US3898982A - Capillary tube for blood examination - Google Patents

Capillary tube for blood examination Download PDF

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Publication number
US3898982A
US3898982A US401175A US40117573A US3898982A US 3898982 A US3898982 A US 3898982A US 401175 A US401175 A US 401175A US 40117573 A US40117573 A US 40117573A US 3898982 A US3898982 A US 3898982A
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United States
Prior art keywords
tube
blood
reagent
capillary tube
staining
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US401175A
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English (en)
Inventor
Itsurou Katsuda
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jintan Terumo Co Ltd
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Jintan Terumo Co Ltd
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Publication date
Priority claimed from JP47113033A external-priority patent/JPS4858403A/ja
Application filed by Jintan Terumo Co Ltd filed Critical Jintan Terumo Co Ltd
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Publication of US3898982A publication Critical patent/US3898982A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L3/00Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
    • B01L3/56Labware specially adapted for transferring fluids
    • B01L3/561Tubes; Conduits
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B5/00Measuring for diagnostic purposes; Identification of persons
    • A61B5/15Devices for taking samples of blood
    • A61B5/150007Details
    • A61B5/150015Source of blood
    • A61B5/150022Source of blood for capillary blood or interstitial fluid
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B5/00Measuring for diagnostic purposes; Identification of persons
    • A61B5/15Devices for taking samples of blood
    • A61B5/150007Details
    • A61B5/150343Collection vessels for collecting blood samples from the skin surface, e.g. test tubes, cuvettes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61BDIAGNOSIS; SURGERY; IDENTIFICATION
    • A61B5/00Measuring for diagnostic purposes; Identification of persons
    • A61B5/15Devices for taking samples of blood
    • A61B5/150007Details
    • A61B5/150755Blood sample preparation for further analysis, e.g. by separating blood components or by mixing

Definitions

  • ABSTRACT Capillary tubes of the double open-ended type used for blood collection and examination are provided over a portion of their internal surfaces with a dry coating of a reagent, e.g., a colorant for staining blood cells, a phagocytic substance for examining phagocytosis of leucocyte, etc.
  • a reagent e.g., a colorant for staining blood cells, a phagocytic substance for examining phagocytosis of leucocyte, etc.
  • the blood introduction end of the tube is left uncoated to promote capillary action in blood sampling.
  • the coating may include an anticoagulant and several different reagents may be mixed in the coating or coated at intervals longitudinally of the tube.
  • FIG. 1c FIG. 2B g 3 FIG. 20
  • This invention relates to a capillary tube for use in staining cells and bacteria for observation and in a phagocytosis test of blood corpuscles or leucocyte.
  • the staining of a blood smear preparation is effected using generally a May-Giemsa staining method. This method is" important in the diagnosis of blood disease staining method, it is conventional to also stain reticulocytes, mitochondria and intracellar granula.
  • a. general staining b. reticulocyte staining c. Heinz bodies staining d. nuclear bodies staining e. mitchondria staining f; Golgi body staining g. oxidase i h. peroxidasei. PAS staining Astainin'gcapillary tube is designed to simplify these methods and one or all of these methods are intended to be effected within the capillary tube.
  • the general staining includes a May-Giemsa staining; Giemsa staining; Wrightstaining; and a method using a fluorescent dye.
  • the fluorescent dye is subject to an ultraviolet ray to produce a varying color tone dependent upon the kind of cells.
  • Staining dyes used are asjfollowsz a. general staining Wright solution, Giemsa solution, May-Gruenwald solution, acridine orange (fluorescent dye) b. reticulocyte staining new methylene blue, brilliant cresyl blue c. Heinz bodies staining methyl, violet d. nuclear bodies staining brilliant cresyl blue e. mitochondria'fstaining janus green 1+; neutral red pinacyanol+ neutral red Various methods for staining cells such as blood corpuscles etc. have been known.
  • a brilliantcresyl blue pure ethanol solution (dye solution) is dropped onto a glass plate 1 which is carefully cleaned and somewhat warmed, and is spread thin, if possible, for drying. Then, a droplet of blood is dropped at the'center of a cover glass and the cover glass is placed on the glass plate.
  • the resultant sample is sealed by petroleum jelly or fluid paraffin and is allowed to stand for to minutes to obtain a complete sample as shown in FIG. 1C.
  • a dye solution is sucked into a capillary tube to an extent that it reaches about one third of a length of the tube (FIG. 2A). Then, about the same amount of blood is sucked into the tube (FIG. 2B). The resultant solutuion is blow spattered on a slide 4 and intimately mixed (FIG. 2C). Then it is sucked back into the capillary tube (FIG. 2D) andallowed to standfor- 10 minutes (FIG. 2E). The solution is again blow spattered on a slide 5 and intimately mixed (FIG. 2F). A part of the solution is taken out and smeared thin on a spreader slider and air dryed. Thus a larger number of steps than those of the pappenheim method are required.
  • the object of this invention is to provide a capillary tube for staining treatment or phagocytosis test which is capable of effecting a staining treatment or performing phagocytosis test with ease and with rapidity.
  • a capillary tube whose inner wall surface is coated with a dry substance consisting primarily of a dye or a phagocytic foreign matter.
  • FIG. 1 is an explanatory view of a pappenheim method, one of staining methods conventionally practised
  • FIG. 2 is an explanatory view of a Brecker staining method
  • FIG. 3 is a perspective view of a capillary tube according to this invention.
  • FIG. 4 is a cross-sectional view of the capillary tube
  • FIGS. 5 and 6 are explanatory views of the capillary tube.
  • a reference numeral 11 is a transparent glass capillary tube.
  • a dry material including a dye as a primary component is coated to provide a coating layer 12.
  • the dry material differs in its components dependent upon the object to be stained.
  • a fluorescent substance may be used.
  • an observation can be made by exciting the substance by subjection to an ultraviolet ray etc. and when use is made of a blood from a vacuum fluid container containing an anticoagulant, no particular addition of an anti-coagulant is necessary, i.e., only a dye is required.
  • a plurality of dyes may be contained simultaneously.
  • Deposition of the dry material on the inner wall of the capillary tube 11 is effected, for example, in the following way.
  • a solution is prepared by dissolving into a solvent such as water, or suspending in a solvent, a dye, phagocytizing foreign matter and anti-coagulant. Then, one end of the capillary tube is inserted into the solution to permit a proper amount of the solution to be .introduced, under a capillary action, into the interior of the capillary tube. A hot air is blown into that end of the capillary tube from which the solution is introduced and the solution so introduced into the capillary tube is blown out towards the other end of the tube, i.e., an excessive amount of the solution is blown out towards the other end of the tube. The solution deposited on the inner wall of the tube 11 is immediately evaporated to form a coating layer 12. Graduations 13 are marked on the peripheral wall of the capillary tube.
  • a capillary tube 11 When a desired amount of blood is collected, a capillary tube 11 is withdrawn from the wound. Then, the capillary tube is, for example, shaked to cause the dye etc. deposited on the inner wall of the capillary tube 11 to be dissolved into the blood to permit them to be sufficiently mixed as shown in FIG. 5B.
  • a smear preparation is obtained by blow spattering the blood within the capillary tube 11 onto glass plate as shown in FIG. 5C. The smear preparation can be permanently preserved.
  • a vital staining sample is prepared, the same process as shown in FIGS. 5A and 5B is effected. Then, the blood within the capillary tube 11 is dropped onto a cover glass 15 as shown in FIG. 6C and the cover glass is inverted and put on a glass plate 16 as shown in FIG. 6D.
  • the vital staining sample so obtained can not be preserved.
  • a capillary tube whose inner surface is coated with a reagent coating layer, for example, a dry material including as a primary component a colorant or dye or a phagocytizing foreign substance, for example, carbon, starch or polystyrene.
  • a reagent coating layer for example, a dry material including as a primary component a colorant or dye or a phagocytizing foreign substance, for example, carbon, starch or polystyrene.
  • a blood corpuscle when a blood corpuscle is stain-treated, one end of the capillary tube is contacted with the human blood to cause the latter to be naturally sucked into the interior of the capillary tube under capillary action to permit the dye coated on the inner wall of the tube to be dissolved into the blood. That is, the collection of blood and the staining of blood corpuscle or cells can be simultaneously effected. Therefore it is not necessary to adjust a staining fluid, as encountered in the prior art, in an attempt to stain cells. Furthermore, there is saved the trouble of forming a dye film on the slide as in the case of the pappenheim method.
  • a transparent capillary tube it is possible to observe the amount of blood sucked into the capillary tube.
  • the amount of blood can be freely selected if the capillary tube is withdrawn when a predetermined amount of blood is reached. The operation is further facilitated when a graduation is marked on the outer wall of the capillary tube. Since the amount of blood can be freely selected, the mixing ratio between the dye and the blood can be easily adjusted.
  • a dye or phagocytic foreign matter is coated on the whole inner wall surface of the capillary tube.
  • a part of the inner wall of the capillary tube for example one third of a length of the tube, may be free from any reagent coating layer.
  • blood etc. can be quickly sucked into the capillary tube without being obstructed by a coated layer.
  • Two or more reagents may be coated at intervals in a lengthwise direction of the tube in a manner that the layer is divided into sections of individual reagents.
  • the inner wall of one end portion of the tube is coated with a culture medium and the inner wall of the other end' portion of the tube is coated with a dye with an intermediate portion of the tube left uncoated.
  • a lymphocyte suspension is sucked from the culture medium side and cultured for a predetermined time period in a humid room and then mixed with the dye.
  • the capillary tube according to this invention can of course be applied to not only a lympphocyte suspension, or whole blood, but also other blood cells.
  • a tube for blood examination which comprises a double open-ended capillary tube having an inner diameter which allows the introduction of blood by capillary action through the inlet end of the tube, at least one reagent coating layer coated on a portion of the inner wall surface thereof and spaced apart from said inlet end, and an uncoated inner wall area for the introduction of blood, which runs from said inlet end to an edge of the reagent coating layer.
  • the tube for blood examination according to claim two kinds of reagent and each reagent is coated at intervals longitudinally of the tube.
  • a blood examining method comprising the steps of drawing by capillary action a prescribed amount of fluid containing blood cells, from one end portion of a double open ended capillary tube where no reagent is coated to an extent corresponding to the prescribed amount of the fluid to be introduced, into said capillary tube having a portion where at least one blood examination reagent-containing layer is coated on the inner wall surface thereof, shaking the capillary tube to permit the reagent to be dissolved into the fluid, and blowing the fluid from the tube onto a substrate whereby an examination sample is prepared.
  • said layer coating portion of said inner wall surface consists of two separate parts, one part being a culture medium and the other part being a staining material, and said shaking step comprises first mixing the fluid with the culture medium and then mixing the fluid-culture medium mixture with the staining material.

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biomedical Technology (AREA)
  • Heart & Thoracic Surgery (AREA)
  • Hematology (AREA)
  • Physics & Mathematics (AREA)
  • Veterinary Medicine (AREA)
  • Biophysics (AREA)
  • Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Medical Informatics (AREA)
  • Molecular Biology (AREA)
  • Surgery (AREA)
  • Animal Behavior & Ethology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Clinical Laboratory Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Dermatology (AREA)
  • Investigating Or Analysing Biological Materials (AREA)
US401175A 1972-11-13 1973-09-27 Capillary tube for blood examination Expired - Lifetime US3898982A (en)

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Application Number Priority Date Filing Date Title
JP47113033A JPS4858403A (fr) 1971-11-13 1972-11-13

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Cited By (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4027660A (en) * 1976-04-02 1977-06-07 Wardlaw Stephen C Material layer volume determination
US4045175A (en) * 1975-12-10 1977-08-30 Ragnar Weber Micro-method of erythrocyte sedimentation
US4137755A (en) * 1976-09-20 1979-02-06 Wardlaw Stephen C Material layer volume determination
EP0005979A1 (fr) * 1978-05-25 1979-12-12 Dynatech Ag Récipient de réaction miniature et méthode et appareil pour l'introduction d'un microvolume de liquide dans un tel récipient
US4190328A (en) * 1978-12-01 1980-02-26 Levine Robert A Process for detection of blood-borne parasites
US4295857A (en) * 1979-04-06 1981-10-20 Peter Schuler Process for the crystalline precipitation of chromogens
US4308029A (en) * 1976-10-18 1981-12-29 Radiometer A/S Method and capillary tube for treating blood sample
US4314030A (en) * 1979-02-27 1982-02-02 C. A. Greiner & Sohne GmbH Test tube for the examination of urine samples
US4576185A (en) * 1983-12-05 1986-03-18 Terumo Medical Corporation Collection device for capillary blood
USD285115S (en) 1983-12-05 1986-08-12 Terumo Medical Corporation Collector for capillary blood
US4634679A (en) * 1982-11-10 1987-01-06 Becton Dickinson And Company Method of determining adhesion of a liquid sample
US4756884A (en) * 1985-08-05 1988-07-12 Biotrack, Inc. Capillary flow device
DE3833408C1 (en) * 1988-10-01 1990-01-04 Juergen 5223 Nuembrecht De Bethkenhagen Capillary tube
US4949728A (en) * 1988-11-30 1990-08-21 Derek Brook Method for performing in vitro diagnostic test on horses utilizing a blood sample
US4963498A (en) * 1985-08-05 1990-10-16 Biotrack Capillary flow device
US5300779A (en) * 1985-08-05 1994-04-05 Biotrack, Inc. Capillary flow device
US5605838A (en) * 1993-09-17 1997-02-25 Boehringer Mannheim Gmbh Method for the quantitative analysis of sample liquid
EP0826955A3 (fr) * 1993-02-03 1999-03-03 HISTAGGEN Incorporated Procédé de stockage d'un ligand dans un récipient séparable et procédé de libération d'un ligand à partir de celui-ci
US6218193B1 (en) * 1995-09-19 2001-04-17 University Of Washington Precision small volume fluid processing apparatus and method
WO2001073396A1 (fr) * 2000-03-28 2001-10-04 Caliper Technologies, Corp. Procedes permettant de reduire un report fluidique dans des dispositifs microfluidiques
US6555386B1 (en) * 1999-07-23 2003-04-29 Clinical Diagnostic Chemicals Limited Apparatus for collecting a liquid sample
US20040156746A1 (en) * 2001-05-10 2004-08-12 Larsen Ulrik Darling Device for sampling small and precise volumes of liquid
US20050287674A1 (en) * 2000-08-24 2005-12-29 Bio-Rad Laboratories, Inc Labeling proteins with dyes that are insoluble or only sparingly soluble in water
EP1055112B1 (fr) * 1998-01-14 2008-02-20 Hemocue AB Procede de melange
US11278225B2 (en) * 2015-08-12 2022-03-22 University Of Tasmania Liquid collection device
WO2023056103A1 (fr) * 2021-10-01 2023-04-06 Essenlix Corporation Préparation d'essai d'échantillon pour uniformité de réactif, en particulier de sang

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2487077A (en) * 1943-12-28 1949-11-08 Us Commerce Colorimetric gas detection
US2940448A (en) * 1957-04-29 1960-06-14 Jr Norman B Furlong Disposable blood-gas analyzer
US3146163A (en) * 1962-01-23 1964-08-25 John H Brewer Apparatus for separating certain components from blood
US3518804A (en) * 1966-10-27 1970-07-07 Horace W Gerarde Pipette assembly having precise quantity stabilized reagent in liquid form and method of preparing same
US3579303A (en) * 1968-03-06 1971-05-18 Donald E Pickering System for handling specimens and other substances in medicine and physical sciences
US3620676A (en) * 1969-02-20 1971-11-16 Sterilizer Control Royalties A Disposable colorimetric indicator and sampling device for liquids
US3732079A (en) * 1969-02-20 1973-05-08 Sterilizer Control Royalties Disposable plastic syringe for use in colorimetry
US3768978A (en) * 1971-03-01 1973-10-30 Hamilton Co Disposable pipette

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2487077A (en) * 1943-12-28 1949-11-08 Us Commerce Colorimetric gas detection
US2940448A (en) * 1957-04-29 1960-06-14 Jr Norman B Furlong Disposable blood-gas analyzer
US3146163A (en) * 1962-01-23 1964-08-25 John H Brewer Apparatus for separating certain components from blood
US3518804A (en) * 1966-10-27 1970-07-07 Horace W Gerarde Pipette assembly having precise quantity stabilized reagent in liquid form and method of preparing same
US3579303A (en) * 1968-03-06 1971-05-18 Donald E Pickering System for handling specimens and other substances in medicine and physical sciences
US3620676A (en) * 1969-02-20 1971-11-16 Sterilizer Control Royalties A Disposable colorimetric indicator and sampling device for liquids
US3732079A (en) * 1969-02-20 1973-05-08 Sterilizer Control Royalties Disposable plastic syringe for use in colorimetry
US3768978A (en) * 1971-03-01 1973-10-30 Hamilton Co Disposable pipette

Cited By (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4045175A (en) * 1975-12-10 1977-08-30 Ragnar Weber Micro-method of erythrocyte sedimentation
US4027660A (en) * 1976-04-02 1977-06-07 Wardlaw Stephen C Material layer volume determination
US4077396A (en) * 1976-04-02 1978-03-07 Wardlaw Stephen C Material layer volume determination
US4137755A (en) * 1976-09-20 1979-02-06 Wardlaw Stephen C Material layer volume determination
US4308029A (en) * 1976-10-18 1981-12-29 Radiometer A/S Method and capillary tube for treating blood sample
EP0005979A1 (fr) * 1978-05-25 1979-12-12 Dynatech Ag Récipient de réaction miniature et méthode et appareil pour l'introduction d'un microvolume de liquide dans un tel récipient
US4190328A (en) * 1978-12-01 1980-02-26 Levine Robert A Process for detection of blood-borne parasites
US4314030A (en) * 1979-02-27 1982-02-02 C. A. Greiner & Sohne GmbH Test tube for the examination of urine samples
US4295857A (en) * 1979-04-06 1981-10-20 Peter Schuler Process for the crystalline precipitation of chromogens
US4634679A (en) * 1982-11-10 1987-01-06 Becton Dickinson And Company Method of determining adhesion of a liquid sample
US4576185A (en) * 1983-12-05 1986-03-18 Terumo Medical Corporation Collection device for capillary blood
USD285115S (en) 1983-12-05 1986-08-12 Terumo Medical Corporation Collector for capillary blood
AU593001B2 (en) * 1985-08-05 1990-02-01 Biotrack, Inc. Capillary flow device
US4756884A (en) * 1985-08-05 1988-07-12 Biotrack, Inc. Capillary flow device
US4963498A (en) * 1985-08-05 1990-10-16 Biotrack Capillary flow device
US5300779A (en) * 1985-08-05 1994-04-05 Biotrack, Inc. Capillary flow device
DE3833408C1 (en) * 1988-10-01 1990-01-04 Juergen 5223 Nuembrecht De Bethkenhagen Capillary tube
US4949728A (en) * 1988-11-30 1990-08-21 Derek Brook Method for performing in vitro diagnostic test on horses utilizing a blood sample
EP0826955A3 (fr) * 1993-02-03 1999-03-03 HISTAGGEN Incorporated Procédé de stockage d'un ligand dans un récipient séparable et procédé de libération d'un ligand à partir de celui-ci
US5605838A (en) * 1993-09-17 1997-02-25 Boehringer Mannheim Gmbh Method for the quantitative analysis of sample liquid
US6218193B1 (en) * 1995-09-19 2001-04-17 University Of Washington Precision small volume fluid processing apparatus and method
EP1055112B1 (fr) * 1998-01-14 2008-02-20 Hemocue AB Procede de melange
JP2009053201A (ja) * 1998-01-14 2009-03-12 Hemocue Ab 混合方法
US6555386B1 (en) * 1999-07-23 2003-04-29 Clinical Diagnostic Chemicals Limited Apparatus for collecting a liquid sample
WO2001073396A1 (fr) * 2000-03-28 2001-10-04 Caliper Technologies, Corp. Procedes permettant de reduire un report fluidique dans des dispositifs microfluidiques
US20050287674A1 (en) * 2000-08-24 2005-12-29 Bio-Rad Laboratories, Inc Labeling proteins with dyes that are insoluble or only sparingly soluble in water
US20040156746A1 (en) * 2001-05-10 2004-08-12 Larsen Ulrik Darling Device for sampling small and precise volumes of liquid
US11278225B2 (en) * 2015-08-12 2022-03-22 University Of Tasmania Liquid collection device
US12588845B2 (en) 2015-08-12 2026-03-31 University Of Tasmania Liquid collection device
WO2023056103A1 (fr) * 2021-10-01 2023-04-06 Essenlix Corporation Préparation d'essai d'échantillon pour uniformité de réactif, en particulier de sang

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Publication number Publication date
BE805489A (fr) 1974-01-16
AU6090573A (en) 1975-04-10

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