US2082817A - Method of producing a concentrate of chrome ores - Google Patents

Method of producing a concentrate of chrome ores Download PDF

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Publication number
US2082817A
US2082817A US724633A US72463334A US2082817A US 2082817 A US2082817 A US 2082817A US 724633 A US724633 A US 724633A US 72463334 A US72463334 A US 72463334A US 2082817 A US2082817 A US 2082817A
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ores
concentrate
producing
chrome
flotation
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US724633A
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Arnold Gustav
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EDUARD VON ORELLI
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EDUARD VON ORELLI
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03DFLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00Flotation
    • B03D1/001Flotation agents
    • B03D1/002Inorganic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03DFLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D2203/00Specified materials treated by the flotation agents; Specified applications
    • B03D2203/02Ores
    • B03D2203/04Non-sulfide ores

Definitions

  • 2o sulphurized may be mentioned by way of example: Au, CuSiOa, SnOz, PbO, PbOs, Pba04 ZnCOs, ZnQ, ZnSiOi, F8203, FeCOs FeO, Cr203, further all manganese-tungsten ores.
  • the above mentioned drawback of the simultaneous floating of the ore and matrix may be overcome with oxidized chrome-ores by preliminarily treating these ores with a complex heteropolyacid or its salts.
  • complex heteropolyacids is to be understood as referring to acids obtained by replacing in an oxygen bearing acid one or more atoms of oxygen by oxygen bearing acid radicals of which one at least is of difterent'chemical nature than the fundamental acid.
  • the iollowing complex heteropolyacids may be mentioned: phosphomolybdic acids, phosphotungstic acids, and the like.
  • Example 1 kilogram of crushed chrome iron ore is, in the presence of water, subjected to the action of 0.135 gramme of phospho-molybdic acid, whereupon 0.8-1" gramme of sodium-palmitate as collecting agent and 0.02 gramme of pine oil as a frothing agent is added.
  • the latter stabilizes the froth in which the ore collects free from the matrix.
  • 0.1 gramme of waterglass is advisable in 1 a further addition, whereupon the floating process is carried out in the known manner.
  • phospho-tungstic acid instead of phospho-molybdic acid or its salts phospho-tungstic acid may be used in the above example. 15
  • the method of producing a concentrate of chrome ores by means of froth-flotation which comprises treating oxidized chrome ores with a substance selected from the group consisting of phosphomolybdic acids, phosphotungstic acids, and their salts, and subjecting the product thus obtained to flotation by means of usual froth flotation agents.
  • the method of producing a concentrate of chrome-ores by means of froth-flotation which comprises treating oxidized chrome ores with a substance selected from the group consisting of phosphomolybdic acids and their salts and subjecting the product thus obtained to flotation by means of usual froth flotation agents.

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  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Description

Patented June 8, 1937 UNITED STATES PATENT OFFlCE Gustav Arnold, Wadenswil, Switzerland, assignor, by mesne assignments, to Eduard von Orelli,
Zurich, Switzerland No Drawing. Application May 8, 1934, Serial No.
724,633. In Switzerland August 19, 1933 3 Claims. (01. 209166) useful particles of the ore the useless matrix takes part in the floating. In order to obviate this drawback the oxygen atoms on the surface of the ore have been substituted by sulphur in order to obtain an easier'floating capacity of the ores. The sulphurizing of the surface of the ore can, however, not be carried out with all the oxidized ores as the degree of the sulphurization depends on the affinity of the respective metal to sulphur.
2o sulphurized may be mentioned by way of example: Au, CuSiOa, SnOz, PbO, PbOs, Pba04 ZnCOs, ZnQ, ZnSiOi, F8203, FeCOs FeO, Cr203, further all manganese-tungsten ores.
. According to the present invention the above mentioned drawback of the simultaneous floating of the ore and matrix may be overcome with oxidized chrome-ores by preliminarily treating these ores with a complex heteropolyacid or its salts.
The term complex heteropolyacids is to be understood as referring to acids obtained by replacing in an oxygen bearing acid one or more atoms of oxygen by oxygen bearing acid radicals of which one at least is of difterent'chemical nature than the fundamental acid. By way of example the iollowing complex heteropolyacids may be mentioned: phosphomolybdic acids, phosphotungstic acids, and the like.
The following ores which cannot be Example 1 kilogram of crushed chrome iron ore is, in the presence of water, subjected to the action of 0.135 gramme of phospho-molybdic acid, whereupon 0.8-1" gramme of sodium-palmitate as collecting agent and 0.02 gramme of pine oil as a frothing agent is added. The latter stabilizes the froth in which the ore collects free from the matrix. 0.1 gramme of waterglass is advisable in 1 a further addition, whereupon the floating process is carried out in the known manner.
Instead of phospho-molybdic acid or its salts phospho-tungstic acid may be used in the above example. 15
I claim:
1. The method of producing a concentrate of chrome ores by means of froth-flotation which comprises treating oxidized chrome ores with a substance selected from the group consisting of phosphomolybdic acids, phosphotungstic acids, and their salts, and subjecting the product thus obtained to flotation by means of usual froth flotation agents.
2. The method of producing a concentrate of chrome-ores by means of froth-flotation which comprises treating oxidized chrome ores with a substance selected from the group consisting of phosphomolybdic acids and their salts and subjecting the product thus obtained to flotation by means of usual froth flotation agents.
3. The method of producing a concentrate of chrome-ores by, means of froth-flotation which comprises treating oxidized chrome ores with a substance selected from the group consisting of 35 phosphotungstic acid and their salts and subjectlng the product thus obtained to 'flotation by means or usual froth flotation agents.
GUSTAV ARNOLD.
US724633A 1933-08-19 1934-05-08 Method of producing a concentrate of chrome ores Expired - Lifetime US2082817A (en)

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CH2082817X 1933-08-19

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