Species 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 238000009940 knitting Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Images
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C1/00—Treatment of vegetable material
- D01C1/02—Treatment of vegetable material by chemical methods to obtain bast fibres
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T292/00—Closure fasteners
- Y10T292/48—Seals
Definitions
- This present invention is characterized in that the very adhesive gum which binds together the fine filaments of decorticated ramie (China grass) can be completely removed by a very simple andeconomical process, and with mechanical means without having recourse to any chemical reaction.
- the process is essentially mechanical, inasmuch as the degumming is obtained by merely submitting the fiber to a suitable vibratory shaking after a short treatment in an open keir with a light solution of hot water and ordinary soda or potash soap.
- Neuter soaps, i. e. free of an excess of alkali are preferable, and the water should be soft.
- Fig. 1 shows a front view of the cage and the vibratory mechanical shaking device
- Fig. 2 shows, in longitudinal section, one of the additional circular trays which can be inserted into the cage
- Fig. 3 shows, in a longitudinal section, the cage introduced into the keir for the degumming operation.
- the fiber there are two ways of operating; but in either .case it is advisable to allow the fiber to soak for several hours beforehand in water before submitting it to the treatment proper, as thiswill remove a considerable portion of the coloring matter and facilitate subsequent bleaching operations.
- first method the fiber is immerged in water either cold or already heated, with about 1% (of the weight of the water) or soap as aforesaid. The temperature is gradually raised to 75-85 centidegrees (167 to 185 F.) and held at that for about 30 minutes, and then raised to boiling point for two or .three' minutes.
- the fiber is extracted from the hot bath and plunged in cold water, running preferably, and submitted to an energetic vibratory shaking. Almost immediately the fiber will be observed to assume the aspect of a silky pulp the filaments disengaging themselves from each other. .In less than a minute the operation is completed and the fiber, after being rinsed, always under According to a vibration, and preferably in running water for the purpose also of eliminating the particles of bark entangled in the fiber, is ready for the bleaching bath which if containing hypochl'orite of calcium as one of its ingredients will have the effect of 5 causing whatever little residue of soapy matter maybe still clinging to the filaments, to flocculate-this flocculation being removed by the subsequent rinsing.
- the process is the same as described in method above indicated; then after the fiber has been allowed to remain at a temperature of from 167 to 185 F. (75-85 centidegrees) for about 30 minutes the vibratory motion is applied in the same hot bath.
- the mass of fiber will at once assume the aspect of a silky pulp and the filaments will become disengaged.
- the fiber is thereupon withdrawn from the soapy solution, is rinsedunder vibration in clean hot water, and immerged in a third bath of hot water which is raised for a short while to boiling point, vibration being applied continually in the meantime.
- Rinsing in cold water, preferably running, follows; also bleaching process as per the first method.
- the vibratory action maybe transmitted in the desired conditions to the entire mass of fiber, the latter should be placed in such a manner as to enable the mechanical device whereby the vibration is produced to effectively exercise its effect in the proper direction.
- the appliance hereinafter described is one of the means especially adapted to obtain the abovesaid result.
- Fig. 1 the-dimen- 40 sions whereof will vary according to the quantity of fiber it is found desirable to treat at a time
- a platform A open at the top and closed at the bottom by a platform A as hereinafter described.
- the topring B is joined to the platform by means of four equidistant rods C, C, C",C"', which will serve also -as legs, the ends whereof are embossed in rubber.
- the rods are strongly bound to each other by crossed stays I.
- the Whole system should be extremely rigid and to this end the metal employed for its construction'should be particularly adapted to resist vibration and suitably protected from corrosion caused by the bleaching liquor.
- the vibrating apparatuses On two of the abovesaid rods which face each other, (I. i. C and C) are fixed, outside of the cage, the vibrating apparatuses. They consist respectively in a supporting block E and E rigidly attached to the cage and connected with the bottom and lateral sections thereof by means of strong stays.
- the supporting block carries on the top part an axis F and F on which revolves, on a. horizontal plane, a metal disc, G'and G, of such' dimensions and weight as to produce the necessary vibration.
- the vibration is obtained by the axis of rotation of the disc being made eccentric and the higher the eccentricity the more ample the vibration will be, of course.
- the axis of rotation of the disc can be displaced so as to regulate the amplitude of the vibration.
- the rotation of the disc is obtained by means of a driving belt on the'pulley H, H which is attached to the disc or by any other suitable mechanical device.
- the transmission of the vibration to the entire mass of fiber under treatment is obtained by the following means.
- the diameter ofthe needles will be that of an ordinary knitting needle.
- the fiber on being removed from the water after the first soaking, is spread out but not pressed on the platform in a layer corresponding in thickness to the length of the needles, and perpendicularly to the direction that the vibratory motion will have, i. e. perpendicular"to the rods which carry the vibratoryapparatuses.
- the second layer is spread out in a like manner on a circular tray L (Fig. 2), made of wire netting same as platform A of a suitable diameter for easy insertion in the tiplying the number of the vibrating units, the
- the cage with its load of fiber being now ready for the degumming operation, it is hoisted by some suitable gear, brought over the keir or vat containing the solution of water and soap and lowered into same. Thereafter the process is as respectively described for the two aforesaid methods.
- the process can be usefully extended to other textile fibers similar to China grass.
- Process for degumming ramie and other like fibers which comprises soaking the fibers in a solution of soft water and washing soap to soften the gummy substance adhering to the fibers and subjecting the fibers to a vibratory motion.
- Process for degumming ramie and other like fibers which comprises subjecting the fibers to a hot saponaceous bath, plunging the fibers into cold water and thereafter subjecting the fibers to vibratory motion.
- a process for degumming ramie and other like fibers which comprises boiling the fibers in a hot soapy solution until the gummy substance adhering to the fibers is softened and then subjecting the fibers to vibratory motion until the said substances are emulsified and separated from the fibers.
- Apparatus for degumming ramie and other fibers comprising an open-topped cage, a wire platform forming the bottom of the cage, a series of needles with rounded points fixed in said platform in spaced relation to each other, a series of wire trays mounted above said platform in superposed relation, similar needles projecting upwardly and downwardly from each of said trays, the needles being embedded in the fibers on the platform and on the trays, and means for vibrating the cage.
- Apparatus for degumming ramie and other like fibers comprising a cage, needles mounted in the cage for engaging the fibers, supporting means at each side of the cage, rotary spindles carried by said means, eccentric discs carried by said spindles and means for rotating the spindles and discs for imparting vibratory movement to the cage.
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Molecular Biology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Textile Engineering (AREA)
- Treatment Of Fiber Materials (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT2071651X | 1935-08-27 | ||
| GB271339A GB521528A (en) | 1939-01-26 | 1939-01-26 | Process and device for de-gumming ramie and other similar fibres |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US2071651A true US2071651A (en) | 1937-02-23 |
Family
ID=31995659
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US4200235 Expired - Lifetime US2071651A (en) | 1935-08-27 | 1935-09-25 | Process and device for degumming ramie and other similar fibers |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US2071651A (fr) |
| BE (1) | BE432220A (fr) |
| DE (1) | DE660150C (fr) |
| FR (2) | FR795166A (fr) |
| GB (1) | GB447013A (fr) |
-
0
- BE BE432220D patent/BE432220A/xx unknown
-
1935
- 1935-09-10 DE DEN38587D patent/DE660150C/de not_active Expired
- 1935-09-14 GB GB2556435A patent/GB447013A/en not_active Expired
- 1935-09-23 FR FR795166D patent/FR795166A/fr not_active Expired
- 1935-09-25 US US4200235 patent/US2071651A/en not_active Expired - Lifetime
-
1939
- 1939-01-18 FR FR50178D patent/FR50178E/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| BE432220A (fr) | 1900-01-01 |
| FR50178E (fr) | 1939-01-17 |
| FR795166A (fr) | 1936-03-07 |
| GB447013A (en) | 1936-05-11 |
| DE660150C (de) | 1938-05-19 |
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