US3053727A - Mounting for electrical resistance elements and method for preparing the same - Google Patents
Mounting for electrical resistance elements and method for preparing the same Download PDFInfo
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- US3053727A US3053727A US62140A US6214060A US3053727A US 3053727 A US3053727 A US 3053727A US 62140 A US62140 A US 62140A US 6214060 A US6214060 A US 6214060A US 3053727 A US3053727 A US 3053727A
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- millboard
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- acid phosphate
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- 238000000034 method Methods 0.000 title description 16
- ILRRQNADMUWWFW-UHFFFAOYSA-K aluminium phosphate Chemical compound O1[Al]2OP1(=O)O2 ILRRQNADMUWWFW-UHFFFAOYSA-K 0.000 claims description 42
- 239000010425 asbestos Substances 0.000 claims description 41
- 229910052895 riebeckite Inorganic materials 0.000 claims description 41
- 230000002093 peripheral effect Effects 0.000 claims description 35
- 239000000835 fiber Substances 0.000 claims description 22
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 21
- 239000005909 Kieselgur Substances 0.000 claims description 20
- 239000004115 Sodium Silicate Substances 0.000 claims description 20
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 20
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 18
- 239000007795 chemical reaction product Substances 0.000 claims description 13
- 239000000243 solution Substances 0.000 description 45
- 239000000203 mixture Substances 0.000 description 22
- 229910052910 alkali metal silicate Inorganic materials 0.000 description 20
- 239000007864 aqueous solution Substances 0.000 description 16
- 239000000047 product Substances 0.000 description 16
- 239000004111 Potassium silicate Substances 0.000 description 15
- 238000005520 cutting process Methods 0.000 description 15
- 229910052913 potassium silicate Inorganic materials 0.000 description 15
- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 description 15
- 235000019353 potassium silicate Nutrition 0.000 description 15
- 238000004519 manufacturing process Methods 0.000 description 14
- 238000013508 migration Methods 0.000 description 14
- 230000005012 migration Effects 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
- 238000010438 heat treatment Methods 0.000 description 12
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 8
- 239000011230 binding agent Substances 0.000 description 8
- 238000012360 testing method Methods 0.000 description 7
- 238000011065 in-situ storage Methods 0.000 description 6
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- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 230000000704 physical effect Effects 0.000 description 4
- 230000008093 supporting effect Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000005470 impregnation Methods 0.000 description 3
- 230000001976 improved effect Effects 0.000 description 3
- 230000007246 mechanism Effects 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- 238000009825 accumulation Methods 0.000 description 2
- 230000004913 activation Effects 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 235000000396 iron Nutrition 0.000 description 2
- 239000010445 mica Substances 0.000 description 2
- 229910052618 mica group Inorganic materials 0.000 description 2
- 239000010452 phosphate Substances 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 230000007928 solubilization Effects 0.000 description 2
- 238000005063 solubilization Methods 0.000 description 2
- 241001251094 Formica Species 0.000 description 1
- 101100114416 Neurospora crassa (strain ATCC 24698 / 74-OR23-1A / CBS 708.71 / DSM 1257 / FGSC 987) con-10 gene Proteins 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000001680 brushing effect Effects 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000002079 cooperative effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- PHTXVQQRWJXYPP-UHFFFAOYSA-N ethyltrifluoromethylaminoindane Chemical compound C1=C(C(F)(F)F)C=C2CC(NCC)CC2=C1 PHTXVQQRWJXYPP-UHFFFAOYSA-N 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000009740 moulding (composite fabrication) Methods 0.000 description 1
- 239000002985 plastic film Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
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- 238000005303 weighing Methods 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
Images
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/02—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances
- H01B3/06—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances asbestos
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/24—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing alkyl, ammonium or metal silicates; containing silica sols
- C04B28/26—Silicates of the alkali metals
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16L—PIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
- F16L59/00—Thermal insulation in general
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
- H05B3/10—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor
- H05B3/16—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor the conductor being mounted on an insulating base
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/30—Nailable or sawable materials
Definitions
- This invention relates to a substitute material or product for mica or ceramic components which is useful in and about electrical devices. More particularly the invention comprises a novel and improved product for the fabrication of mountings, supports or the like for electrical resistance heating elements, and the method of producing the same.
- Asbestos millboard, and various compositions or products based upon or comprising asbestos millboard have heretofore been proposed and utilized in the manufacture of mountings or supports for electrical resistance elements, and some have been so employed with varying degrees of success.
- One type of improved asbestos millboard support for high resistance electrical conductors for example, is illustrated by United States Letters Patent No. 2,541,273.
- the asbestos millboard mounting or support products now available for electrical appliance and the like nevertheless, have not been extensively adapted or utilized by manufacturers of electrical devices or appliances because of their generally poor electrical properties and/ or lack of strength, among other disadvantages.
- Another object of this invention is to provide an asbestos millboard product or composition which exhibits improved and adequate electrical insulating properties throughout all humidity conditions over extended periods of time and which is completely resistant to the temperature conditions encountered in electrical heating devices or mechanisms such as irons, toasters, heaters, etc.
- An additional object of this invention is to provide mounting or support means for electrical resistance heating elements or wires and a method of producing the same, which will resist warping or deformation and will maintain their rigidity, coherency, dimensional stability,
- portions generally comprise the means for supporting, securing and retaining the wires comprising the heating ele ents and accordingly consist of a critical portion or area which is subjected to the greatest stress and severest temperature conditions.
- a still further object of this invention is to provide a method or means for producing an inexpensive asbestos millboard product or composition which has greater strength and electrical insulating properties than have heretofore been available in such products for use as a mounting or support for electrical resistance heating elements.
- FIG. 1 is a plane view illustrating a typical millboard mounting for toaster heating elements showing the serrated edge portions comprising a series of cut-out forming projections or nibs;
- FIG. 2 is a cross-sectional view taken on line 2-2 of FIG. 1.
- the porous asbestos millboard which has been determined to be effectively receptive to the indurating procedure or treatment briefly comprises a medium density board composed of asbestos fiber, a relatively high proportion of diatomaceous earth, and, as a binder, a dry, activated in situ, alkali metal silicate consisting of sodium and/or potassium silicate.
- the indurating procedure which has been found to effectively complement the asbestos millboard of this invention comprises the application of an aluminum acid phosphate impregnant coupled with a unique means of curing the same.
- porous millboard comprising the foregoing components, upon substantially complete solubilization or activation of the dry alkali metal silicate binder may be cut, punched or otherwise reduced to its ultimate size and/or configuration for an electrical resistance mounting or support prior to the indurating treatment comprising the aqueous aluminum acid phosphate solution impregnation or in accordance with the more preferred procedure, the board is initially impregnated with the indurating aluminum acid phosphate solution and subsequently cut, punched or the like to obtain a mounting or support of the ultimate configuration and/or size desired while still wet or containing the absorbed aluminum acid phosphate solution.
- the sequence or order of rendering the board to the ultimate size and configuration of the intended product and of applying the indurating impregnation is not critical provided that the cutting or shaping of the millboard mount or support to its ultimate physical form or configuration is completed before removal or loss of a substantial amount of the absorbed aqueous aluminum acid phosphate impregnating solution.
- the two major surfaces, i.e., the front and back sides, of the board or mounting formed therefrom are blanketed or covered with a substantially water-impervious material such as a plastic sheet to bar or impede egress or escape of the water content of the impregnating solution from either of said major surfaces and to direct and confine migration of the aqueous solution to the marginal or peripheral edge portion(s) of the shaped mounting or support whereby the escape of the water content therefrom results in an accumulation or higher concentration of the solution solute in and about said marginal or peripheral edge portion(s) of the mounting and in turn further increases the beneficial effects of the impregnant in the critical portions of the object.
- a substantially water-impervious material such as a plastic sheet to bar or impede egress or escape of the water content of the impregnating solution from either of said major surfaces and to direct and confine migration of the aqueous solution to the marginal or peripheral edge portion(s) of the shaped mounting or support whereby the escape of the water content therefrom results in an accumulation or higher
- Asbestos millboard electrical resistance element or wire mountings or supports typically consist of sheets of more or less conventional types of inorganic millboard products which are cut or otherwise shaped to a general configuration suitably adaptable for installation in the particular electrical device or appliance contemplated.
- the peripheral edge portion(s), or segments thereof, of the shaped mount or support of the usual sheet construction is provided with some means of supporting and retaining or securing the electrical resistance heating elements or wires, or coils composed of the same, which generally consist simply of a multiplicity of marginal perforations or a series of edge cuts or notches forming a serrated or scalloped border area of alternating slots and projections or nibs through or in which the wire or like component may be threaded and securely retained.
- 1 of the drawing comprises a typical design or configuration of an asbestos millboard sheet mounting or support for an electric toaster resistance wire heating element illustrating a conventional serrated border or peripheral edge portion(s) configuration which provides effective retaining and spacing means for resistance wires or elements and conveniently ready access in stringing or winding the same.
- the marginal or peripheral edge and corners or ends of a product of an object composed of a frangible material such as a sheet of asbestos millboard naturally comprise an area(s) of maximum stress and in turn breakage, and such a precarious condition or susceptibility is obviously further aggravated or intensified by the cutting of perforations, slots or the like and removal of a portion of the material from this area, and subsequent installation of wires, etc., handling, and repeated exposure to the high temperatures of the wires comprising the heating elements.
- this invention In addition to providing an asbestos millboard composition or product of sufiicient strength and electrical properties to replace and surpass previous conventional materials, this invention also embodies or provides for the reinforcement of the critical marginal edge or corner portions of the millboard article by concentrating the effects thereof or characteristics imparted thereby, such as structural strength, resistance to heat, breakage and deformation, and dielectric properties, within and about said portions or areas.
- the reinforcing effect of this invention is produced by a concentration or accumulation of the aluminum acid phosphate indurating solution solute in the portions or areas most suspectible to damage, breakage and deterioration or the like.
- FIG. 2 cross-sectional view of the object of FIG. 1 visually illustrates the concentration of the aluminum acid phosphate indurating solution solute or reaction product(s) thereof in and about the edge(s) portions of the millboard mount.
- the asbestos millboard component of this invention should comprise approximately 40-60% by weight of asbestos fiber, approximately 35-45% by weight of diatomaceous earth, and approximately 7.5-12.5% by weight of dry sodium and/or potassium silicate, preferably consisting of about 50% by weight of asbestos fiber, about 40% by weight of diatomaceous earth, and about 10% by Weight of dry sodium silicate, and may be prepared or formed from any typical source or grade of the specified components commonly utilized in the manufacture of millboard. It has been determined, however, that the use of a relatively short grade asbestos fiber in the board will further enhance both the strength and electrical properties of the final product.
- a suitable and preferred grade of asbestos fiber comprises one having approximately the following McNett analysis stated as the weight percent passing through a standard mesh screen:
- Formation of the millboard can be effected on a wet machine or in any conventional manner, but activation or solubilization of the relatively insoluble dry alkali metal silicate binder requires substantial periods of exposure to elevated temperature and moisture conditions, such, for example, as temperature in the vicinity of approximately 200 to 400 F., preferably about 300 F., and high moisture conditions ranging from about to 100% relative humidity for periods of approximately 4 to 8 hours.
- the indurating impregnant an aqueous solution of aluminum acid phosphate, is prepared by combining hydrated alumina (Al O .H O) with phosphoric acid (H PO in a mol ratio of, for example, about 1.4/3.0 of hydrated alumina to phosphoric acid.
- H PO phosphoric acid
- the products thereof should be diluted to produce a readily handleable solution for the subsequent impregnation, typically about a 25% solution concentration.
- 'Induration of the millboard may be carried out by any convenient or suitable impregnating procedure, viz., dipping or submerging, spraying, brushing, coating, etc., but should be carried to the point wherein the millboard retains 15 to 50% by weight of the aluminum acid phosphate solute, preferably approximately 30% of solute by weight of the board.
- the aluminum acid phosphate indurant, or a component or components thereof reacts with the millboard or the asbestos constituent thereof to result in a hard, lntegrated product(s) of outstanding strength and electrical properties.
- Asbestos fiber (Grade 5K) 1, 000 50 Diatomaceous earth 800 40 Dry silicate of soda 200 Table 1 PHYSICAL PROPERTIES OF UNTREA'IED MILLBOARD [Avg of 12 samples-cross section of entire run] 4 .6. 10.62163 lb./sq. in.
- An indurating impregnant for the millboard was prepared by combining 55.3 lbs. of 85% phosphoric acid (H PO with 17.3 lbs. of hydrated alumina (Alcoa C-31) and upon allowing the reaction to go to substantial completion, adding suflicient water, in this case 134 lbs, to produce a 25% solids solution.
- the millboard cut into strips 5 m" x 48" for convenience in handling and subsequent processing and saturated with a 25% solids aluminum acid phosphate solution by pouring this solution on a strip ahead of a small hand operated wringer and duplicating the procedure for the other side whereby a solution pick-up was obtained of approximately 17-18% solution solids based upon the weight of the millboard and the solids of the solution.
- the treated millboard strips were divided into two equal groups and half were first dried at 170-180 F. for approximately 20 hours and then toaster mounts were die punched from the dry millboard strips in the configuration illustrated in FIG. 1. From the other half of the impregnated millboard strips, toaster elements of an identical configuration were die punched while the millboard was still wet with and containing the absorbed aluminum acid phosphate solution.
- the wet punched mounts were PHYSICAL PROPERTIES OF TREATED MILLBOARD [Avg of 10 samples (18% phosphate solids pick-upbased ontnoiimal wt. of board). Weighed immediately after satura 10H Weight (lo/sq. ft.) Caliper mils) Density (lb/cu. ft; MD tensile (lb/in. 54D tensile (1b./in.)
- Density (lb/cu. ft.) 41 MD tensile (p.s.i.) 457 CD tensile (p.s.i.) 276 was saturated by submersion in an aluminum phosphate indurating impregnant comprising phosphoric acid and hydrated alumina (Alcoa C-31) in a mol ratio of 321.4, prepared by combining 52 lbs. of hydrated alumina with 166 lbs. of phosphoric acid (85%) and upon completion of the reaction diluted with sutficient water to produce a 25% solution. The average pick-up was 21% by weight.
- the saturated boards were dried at approximately 200 F. and portions thereof were cut for testing.
- the method of manufacturing mountings for electrical resistance elements which comprises treating millboard consisting essentially of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45% by weight of diatomaceous earth and approximately 7.5 to 12.5% by weight of alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, by accumulating a higher concentration of indurating impregnant in the peripheral edge portion of the cut millboard mounting impregnated with an aqueous solution of aluminum acid phosphate indurant and containing at least about by weight of aluminum acid phosphate solute, comprising the step of blanketing the millboard mounting while wet on its two major surfaces to impede egress of the absorbed aqueous impregnating solution from these surfaces and to direct migration of the aqueous impregnating solution to the o peripheral edge portion and permit escape of the water content therefrom.
- alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof
- the method of manufacturing mountings for electrical resistance elements which comprises treating millboard consisting essentially of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45% by weight of diatomaceous earth and approximately 7.5 to 12.5% by weight of alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof by impregnating the same with an indurating aqueous solution of aluminum acid phosphate until the millboard retains at least about 15 by weight of solute, accumulating a higher concentration of the indurating impregnant in the peripheral edge portion of the millboard mounting to reinforce the same by cutting the millboard to its ultimate configuration while wet with the absorbed aqueous impregnating solution, then blanketing the wet millboard mounting on its two major surfaces to impede egress of the absorbed aqueous impregnating solution from these surfaces and to direct migration of the aqueous impregnating solution to the peripheral edge portion of the mounting and permit escape of the water content therefrom.
- alkali metal silicate selected from the group
- the method of manufacturing mountings for electrical resistance elements which comprises treating millboard consisting essentially of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45% by weight of diatomaceous earth and approximately 7.5 to 12.5 by weight of alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, by cutting the millboard to its ultimate configuration and impregnating the same with an indurating aqueous solution of aluminum acid phosphate until the millboard retains at least about 15 by weight of solute, accumulating a higher concentration of the indurating impregnant in the peripheral edge portion of the millboard mounting to reinforce the same by blanketing the wet millboard mounting on its two major surfaces to impede egress of the absorbed aqueous impregnating solution from the surfaces and to direct migration of the aqueous impregnating solution to the periph eral edge portion of the mounting and permit escape of the water content therefrom.
- the method of manufacturing mountings for electrical resistance elements which comprises treating millboard consisting essentially of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45 by weight of diatomaceous earth and approximately 7.5 to 12.5% by weight of alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, by impregnating the same with an indurating aqueous solution of aluminum acid phosphate until the millboard retains about 15 to 40% by weight of solute, accumulating a higher concentration of the indurating impregnant in the peripheral edge portion of the millboard mounting to reinforce the same by completing the cutting of the millboard to its ultimate configuration while wet with the absorbed aqueous impregnating solution, then blanketing the wet millboard mounting on its two major surfaces to impede egress of the absorbed aqueous impregnating solution from these surfaces and to direct migration of the aqueous impregnating solution to the peripheral edge portions of the mounting and permit escape of the water content therefrom.
- alkali metal silicate
- the method of manufacturing mountings for electrical resistance elements which comprises treating millboard consisting essentially of approximately 50% by weight of asbestos fiber, approximately 40% by weight of diatomaceous earth and approximately 10% by weight of alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, by impregnating the same with an indurating aqueous solution of aluminum acid phosphate until the millboard retains at least about 20 to 30% by weight of the solute, accumulating a higher concentration of the indurating impregnant in the peripheral edge portion of the millboard mounting to reinforce the same by cutting the millboard to its ultimate configuration while wet with the absorbed aqueous impregnating solution, then blanketing the wet millboard mounting on its two major surfaces to impede egress of the absorbed aqueous impregnating solution from these surfaces and to direct migration of the aqueous impregnating solution to the peripheral edge portion of the mounting and permit escape of the water content therefrom.
- the method of manufacturing mountings for electrical resistance elements which comprises forming a millboard from a furnish consisting essentially of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45% by weight of diatomaceous earth and approximately 7.5 to 12.5% by weight of dry alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, activating the dry alkali metal silicate binder by exposing the formed millboard to high temperature and moisture conditions to solubilize the same, indurating the millboard by impregnating the same with an aqueous solution of aluminum acid phosphate until it retains at least about 15% by weight of solute and accumulating a higher concentration of the indurating impregnant in the peripheral edge portion of the millboard mounting to reinforce the same by cutting the millboard to its ultimate configuration either before or upon completion of the impregnating treatment but prior to drying of the absorbed aqueous impregnating solution from the millboard, then blanketing the wet millboard mounting on its two major surfaces to impede egress of
- the method of manufacturing mountings for electrical resistance elements which comprises forming a millboard from a furnish consisting essentially of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45 by weight of diatomaceous earth and approximately 7.5 to 12.5% by weight of dry alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, activating the dry alkali metal silicate binder by exposing the formed millboard to high temperature and moisture conditions to solubilize the same, indurating the millboard by impregnating the same with an aqueous solution of aluminum acid phosphate until it retains at least about 15 by Weight of the solute and accumulating a higher concentration of the indurating impregnant in the peripheral edge portion of the millboard mounting to reinforce the same by cutting the millboard to its ultimate configuration prior to drying of the absorbed aqueous impregnating solution, then blanketing the wet millboard mounting on its two major surfaces to impede egress of the absorbed aqueous impregnating solution from these surfaces and to
- the method of manufacturing mountings for electrical resistance elements which comprises forming a millboard from a furnish consisting essentially of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45% by weight of diatomaceous earth and approximately 7.5 to 12.5 by weight of dry alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, activating the dry alkali metal silicate binder by exposing the formed billboard to high temperature and moisture conditions to solubilize the same, cutting the millboard to its ultimate configuration and indurating the same by impregnating it with an aqueous solution of aluminum acid phosphate until the millboard retains at least about 15% by weight of solute and accumulating a higher con- 10 centration of indurating impregnant in the peripheral edge portion of the millboard mounting to reinforce the same by blanketing the wet millboard mounting on its two major surfaces to impede egress of the absorbed aqueous solution from these surfaces and to direct migration of the aqueous impregnating solution to the peripheral edge portion
- the method of manufacturing mountings for electrical resistance elements which comprises forming a millboard from a furnish consisting essentially of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45% by weight of diatomaceous earth, and approximately 7.5 to 12.5 by weight of dry alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, activating the dry alkali metal silicate binder by exposing the formed millboard to temperatures of at least about 200 F.
- the method of manufacturing mountings for electrical resistance elements which comprises forming a millboard from a furnish consisting essentially of approximately 50% by weight of asbestos fiber, approximately 40% by weight of diatomaceous earth and approximately 10% by weight of dry sodium silicate, activating the dry sodium silicate binder by exposing the formed millboard to temperatures of about 200-400 F.
- a mounting for electrical resistance elements which consists essentially of a millboard composed of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45% by weight of diatomaceous earth and approximately 7.5 to 12.5 by weight of solubilized in situ alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, containing at least about 15% by weight of aluminum acid phosphate and the reaction products of the millboard and aluminum acid phosphate, said aluminum acid phosphate and the reaction products of the same with the millboard being present in a higher concentration in the peripheral edge portion of the millboard mounting than in the intermediate portion thereof.
- a mounting for electrical resistance elements which consists essentially of a millboard composed of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45% by weight of diatomaceous earth and approximately 7.5 to 12.5% by weight of solubilized in situ alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, containing about 15 to 40% by weight of aluminum acid phosphate and the reaction product of the millboard and the aluminum acid phosphate, said aluminum acid phosphate and the reaction products of the same with the millboard being present in a higher concentration in the peripheral edge portion of the millboard mounting than in the' intermediate portion thereof.
- a mounting for electrical resistance elements which consists essentially of a millboard prepared from a furnish consisting essentially of approximately 40 to 60% by weight of asbestos fiber, approximately 35 to 45% by weight of diatomaceous earth and approximately 7.5 to 12.5% by weight of solubilized in situ alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, containing about 15 to 40% by weight of aluminum acid phosphate and the reaction products of the millboard and the aluminum acid phosphate, said aluminum acid phosphate and the reaction products of the same With the millboard being present in a higher concentration in the peripheral edge portion of the millboard mounting than in the intermediate portion thereof.
- a mounting for electrical resistance elements which consists essentially of a millboard prepared from a furnish consisting essentially of approximately 50% by weight of asbestos fiber, approximately 40% by Weight of diatomaceous earth and approximately 10% by weight of solubilized in situ alkali metal silicate selected from the group consisting of sodium silicate and potassium silicate and mixtures thereof, containing about 20 to 30% by weight of aluminum acid phosphate and the reaction products of the millboard and aluminum acid phosphate, said aluminum acid phosphate and the reaction products of the same with the millboard being present in a higher concentration in the peripheral edge portion of the millboard mounting than in the intermediate portion thereof.
- a mounting for electrical resistance elements which consists essentially of a millboard prepared from a furnish consisting essentially of approximately 50% by weight of asbestos fiber, approximately 40% by Weight of diatomaceous earth and approximately 10% by Weight or" solubilized in situ sodium silicate, containing about 20 to 30% by weight of aluminum acid phosphate and the reaction products of the millboard and aluminum acid phosphate, said aluminum acid phosphate and the reaction products of the same with the millboard being present in a higher concentration in the peripheral edge portion of the millboard mounting than in the intermediate portion thereof.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Mechanical Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Fireproofing Substances (AREA)
- Insulating Bodies (AREA)
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US62140A US3053727A (en) | 1960-10-12 | 1960-10-12 | Mounting for electrical resistance elements and method for preparing the same |
| GB33623/61A GB943864A (en) | 1960-10-12 | 1961-09-20 | Mounting for electrical resistance elements and method for preparing the same |
| BE608953A BE608953A (fr) | 1960-10-12 | 1961-10-09 | Monture d'éléments de résistance électrique et leur procédé de fabrication. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US62140A US3053727A (en) | 1960-10-12 | 1960-10-12 | Mounting for electrical resistance elements and method for preparing the same |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US3053727A true US3053727A (en) | 1962-09-11 |
Family
ID=22040461
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US62140A Expired - Lifetime US3053727A (en) | 1960-10-12 | 1960-10-12 | Mounting for electrical resistance elements and method for preparing the same |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US3053727A (fr) |
| BE (1) | BE608953A (fr) |
| GB (1) | GB943864A (fr) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3212960A (en) * | 1962-12-04 | 1965-10-19 | Johns Manville | Asbestos-glass fiber saturating paper containing thermoplastic resin and aluminum acid phosphate |
| US3493463A (en) * | 1966-05-10 | 1970-02-03 | Bird Machine Co | Process and apparatus for forming a high strength band along the length of a paper web |
| US20090149310A1 (en) * | 2007-01-19 | 2009-06-11 | Dean Veral Neubauer | Pulling roll material for manufacture of sheet glass |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5057349A (en) * | 1990-03-02 | 1991-10-15 | William Perry | Insert for use in fabric-painting |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1780623A (en) * | 1929-07-26 | 1930-11-04 | Emil C Loetscher | Process for manufacturing building material of varying densities |
| US1812969A (en) * | 1926-03-01 | 1931-07-07 | Masonite Corp | Process of making integral insulating board with hard welded surfaces |
| US2341645A (en) * | 1940-05-16 | 1944-02-15 | Celotex Corp | Tiling |
| US2541273A (en) * | 1947-10-13 | 1951-02-13 | Proctor Electric Co | Support for high resistance electrical conductors and method of making the same |
| US2702761A (en) * | 1949-07-12 | 1955-02-22 | Celotex Corp | Method of impregnating fiber insulation board |
| US2826236A (en) * | 1954-05-29 | 1958-03-11 | Balzaretti Modigliani Spa | Method and apparatus for uninterrupted production of surface coated layers of bondedmineral wool |
-
1960
- 1960-10-12 US US62140A patent/US3053727A/en not_active Expired - Lifetime
-
1961
- 1961-09-20 GB GB33623/61A patent/GB943864A/en not_active Expired
- 1961-10-09 BE BE608953A patent/BE608953A/fr unknown
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1812969A (en) * | 1926-03-01 | 1931-07-07 | Masonite Corp | Process of making integral insulating board with hard welded surfaces |
| US1780623A (en) * | 1929-07-26 | 1930-11-04 | Emil C Loetscher | Process for manufacturing building material of varying densities |
| US2341645A (en) * | 1940-05-16 | 1944-02-15 | Celotex Corp | Tiling |
| US2541273A (en) * | 1947-10-13 | 1951-02-13 | Proctor Electric Co | Support for high resistance electrical conductors and method of making the same |
| US2702761A (en) * | 1949-07-12 | 1955-02-22 | Celotex Corp | Method of impregnating fiber insulation board |
| US2826236A (en) * | 1954-05-29 | 1958-03-11 | Balzaretti Modigliani Spa | Method and apparatus for uninterrupted production of surface coated layers of bondedmineral wool |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3212960A (en) * | 1962-12-04 | 1965-10-19 | Johns Manville | Asbestos-glass fiber saturating paper containing thermoplastic resin and aluminum acid phosphate |
| US3493463A (en) * | 1966-05-10 | 1970-02-03 | Bird Machine Co | Process and apparatus for forming a high strength band along the length of a paper web |
| US20090149310A1 (en) * | 2007-01-19 | 2009-06-11 | Dean Veral Neubauer | Pulling roll material for manufacture of sheet glass |
| US7842632B2 (en) * | 2007-01-19 | 2010-11-30 | Corning Incorporated | Pulling roll material for manufacture of sheet glass |
Also Published As
| Publication number | Publication date |
|---|---|
| GB943864A (en) | 1963-12-11 |
| BE608953A (fr) | 1962-04-09 |
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