WO1999044806A1 - Filiere d'extrusion pour materiau biodegradable a dispositif modificateur de l'orifice de la filiere et dispositif regulateur de debit - Google Patents

Filiere d'extrusion pour materiau biodegradable a dispositif modificateur de l'orifice de la filiere et dispositif regulateur de debit Download PDF

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Publication number
WO1999044806A1
WO1999044806A1 PCT/US1999/004774 US9904774W WO9944806A1 WO 1999044806 A1 WO1999044806 A1 WO 1999044806A1 US 9904774 W US9904774 W US 9904774W WO 9944806 A1 WO9944806 A1 WO 9944806A1
Authority
WO
WIPO (PCT)
Prior art keywords
mandrel
extrusion
biodegradable material
extrusion die
orifice
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US1999/004774
Other languages
English (en)
Inventor
Hans G. Franke
Don R. Bittner
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Standard Starch LLC
Original Assignee
Standard Starch LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US09/035,200 external-priority patent/US6183672B1/en
Priority claimed from US09/035,560 external-priority patent/US6103151A/en
Application filed by Standard Starch LLC filed Critical Standard Starch LLC
Priority to CA002323157A priority Critical patent/CA2323157C/fr
Priority to EP99912276A priority patent/EP1069982A1/fr
Priority to AU30687/99A priority patent/AU3068799A/en
Priority to JP2000534387A priority patent/JP2002514522A/ja
Publication of WO1999044806A1 publication Critical patent/WO1999044806A1/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/25—Component parts, details or accessories; Auxiliary operations
    • B29C48/30—Extrusion nozzles or dies
    • B29C48/32—Extrusion nozzles or dies with annular openings, e.g. for forming tubular articles
    • B29C48/33—Extrusion nozzles or dies with annular openings, e.g. for forming tubular articles with parts rotatable relative to each other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
    • B29C48/07—Flat, e.g. panels
    • B29C48/08—Flat, e.g. panels flexible, e.g. films
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
    • B29C48/09—Articles with cross-sections having partially or fully enclosed cavities, e.g. pipes or channels
    • B29C48/10—Articles with cross-sections having partially or fully enclosed cavities, e.g. pipes or channels flexible, e.g. blown foils
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29K—INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2003/00—Use of starch or derivatives as moulding material

Definitions

  • This invention relates generally to the formation of shaped objects from expanded biodegradable materials, and. in particular, to an extrusion die for ultimately forming sheets of biodegradable material.
  • Biodegradable materials are presently in high demand for applications in packaging materials. Commonly used polystyrene (“Styrofoam” (Trademark)), polypropylene, polyethylene, and other non-biodegradable plastic-containing packaging materials are considered detrimental to the environment and may present health hazards. The use of such non- biodegradable materials will decrease as government restrictions discourage their use in packaging applications. Indeed, in some countries in the world, the use of styrofoam (trademark) is already extremely limited by legislation. Biodegradable materials that are flexible, pliable and non-brittle are needed in a variety of packaging applications, particularly for the manufacture of shaped biodegradable containers for food packaging. For such applications, the biodegradable material must have mechanical properties that allow it to be formed into and hold the desired container shape, and be resistant to collapsing, tearing or breaking.
  • Starch is an abundant, inexpensive biodegradable polymer.
  • a variety of biodegradable based materials have been proposed for use in packaging applications. Conventional extrusion of these materials produces expanded products that are brittle, sensitive to water and unsuitable for preparation of packaging materials.
  • Attempts to prepare biodegradable products with flexibility, pliability, resiliency, or other mechanical properties acceptable for various biodegradable packaging applications have generally focused on chemical or physio-chemical modification of starch, the use of expensive high amylose starch or mixing starch with synthetic polymers to achieve the desired properties while retaining a degree of biodegradability.
  • a number of references relate to extrusion and to injection molding of starch-containing compositions.
  • U.S. Patent No. 5,397.834 provides biodegradable, thermoplastic compositions made of the reaction product of a starch aldehyde with protein. According to the disclosure, the resulting products formed with the compositions possess a smooth, shiny texture, and a high level of tensile strength, elongation, and water resistance compared to articles made from native starch and protein.
  • Suitable starches which may be modified and used according to the invention include those derived, for example, from corn including maize, waxy maize and high amylose corn; wheat including hard wheat, soft wheat and durum wheat; rice including waxy rice; and potato, rye, oat, barley, sorghum, millet, triticale, amaranth, and the like.
  • the starch may be a normal starch (about 20-30 wt-% amylose), a waxy starch (about 0-8 wt-% amylose), or a high- amylose starch (greater than about 50 wt-% amylose).
  • U.S. Patent Nos. 4,133,784, 4,337,181, 4,454,268, 5,322,866, 5,362,778, and 5,384,170 relate to starch-based films that are made by extrusion of destructurized or gelatinized starch combined with synthetic polymeric materials.
  • U.S. Patent No. 5,322,866 specifically concerns a method of manufacture of biodegradable starch-containing blown films that includes a step of extrusion of a mixture of raw unprocessed starch, copolymers including polyvinyl alcohol, a nucleating agent and a plasticizer. The process is said to eliminate the need of pre-processing the starch.
  • U.S. Patent No. 5,409,973 reports biodegradable compositions made by extrusion from destructurized starch and an ethylene-vinyl acetate copolymer.
  • U.S. Patent No. 5,087,650 relates to injection-molding of mixtures of graft polymers and starch to produce partially biodegradable products with acceptable elasticity and water stability.
  • U.S. Patent No. 5,258,430 relates to the production of biodegradable articles from destructurized starch and chemically-modified polymers, including chemically-modified polyvinyl alcohol.
  • the articles are said to have improved biodegradability, but retain the mechanical properties of articles made from the polymer alone.
  • U.S. Patent No. 5,292,782 relates to extruded or molded biodegradable articles prepared from mixtures of starch, a thermoplastic polymer and certain plasticizers.
  • U.S. Patent No. 5,095,054 concerns methods of manufacturing shaped articles from a mixture of destructurized starch and a polymer.
  • U.S. Patent No. 4,125,495 relates to a process for manufacture of meat trays from biodegradable starch compositions.
  • Starch granules are chemically modified, for example with a silicone reagent, blended with polymer or copolymer and shaped to form a biodegradable shallow tray.
  • U.S. Patent No. 4,673,438 relates to extrusion and injection molding of starch for the manufacture of capsules.
  • U.S. Patent No. 5,427,614 also relates to a method of injection molding in which a non- modified starch is combined with a lubricant, texturing agent and a melt-flow accelerator.
  • EP published application No. 712883 (published May 22, 1996) relates to biodegradable, structured shaped products with good flexibility made by extruding starch having a defined large particle size (e.g., 400 to 1500 microns).
  • the application exemplifies the use of high amylose starch and chemically-modified high amylose starch.
  • U.S. Patent No. 5,512,090 refers to an extrusion process for the manufacture of resilient, low density biodegradable packaging materials, including loose-fill materials, by extrusion of starch mixtures comprising polyvinyl alcohol (PVA) and other ingredients.
  • PVA polyvinyl alcohol
  • the patent refers to a minimum amount of about 5% by weight of PVA.
  • U.S. Patent No. 5,186,990 reports a lightweight biodegradable packaging material produced by extrusion of corn grit mixed with a binding agent (guar gum) and water. Corn grit is said to contain among other components starch (76-80%), water (12.5-14%), protein (6.5-8%) and fat (0.5-1%).
  • the patent teaches the use of generally known food extruders of a screw-type that force product through an orifice or extension opening. As the mixture exits the extruder via the flow plate or die, the super heated moisture in the mixture vaporizes forcing the material to expand to its final shape and density.
  • U.S. Patent No. 5,208,267 reports biodegradable, compressible and resilient starch- based packaging fillers with high volumes and low weights.
  • the products are formed by extrusion of a blend of non-modified starch with polyalkylene glycol or certain derivatives thereof and a bubble-nucleating agent, such as silicon dioxide.
  • U.S. Patent No. 5,252,271 reports a biodegradable closed cell light weight loose-fill packaging material formed by extrusion of a modified starch.
  • Non-modified starch is reacted in an extruder with certain mild acids in the presence of water and a carbonate compound to generate CO .
  • Resiliency of the product is said to be 60% to 85%, with density less than 0.032 g/cm 3 .
  • U.S. Patent No. 3,137,592 relates to gelatinized starch products useful for coating applications produced by intense mechanical working of starch/plasticizer mixtures in an extruder.
  • Related coating mixtures are reported in U.S. Patent No. 5,032,337 which are manufactured by the extrusion of a mixture of starch and polyvinyl alcohol.
  • Application of thermomechanical treatment in an extruder is said to modify the solubility properties of the resultant mixture which can then be used as a binding agent for coating paper.
  • Biodegradable material research has largely focused on particular compositions in an attempt to achieve products that are flexible, pliable and non-brittle. The processes used to produce products from these compositions have in some instances, used extruders.
  • U.S. Patent Number 5,660,900 discloses several extruder apparatuses for processing inorganically filled, starch-bound compositions. The extruder is used to prepare a moldable mixture which is then formed into a desired configuration by heated molds.
  • U. S. Patent Number 3,734,672 discloses an extrusion die for extruding a cup shaped shell made from a dough.
  • the die comprises an outer base having an extrusion orifice or slot which has a substantial horizontal section and two upwardly extending sections which are slanted from the vertical.
  • a plurality of passage ways extend from the rear of the die to the slot in the face of the die. The passage way channels dough from the extruder through the extrusion orifice or slot.
  • biodegradable material was extruded as a flat sheet through a horizontal slit or linear extrusion orifice.
  • the flat sheet of biodegradable material was then pressed between molds to form the clam shell, tray or other food package.
  • these die configurations produced flat sheets of biodegradable material which were not uniformly thick, flexible, pliable and non-brittle.
  • the packaging products molded from the flat sheets also had these negative characteristics.
  • the biodegradable material typically had greater structural stability in a direction parallel to the extrusion flow direction compared to a direction transverse to the extrusion flow direction.
  • fracture planes or lines along which the sheet of biodegradable material was easily broken tended to form in the biodegradable sheet as it exited from the extrusion orifice.
  • Food packages which were molded from the extruded sheet also tended to break or fracture along these planes. Therefore, there is a need for a process which produces a flexible, pliable and non-brittle biodegradable material which has structural stability in both the longitudinal and transverse directions
  • a extrusion die through which biodegradable material can be extruded which has structural stability in both the longitudinal and transverse directions of the material, which has a flow control device which controls flow of biodegradable material through the extrusion die, and which allows the inner
  • the die extrudes a tubular shaped structure which has its greatest structural stability in a direction which winds helically around the tubular structure.
  • the direction of greatest stability twists in one direction while at the bottom the direction of greatest stability twists in the opposite direction.
  • This tubular structure is then pressed into a sheet comprised of two layers having their directions of greater stability approximately normal to each other.
  • This 2-ply sheet is a flexible, pliable and non-brittle sheet with strength in all directions.
  • the flow rate of the biodegradable material is regulated at a location upstream from the orifice and at the orifice itself to provide complete control of extrusion parameters.
  • an annular extrusion die allows the inner and outer walls of the extrusion orifice to be adjusted relative to each other to modify the circumferencial wall thickness of the cylindrical extrudate.
  • an extrusion die for extruding biodegradable material, the extrusion die comprising: a mandrel; an outer member positioned near the mandrel; an extrusion orifice between the mandrel and the outer member; a member in communication with at least one defining member of the extrusion orifice, wherein the member is capable of producing relative movement between the outer member and the mandrel, wherein the relative movement has a component transverse to an extrusion direction of biodegradable material through the extrusion orifice; a flow control device which controls flow of biodegradable material through the extrusion die; and a positioning device which positions the outer member and the mandrel relative to each other.
  • an extrusion die for extruding biodegradable material, the extrusion die comprising: a cylindrical mandrel; a cylindrical outer ring positioned around the mandrel; an annular extrusion orifice between the mandrel and the outer ring; a member in communication with at least one defining member of the annular extrusion orifice which produces angular relative movement between the outer ring and the mandrel; a flow control device which controls flow of biodegradable material through the extrusion die, wherein the flow control device comprises a mechanism which translates the
  • an extrusion die for extruding biodegradable material, the extrusion die comprising: a mandrel; an outer member positioned near the mandrel; an extrusion orifice between the mandrel and the outer member; a mounting plate having a flow bore which conducts biodegradable material toward the extrusion orifice, wherein the mandrel is fixedly mounted to the mounting plate and the outer member is movably mounted to the mounting plate; a shearing member which moves the outer member relative to the mandrel in a direction having a component transverse to an extrusion direction of biodegradable material through the extrusion orifice; a flow control device which controls flow of biodegradable material through the extrusion die, wherein the flow control device comprises a flow control channel upstream of the extrusion orifice, wherein the flow control channel throttles flow of the biodegradable material through the die, wherein the mandrel is attached to the mounting plate
  • an improved process for the extrusion of biodegradable material wherein the extrusion comprises flowing the biodegradable material in a flow direction through an orifice, the improvement comprising: moving or shearing the biodegradable material, in a direction having a component transverse to the flow direction, during extrusion; controlling the flow rate of biodegradable material through the extrusion die during extrusion, wherein the controlling comprises adjusting the head pressure of the biodegradable material in the extrusion die and adjusting at least one cross- sectional area of a biodegradable material flow path within the extrusion die; and modifying the orifice geometry.
  • a process for manufacturing biodegradable shaped products of increased strength comprising: extruding a biodegradable material, wherein the extruding comprises moving the biodegradable material in a first direction through an orifice to produce an extrudate; modifying the orifice geometry; shearing the biodegradable material, in a second direction having a component transverse to the first direction, during the extruding; controlling the flow rate of biodegradable
  • controlling comprises adjusting the cross-sectional area of an extrusion orifice and wherein the controlling further comprises adjusting the cross-sectional area of a biodegradable material flow path at a location upstream of the extrusion orifice; compressing the extrudate; and molding the compressed extrudate of biodegradable material into a structure.
  • Figure 1 is a cross-sectional view of a rotating die embodiment of the invention fully assembled.
  • Figure 2 is a cross-sectional view of a rotating embodiment of the die fully assembled with orifice modifying and flow control devices.
  • Figure 3 is an exploded perspective view of the several parts which comprise the die shown in Figure 2.
  • Figure 4 is a cross-sectional exploded view of a mandrel, mounting plate and spacers.
  • Figure 5 is a cross-sectional exploded view of a gap adjusting ring, a bearing housing and an end cap.
  • Figure 6 is an exploded cross-sectional view of a seal ring, an outer ring and a die wheel.
  • Figure 7A is a cross-sectional side view of an embodiment of the invention having a motor and belt for rotating an outer ring about a mandrel.
  • Figure 7B is an end view of the embodiment of the invention as shown in Figure 7A.
  • Figure 8 is a side view of a system for producing molded objects from biodegradable material, the system comprising an extruder, a rotating extrusion die, a cylindrical extrudate, rollers, and molding devices.
  • Figure 9 is a flow chart of a process embodiment of the invention.
  • Figure 10A is a perspective view of a cylindrical extrudate of biodegradable material having helical extrusion lines.
  • Figure 1 OB is a perspective view of a sheet of biodegradable material produced from the extrudate shown in Figure 10A.
  • Figure 11 is an end view of an embodiment of the invention for rotating the die wheel of the rotating die, the device having a rack gear.
  • Figure 12A is a perspective view of a cylindrical extrudate having sinusoidal extrusion lines.
  • Figure 12B is a top view of a sheet of biodegradable material produced from the extrudate shown in Figure 12 A.
  • Figure 13 is an end view of a device for rotating the die wheel of an embodiment of the invention wherein the system comprises a worm gear.
  • Figure 14A is a perspective view of an extrudate of biodegradable material wherein the extrudate is cylindrical in shape and has zigzag extrusion lines.
  • Figure 14B is a top view of a sheet of biodegradable material produced from the extrudate shown in Figure 14A.
  • Figure 15 is a cross-sectional view of a flow control embodiment of the die fully assembled.
  • Figure 16 is a cross-sectional view of an orifice modifying embodiment of the die fully assembled.
  • the die 1 is made up of several discrete annular members which share the same longitudinal central axis 3.
  • a mounting plate 20 is located in the center of the die 1 and is the member to which most of the remaining parts are attached.
  • an extruder adapter 10 is attached for connecting the die 1 to an extruder (not shown).
  • a backplate 11 is attached between the extruder adapter 30 and the mounting plate 20.
  • several spacers 100 are positioned in counter sunk holes in the mounting plate 20 at various locations equidistant from the longitudinal central axis 3.
  • a mandrel 30 has counter sunk holes which correspond to those in the mounting plate 20.
  • the mandrel 30 is fixed to the mounting plate 20 with the spacers 100 between, the spacers being inserted into the respective counter sunk holes.
  • a seal ring 40 is inserted into an annular spin channel 22 of the mounting plate 20.
  • the mounting plate 20 has a bearing portion 71 which extends around the seal ring 40.
  • An end cap 80 is attached to the distal end of the bearing portion 71 of the mounting plate 20 to lock the seal ring 40 in the spin channel 22.
  • An outer ring 50 is attached to the seal ring 40 around the outside of the mandrel 30 to form an extrusion orifice 5 between the outer ring 50 and the mandrel 30.
  • a die wheel 90 is attached to the outer ring 50. As described more fully below, a motor and drive system drive the die wheel 90 to rotate the outer ring 50 about the mandrel 30.
  • Biodegradable material is pushed through the die 1 under pressure by an extruder (not shown) which is attached to the extruder adapter 10.
  • the biodegradable material passes through flow bore 23 which conducts the material through the extruder adapter 10 and the mounting plate 20 to a central location at the backside of the mandrel 30.
  • the biodegradable material is then forced radially outward through a disc-shaped cavity called a flow control channel 4 which is defined by the mounting plate 20 and the mandrel 30.
  • the biodegradable material is pushed through the extrusion orifice 5 defined by the mandrel 30 and the outer ring 50.
  • the biodegradable material is forced through the extrusion orifice 5, the die wheel 90, outer ring 50 and seal ring 40 are rotated relative to the stationary mounting plate 20 and mandrel 30.
  • the die 1 is made up of several discrete annular members which share the same longitudinal central axis
  • Amounting plate 20 is located in the center of the die 1 and is the member to which most of the remaining parts are attached. At one end of the mounting plate 20, an extruder adapter is attached for connecting the die 1 to an extruder (not shown).
  • a gap adjusting ring 60 is placed concentrically around the cylindrical exterior of the mounting plate 20.
  • a bearing housing 70 lies adjacent the gap adjusting ring 60 and the mounting plate 20.
  • a seal ring 40 is placed within the bearing housing 70 and is inserted into an annular spin channel of the mounting plate 20.
  • several spacers 100 are positioned in counter sunk holes in the mounting plate 20 at various locations equidistant from the longitudinal central axis 3.
  • a mandrel 30 has counter sunk holes which correspond to those in the mounting plate 20.
  • the mandrel is fixed to the mounting plate 20 with the spacers 100 between.
  • An outer ring 50 is attached to the seal ring 40 around the outside of the mandrel 30 to form an extrusion orifice 5 between the outer ring 50 and the mandrel 30.
  • a die wheel 90 is attached to the outer ring 50 for rotating the outer ring 50 about the mandrel 30.
  • the mounting plate 20 is basically a solid cylinder with a cylindrical flow bore 23 cut in the middle along the longitudinal central axis 3.
  • One end of the mounting plate 20 comprises a mounting shoulder 21 for engagement with the extruder adapter 10 (shown in Figs. 2 and 3).
  • the mounting plate 20 has a annular spin channel 22 for receiving the seal ring 40 (shown in Figs. 2 and 3).
  • the mounting plate 20 has a discshaped flow surface 25.
  • the mounting plate 20 also has several mounting plate counter sunk holes 24 for receiving spacers 100 such that the counter sunk holes 24 are drilled in the flow surface 25.
  • FIG 4 only two counter sunk holes 24 are shown because the view is a cross section along a plane which intersects the longitudinal central axis 3. All of the mounting plate counter sunk holes 24 are equidistant from each other and from the longitudinal central axis 3.
  • the mandrel 30 is a bowl shaped structure having a base 31 and sides 32. As shown in Figure 4, the mandrel 30 is oriented sideways so that the central axis of the mandrel is collinear with the longitudinal central axis 3 of the die. Unlike the mandrel 20, which has a flow bore 23 through the center, the mandrel 30 has a solid base 31. The outside surface of the base 31 is a base flow surface 33. The mandrel 30 has several countersunk holes 34 which are cut in the base flow surface 33. In Figure 4, only two mandrel countersunk holes 34 are shown because the view is a cross-section along a plane which intersects the longitudinal central axis 3. All of the mandrel countersunk holes 34 are equidistant from each other and from the central axis 3. The inside of the mandrel 30 is hollowed out to reduce its overall weight.
  • Spacers 100 are used to mount the mandrel 30 to the mounting plate 20.
  • Each of the spacers 100 comprise male ends 102 for insertion into mounting plate and mandrel countersunk holes 24 and 34.
  • the outside diameter of the male ends 102 is slightly smaller than the inside diameters of mounting plate and mandrel countersunk holes 24 and 34.
  • each of the spacers 100 comprise a rib 101 which has an outside diameter larger than the inside diameters of the mounting plate and mandrel countersunk holes 24 and 34.
  • the rib 101 of each spacer 100 has a uniform thickness in the longitudinal direction to serve as the spacer mechanism between the assembled mounting plate and mandrel.
  • the mandrel 30 is attached to the mounting plate 20 with mandrel bolts 36.
  • the mandrel bolts 36 extend through the base 31 of the mandrel 30, through the spacers 100 and into treaded portions in the bottom of the mounting plate counter sunk holes 24. While the heads of
  • the mandrel bolts 36 could be made to rest firmly against the inside of the base 31 of the mandrel, in the embodiment shown, the mandrel bolts extend through risers 35 so that the heads of the mandrel bolts 36 are more accessible from the open end of the mandrel 30.
  • one end of each of the risers 35 rests securely against the inside of the mandrel base 31 while the other end of each riser is engaged by the head of a mandrel bolt 36.
  • the gap adjusting ring 60 is a ring shaped member having a longitudinal central axis 3 and an inner diameter slightly greater than the outside diameter of the mounting plate 20 (shown in Figs. 2 and 3).
  • the gap adjusting ring 60 also has several lock screws 61 which extend through an inner portion 62 of the gap adjusting ring 60 for engagement with the mounting plate 20 once the gap adjusting ring 60 is placed around the outside of the mounting plate 20.
  • the gap adjusting ring 60 has an outer portion 63 for engagement with the bearing housing 70.
  • the gap adjusting ring 60 has shifting lugs 64 which are attached via lug bolts 65.
  • four shifting lugs 64 are attached to the outer portion 63 of the gap adjusting ring 60.
  • the shifting lugs 64 are spaced around the gap adjusting ring 60 so that one is at the top, bottom, and sides, respectively.
  • the shifting lugs 64 extend from the outer portion 63 in a longitudinal direction for positioning engagement with the bearing housing 70.
  • the shifting bolts 66 poke through the shifting lugs 64 in the part of the shifting lugs 64 which extend from the outer portion 63 in the longitudinal direction.
  • the shifting bolts 66 poke through in a direction from outside the die toward the longitudinal central axis 3.
  • the gap adjusting ring 60 has threaded holes 67 at various locations around the outer portion 63 for receiving screws 74.
  • the bearing housing 70 is an annular ring which has a longitudinal central axis 3.
  • the bearing housing 70 has a bearing portion 71 and a support portion 72.
  • the support portion 72 is annular with is greatest cross-section in a direction transverse to the longitudinal central axis 3.
  • the bearing housing 70 is attachable to the gap adjusting ring 60 by the support portion 72 which engages the outer portion 63 of the gap adjusting ring 60. In the embodiment shown, this engagement between the bearing housing 70 and the gap adjusting ring 60 is accomplished by screws 74 between these two members.
  • the support portion 72 has several slip holes 75 which protrude through the support portion 72 in a longitudinal direction. In one embodiment, twelve slip holes 75 are positioned equidistant from each other around the support portion 72 and are positioned equidistant from the longitudinal central axis 3. The inside diameter of each slip
  • 11 hole 75 is larger than the outside diameter of screws 74 so that there is substantial "play” between the screws 74 and the slip holes 75. While the slip holes 75 are larger than the screws 74, the slip holes 75 are small enough so that the heads of the screws 74 securely engage the support portion 72 of the bearing housing 70.
  • the other major part of the bearing housing 70 is the bearing portion 71 which is an annular section having its greatest thickness in the longitudinal direction.
  • the interior surface of the bearing portion 71 is a bearing surface 76 for engaging lateral support bearings 42 (shown in Fig. 6).
  • the bearing surface 76 supports the lateral support bearings 42 in a plane normal to the longitudinal central axis 3.
  • the bearing housing 70 Protruding from the bearing surface 76 near the support portion 72, the bearing housing 70 has a bearing housing lateral support flange 73 which supports a lateral support bearing 42 of the seal ring 40 (shown in Fig. 6).
  • the relative positions of the two devices may be adjusted.
  • the shifting bolts 66 of the gap adjusting ring 60 are relaxed to provide enough space for the support portion 72 of the bearing housing 70.
  • the bearing housing 70 is then placed directly adjacent the gap adjusting ring 60 with the support portion 72 within the extended portions of shifting lugs 64.
  • the screws 74 are then inserted through the slip holes 75 and loosely screwed into threaded holes 67 in the gap adjusting ring 60.
  • the shifting bolts 66 are then adjusted to collapse on the support portion 72 of the bearing housing 70.
  • the shifting bolts 66 may be adjusted to push the bearing housing 70 off center relative to the gap adjusting ring 60.
  • the shifting bolts 66 freely push the bearing housing 70 in one direction or the other.
  • the bearing housing 70, seal ring 40 and outer ring 50 may be perturbed from their original positions to more desirable positions.
  • the end cap 80 is preferably a ring which has a longitudinal central axis 3.
  • the interior portion of the end cap 80 is a stabilizer 81 and the exterior is a fastener flange 82.
  • Fastener holes 83 are drilled in the fastener flange 82 for inserting fasteners which secure the end cap 80 to the bearing portion 71 of the bearing housing 70.
  • the outside diameter of the stabilizer 81 of the end cap 80 is slightly smaller than the inside diameter of the bearing portion 71 of the bearing housing 70. This allows the stabilizer 81 to be inserted into the bearing portion 71.
  • At the distal end of the stabilizer 81 there is an end cap lateral support flange 84 which supports a
  • FIG. 6 a cross-sectional view of the seal ring 40, the outer ring 50 and the die wheel 90 are shown disassembled.
  • the seal ring 40 is a cylindrical member having a longitudinal central axis 3.
  • the seal ring 40 has an interior diameter which decreases from one end to the other. At the end of the seal ring 40 which has the smallest inside diameter, the seal ring 40 has a notch 47 for engaging the outer ring 50 as discussed below.
  • the seal ring 40 On the outside of the seal ring 40, there are four superior piston rings 41 for engaging the mounting plate 20 and the end cap 80 (both shown in Figs. 2 and 3).
  • the seal ring 40 also comprises two lateral support bearings 42.
  • the lateral support bearings 42 are separated by a bearing spacer flange 43 which is positioned between the two lateral support bearings 42.
  • the seal ring 40 further comprises two retaining rings 44 which are positioned on the outsides of the lateral support bearings 42.
  • retaining rings 44 are slipped over each end of the seal ring 40 until they snap into grooves 45 at the outsides of the lateral support bearings 42.
  • the lateral support bearings 42 are secured between the bearing spacer flange 43 and the retaining rings 44.
  • the superior piston rings 41 are placed in piston slots 46.
  • the outer ring 50 is a cylindrical member having a longitudinal central axis 3.
  • the outer ring 50 has a ring portion 51 and a fastener flange 52. Longitudinal holes are cut through the fastener flange 52 for inserting fasteners which secure the outer ring 50 to an end of the seal ring 40.
  • the outside diameter of the ring portion 51 is slightly smaller than the inside diameter of the notch 47 of the seal ring 40. This allows the outer ring 50 to be assembled to the seal ring
  • the die wheel 90 is a cylindrical member with a wheel flange 92 and a drive section 93.
  • the drive section 93 is a device which
  • the drive section is a pulley for engaging a drive belt.
  • the extruder adapter 10 is secured to the mounting plate 20 with a back plate 11 between.
  • several spacers 100 are placed in the mandrel 30 by inserting a male end 102 of each spacer 100 into a mandrel counter sunk hole 34, until all the mandrel counter sunk holes 34 have a spacer 100.
  • the mandrel 30 is then placed adjacent the mounting plate 20 with the protruding male ends 102 of the spacers 100 being inserted into the mounting plate counter sunk holes 24.
  • the mandrel 30 is then attached to the mounting plate 20 with spacers 100 between the mandrel bolts 36.
  • the risers 35 are slipped over the shanks of the mandrel bolts 36 and the mandrel bolts 36 are inserted through the mandrel base 31, the mandrel counter sunk holes 34, the spacers 100, and the mounting plate counter sunk holes 24.
  • the bottoms of the mounting plate counter sunk holes 24 are threaded so that the mandrel bolts 36 may be screwed into the mounting plate 20.
  • the mandrel bolts 36 are then screwed into the threaded bottoms of each mounting plate counter sunk hole 24 to fasten the mandrel 30 to the mounting plate 20.
  • the gap adjusting ring 60 is slipped over the exterior of the mounting plate 20.
  • the lock screws 61 are then tightened against the exterior of the mounting plate 20.
  • the bearing housing 70 is then positioned with the support portion 72 against the outer portion 63 of the gap adjusting ring 60.
  • the shifting bolts 66 are adjusted to center the bearing housing 70 about the longitudinal central axis 3 and the screws inserted through slip holes 75 and tightened into the threaded holes 67 of the gap adjusting ring 60.
  • the seal ring 40 having superior piston rings 41, lateral support bearings 42 and retaining rings 44 attached thereto, is rotatably attached to the bearing housing 70.
  • the seal ring 40 is inserted into the bearing housing 70 and then into the spin channel 22 of the mounting plate 20.
  • the seal ring 40 is pushed all the way into the spin channel 22 of the mounting plate 20 until the first of the lateral support bearings 42 rests firmly against the bearing housing lateral support flange 73. In this position, two of the four superior piston rings 41 form a seal between the seal ring 40 and the spin channel 22 of the mounting plate 20.
  • the seal ring 40 is held in this position by inserting the stabilizer 81 of the end cap 80 into the bearing portion 71 of the bearing housing 70.
  • the end cap 80 is pushed all the way into the bearing housing 70 until the end cap lateral support flange 84 contacts the second of the lateral support bearings 42 of the seal ring 40. Once in place, the end cap 80 is fixed to the bearing housing 70 by inserting fasteners through the
  • the ring portion 51 of the outer ring 50 is inserted into the notch 47 of the seal ring 40 and the wheel flange 91 of the die wheel 90 is positioned adjacent the fastener flange 52 of the outer ring 50.
  • Wheel fasteners 91 are then inserted through the wheel flange 92 and the fastener flange 52 and locked into the seal ring 40.
  • both the extruder adapter 10 and the mounting plate 20 further comprise a flow bore 23 which extends from the extruder (not shown) to the flow surface 25, as shown in Figures 2 and 4.
  • the die 1 operates such that biodegradable extrudate material is pushed by the extruder through the flow bore 23 until it reaches the base flow surface 33 of the mandrel 30.
  • the biodegradable extrudate then flows radially outward around the spacers 100 between the flow surface 25 of the mounting plate 20 and the base flow surface 33 of the mandrel 30.
  • This disc-like space between the mounting plate 20 and the mandrel 30 is the flow control channel 4.
  • the biodegradable extrudate then enters a cylindrical space between the seal ring 40 and the mandrel 20 and is pushed through this space toward the extrusion orifice 5 between the mandrel 30 and the outer ring 50.
  • the die wheel 90 is rotated to rotate the outer ring 50 and seal ring 40 around the stationary mandrel 30.
  • the biodegradable extrudate is twisted by the rotating outer ring 50.
  • a tubular product of twisted biodegradable material is produced.
  • the seal ring 40 is rotatably mounted within the bearing housing 70, the seal ring 40 may be made to rotate about the mandrel 30 as the extrudate is pushed through the orifice 5.
  • Flow of the biodegradable material through the die 1 is controlled in two ways: (1) adjusting the width of the flow control channel 4, and (2) controlling the size of the extrusion orifice 5.
  • biodegradable material is passed from the extruder through a flow bore 23 in the mounting plate 20 until it reaches the base flow surface 33 of the mandrel 30. From the central location, the biodegradable material is
  • the biodegradable material flows between the surfaces through the flow control channel 4, it passes around each of the spacers 100 which separate the mandrel 30 and the mounting plate 20.
  • the width of the flow control channel 4 is adjusted by using spacers which have larger or smaller ribs 101 (See Figure 4).
  • spacers 100 having ribs 101 which are relatively thin in the longitudinal direction are inserted between the mounting plate 20 and the mandrel 30.
  • the die 1 has several sets of spacers 100 which may be placed between the mounting plate 20 and the mandrel 30 to control the width of the flow control channel 4.
  • flow of the biodegradable material through the extrusion orifice 5 is controlled by altering the width of the extrusion orifice 5.
  • the gap adjusting ring 60 is moved slightly away from the mounting plate 20 along the longitudinal central axis 3 in the direction of direction arrow 6 (shown in Figure 2), so that the outer ring lip 53 is positioned beyond the mandrel lip 37. Thus, a wider section of the ring portion 51 is adjacent the lip 37 of the mandrel 30 so that the extrusion orifice 5 is thicker.
  • lock screws 61 are screwed into the gap adjusting ring 60 to re-engage the mounting plate 20. This locks the gap adjusting ring 60, the bearing housing 70, the seal ring 40, and the outer ring 50 in place to ensure the thickness of the extrusion orifice 5 remains constant during operation. A thicker extrusion orifice 5 increases flow through the die.
  • the device also has a motor 110 which has a drive axis 113 which is parallel to longitudinal central axis 3. Attached to a drive shaft of motor 110, there is a drive wheel 111. The motor 110 and drive wheel 111 are positioned so that drive wheel 111 lies in the same plane as the die wheel 90, the plane being perpendicular to the longitudinal central axis 3.
  • the system further has a snubber wheel 115 which is also positioned in the perpendicular plane of the drive wheel 111 and the die wheel 90.
  • the snubber wheel 115 has a snubber axis 116 which is also parallel to the longitudinal central axis 3.
  • a drive belt 112 engages the drive wheel 111, the die wheel 90 and the snubber wheel 115.
  • the snubber wheel 115 has no drive mechanism for turning the drive belt 112.
  • the snubber wheel 115 is an idle wheel which only turns with the drive belt 112 when the drive belt 112 is driven by the motor 110.
  • the snubber wheel 115 serves only to evenly distribute forces exerted by the drive belt 112 on the die wheel 90. Because the drive wheel 111 and snubber wheel 115 are positioned on opposite sides of the die wheel 90, forces exerted by the drive belt 112 on the die wheel 90 are approximately equal in all transverse directions. If the snubber wheel 115 were not placed in this position and the drive belt 112 engaged only the drive wheel 111 and the die wheel 90, a net force would be exerted by the drive belt 112 on the die wheel 90 in the direction of the motor 110.
  • the snubber wheel 115 is positioned in the system to prevent the die wheel 90 from being pulled from its central location around the mandrel 30.
  • the drive belt 112 is a rubber belt.
  • chains or mating gears may be used to mechanically connect the motor 110 to the die wheel 90.
  • a typical one-third horse power electric motor is sufficient to produce the necessary torque to drive the drive belt 112.
  • the gear ratios between the drive wheel 111 and the die wheel 90 are such that the die wheel 90 may preferably rotate at approximately 15 rotations per minute. Depending on the particular gear system employed, alternative embodiments require more powerful motors.
  • the system 130 has a hopper 131 into which biodegradable material is initially placed (step 140).
  • the hopper 131 supplies (step 141) biodegradable material to an extruder 132 which pressurizes (step 142) and cooks (step 143) the biodegradable material.
  • the extruder 132 pushes (step 144) the biodegradable material through an extrusion die 1.
  • the extrusion die 1 is an embodiment of the rotating extrusion die of the present invention and is driven by a motor 110 with a drive belt 112.
  • step 144 As the biodegradable material is pushed (step 144) through the extrusion die 1, an outer ring of the die 1 is rotated (step 145) around an inner mandrel.
  • the biodegradable material is pushed (step 146) from the extrusion die 1 through an extrusion orifice to form a cylindrical extrudate 15.
  • the cylindrical extrudate 15 is then pulled (step 147) from the extrusion orifice by a pair of press rollers 133.
  • the press rollers 133 flatten (step 148) the cylindrical extrudate 15 into a sheet 17 of biodegradable material.
  • the sheet 17 of biodegradable material is then molded (step 149) between corresponding molds 134 to form the biodegradable material into final products.
  • the shaped final products are then deposited in bin 135.
  • FIG 10A an example of a biodegradable extrudate from the extrusion die of the present invention is shown.
  • the extrudate 15 exits from the extrusion orifice 5 (see Figure 2 for die components) as a cylindrical structure.
  • the polymer chains of the biodegradable material are aligned in the direction of extrusion to produce an extrudate which has its greatest structural integrity in the extrusion direction. If the extrudate 15 exits the extrusion orifice 5 as the outer ring 50 is rotated around the mandrel 30, the extrudate 15 orients along extrusion lines 16.
  • the cylindrical extrudate 15 is collapsed to form a sheet of biodegradable material having two extrudate layers.
  • Figure 10B a perspective view of a sheet of extrudate material produced from the tubular extrudate of Figure 10A is shown.
  • the sheet 17 is produced simply by rolling the extrudate 15 through two rollers to compress the tubular
  • the sheet 17 consequently comprises extrusion lines 16 which form a cross-hatch pattern.
  • the sheet 17 is comprised of two layers, one of which previously formed one side of the tubular extrudate 15 while the second layer of the sheet 17 previously formed the other side of the extrudate 15. Therefore, because the extrusion lines 16 were helically wound around the extrudate 15, when the sheet 17 is formed, the extrusion lines 16 of the two layers run in opposite directions.
  • the extrusion line angle 18 of the extrusion lines 16 may be adjusted by controlling the flow rate of the extrudate 15 from the extrusion orifice 5 of the die 1 (see Figure 2 for die components), and controlling the speed of angular rotation of the outer ring 50 about the mandrel 30.
  • the die is adjusted to increase the angular speed of the outer ring 50 relative to the mandrel 30, and/or to decrease the flow rate of the extrusion material from the extrusion die.
  • the flow rate of the biodegradable material through the die is controlled by adjusting the size of the extrusion orifice 5 and/or the flow control channel 4.
  • the outer ring 50 of the die 1 is made to rotate in both clockwise and counter-clockwise directions about the mandrel 30 to produce a biodegradable extrudate wherein the extrusion lines have a wave pattern.
  • the outer ring 50 is first rotated in one direction and then rotated in the opposite direction.
  • the pattern produced is sinusoidal, zigzag, or boxed. The periods and amplitudes of these wave patterns are adjusted by altering the rate of rotation of the outer ring 50 and the flow rate of the biodegradable material through the extrusion die 1.
  • the motor 110 of the embodiment shown in Figures 7A and 7B is made to alternate directions of rotation. As the motor 110 changes directions of rotation, the drive wheel 111, drive belt 112 and die wheel 90 consequently change directions.
  • the die wheel 90 is a spur gear with radial teeth parallel to the longitudinal central axis 3.
  • the teeth of the die wheel 90 are engaged by teeth of a rack gear 117.
  • an idler gear 124 is engaged with the die wheel 90 to prevent the rack gear 117 from pushing the outer ring 50 out of alignment with the mandrel 30 (See Figure 2).
  • the rack gear 117 is mounted on a slide support 118 and moves linearly along a slide direction 120 which is transverse to the longitudinal central axis 3.
  • the slide support 118 is connected to a drive wheel 111 via a linkage 114.
  • one end of the linkage 114 is connected to an end of the slide support 118 and the other end of the linkage 114
  • the slide support 118 is braced by brackets 125 so that slide support 118 is only allowed to move along slide direction 120.
  • the linkage 114 pushes and pulls the slide support 118 back and forth along slide direction 120.
  • the back and forth movement of the slide support 118 rotates the die wheel 90 and the outer ring 50 alternatively in clockwise and counter-clockwise directions.
  • this embodiment of the invention produces a biodegradable extrudate 15 with extrusion lines 16 which have a sine wave pattern as shown in
  • FIG 12A As described above, the extrudate 15 is rolled into a sheet 17 having two layers as shown in Figure 12B.
  • the period of the sine waves are identified by reference character 19 and the amplitude is identified by reference character 14.
  • the period 19 and amplitude 14 of extrusion lines 16 may be adjusted by controlling the flow rate of the extrudate 15 from the extrusion orifice 5 of the die 1 (see Figure 2 for die components), and controlling the speed of angular rotation of the outer ring 50 about the mandrel 30. If it is desirable to increase the period of the sine waves, the die is adjusted to decrease the angular speed of the outer ring 50 relative to the stationary mandrel 30, and/or to increase the flow rate of the extrusion material from the extrusion orifice 5.
  • the flow rate of the biodegradable material through the die is controlled by adjusting the size of the extrusion orifice 5 and/or the flow control channel 4. Further, if it is desirable to increase the amplitude 14 of the sine waves, the angular range of motion of the outer ring 50 is increased so that the outer ring 50 rotates further around the stationary mandrel 30 before it stops and changes direction. While many parameters may be altered to produce this result, a simple modification is to use a drive wheel 111 which has a relatively larger diameter.
  • the die wheel 90 is a spur gear with radial teeth parallel to the longitudinal central axis 3.
  • the teeth of the die wheel 90 are engaged by teeth of a worm gear 122 which is positioned with its axis of rotation transverse to the longitudinal central axis 3.
  • an idler gear 124 is engaged with the die wheel 90 to prevent the worm gear 122 from pushing the outer ring 50 out of alignment with the mandrel 30 (see Figure 2).
  • the worm gear 122 is driven by a motor 110 with a transmission 121 between.
  • a drive shaft 123 of the motor 110 is connected to a power side of
  • the transmission 121 and the worm gear 122 is connected to a drive side of the transmission 121. While the motor 110 rotates the drive shaft 123 in only one direction, the transmission 121 rotates the worm gear 122 in both clockwise and counter-clockwise directions. Further, in one embodiment, the transmission 121 rotates the worm gear 122 at different speeds even though the motor 110 operates at only one speed.
  • a similar embodiment comprises a motor and transmission which drive a pinion gear which engages the die wheel 90. Since the worm gear 122 is rotated at a constant speed in each direction, this embodiment of the invention produces a biodegradable extrudate which has a zigzag pattern of extrusion lines 16.
  • this embodiment of the invention produces a biodegradable extrudate 15 with extrusion lines 16 which have a linear oscillatory wave pattern or zigzag wave pattern as shown in Figure 14A.
  • the extrudate 15 is rolled into a sheet 17 having two layers as shown in Figure 14B.
  • the period of the zigzag waves are identified by reference character 19 and the amplitude is identified by reference character 14.
  • the period 19 and amplitude 14 of extrusion lines 16 is adjusted by controlling the flow rate of the extrudate 15 from the extrusion orifice 5 of the die 1 (see Figure 2 for die components), and controlling the speed of angular rotation of the outer ring 50 about the mandrel 30. If it is desirable to increase the period of the zigzag waves, the die is adjusted to decrease the angular speed of the outer ring 50 relative to the stationary mandrel 30, and/or to increase the flow rate of the extrusion material from the extrusion orifice 5. As noted above, the flow rate of the biodegradable material through the die is controlled by adjusting the size of the extrusion orifice 5 and/or the flow control channel 4.
  • the angular range of motion of the outer ring 50 is increased so that the outer ring 50 rotates further around the stationary mandrel 30 before it stops and changes direction. While many parameters may be altered to produce this result, a simple modification is to control the transmission 121 to allow the worm gear 122 to run longer in each direction before reversing the direction.
  • the die 1 is made up of several discrete annular members which share the same longitudinal central axis 3.
  • a mounting plate 20 is located in the center of the die 1 and is the member to which most of the remaining parts are attached. At one end of the mounting plate 20, an extruder adapter 10 is attached for
  • a mandrel 30 has counter sunk holes which correspond to those in the mounting plate 20.
  • the mandrel 30 is fixed to the mounting plate 20 with the spacers 100 between.
  • the spacers 100 create a gap between the mandrel 30 and the mounting plate 20, the thickness of which is dependent upon the thickness of the spacers 100. This gap is the flow control channel 4.
  • An outer die structure 55 is attached to the mounting plate 20.
  • the outer die structure 55 has a gap adjusting ring 60 at one end which is positioned concentrically around the cylindrical exterior of the mounting plate 20 and an outer ring 50 at the other end.
  • the outer ring 50 of the outer die structure 55 and the mandrel 30 combine to form an extrusion orifice 5.
  • the gap adjusting ring 60 secures the outer die structure 55 to the mounting plate 20 with lock screws 61 which engage the outer surface of the mounting plate 20.
  • Flow of the biodegradable material through the die 1 is controlled in two ways: (1) adjusting the width of the flow control channel 4, and (2) controlling the size of the extrusion orifice 5.
  • biodegradable material is passed from the extruder through a flow bore 23 in the mounting plate 20 until it reaches the mandrel 30. From the central location, the biodegradable material is pushed radially outward between the mandrel 30 and the mounting plate 20 through the flow control channel 4.
  • the biodegradable material flows between the surfaces through the flow control channel 4, it passes around each of the spacers 100 which separate the mandrel 30 and the mounting plate 20.
  • the width of the flow control channel 4 is adjusted by using spacers which have larger or smaller thicknesses in the longitudinal direction.
  • spacers which have larger or smaller thicknesses in the longitudinal direction.
  • relatively thin spacers 100 in the longitudinal direction are inserted between the mounting plate 20 and the mandrel 30.
  • relatively thick spacers 100 in the longitudinal direction are inserted between the mounting plate 20 and the mandrel 30. Therefore, in a preferred embodiment, the die 1 has several sets of spacers 100 which may be placed between the mounting plate 20 and the mandrel 30 to control the width of the flow control channel 4.
  • flow of the biodegradable material through the extrusion orifice 5 is controlled by altering the width of the orifice.
  • the thickness of the extrusion orifice 5 between the mandrel 30 and the outer ring 50 is adjusted by sliding the outer die structure 55 along the longitudinal central axis 3 out away from the stationary mandrel 30. Since the interior diameter
  • the outer die structure 55 has its smallest interior diameter at the outer ring 50.
  • the gap adjusting ring 60 is pushed all the way onto the mounting plate 20.
  • the gap adjusting ring 60 is moved slightly away from the mounting plate 20 along the longitudinal central axis 3 in the direction of direction arrow 6, so that the outer ring 50 is positioned beyond the mandrel 30.
  • a wider section of the outer die structure 55 is adjacent an orifice forming portion of the mandrel 30 so that the extrusion orifice 5 is thicker.
  • lock screws 61 are screwed into the gap adjusting ring 60 to re-engage the mounting plate 20. This locks the outer die structure 55 in place to ensure the thickness of the extrusion orifice 5 remains constant during operation. Of course, a thicker orifice 5 allows the biodegradable material to flow more freely through the die 1.
  • the die 1 is made up of several discrete annular members which share the same longitudinal central axis 3.
  • a mounting plate 20 is located in the center of the die 1 and is the member to which most of the remaining parts are attached.
  • an extruder adapter 10 is attached for connecting the die 1 to an extruder (not shown).
  • several spacers 100 are positioned in counter sunk holes in the mounting plate 20 at various locations equidistant from each other and from the longitudinal central axis 3.
  • a mandrel 30 has counter sunk holes which correspond to those in the mounting plate 20.
  • the mandrel is fixed to the mounting plate 20 with the spacers 100 between.
  • An outer die structure 55 is also attached to the mandrel 30.
  • the outer die structure 55 has a support portion 72 at one end and an outer ring 50 at the other.
  • the outer ring 50 and the mandrel 30 combine to form an extrusion orifice 5.
  • the support portion 72 is used to attach the outer die structure 55 to an outer portion 63 of the mounting plate 20.
  • the mounting plate 20 also has shifting lugs 64 which are screwed to the outer portion 63 of the mounting plate 20 with lug bolts 65.
  • shifting lugs 64 which are screwed to the outer portion 63 of the mounting plate 20 with lug bolts 65.
  • the shifting lugs 64 extend from the mounting plate 20 in a longitudinal direction toward the mandrel 30.
  • Shifting bolts 66 extend through distal ends of the center lugs 64 in directions transverse to the longitudinal central axis 3.
  • the support portion 72 of the outer die structure 55 is positioned within the shifting lugs 64 so that the shifting bolts 66 engage an outer surface of the support portion 72 of the outer die structure 55.
  • the outer die structure 55 is actually
  • Threaded holes 67 extend through the outer portion 63 of the mounting plate 20 in directions parallel to the longitudinal central axis 3.
  • Corresponding slip holes 75 extend through the support portion 72 of the outer die structure 55 in directions parallel to the longitudinal central axis 3. The slip holes 75 have a larger inside diameters than the threaded outside diameters of the screws 74 to allow "play" between the screws 74 and the slip holes 75.
  • the orifice 5 geometry is modified by moving the outer die structure 55 relative to the mandrel 30. In the above described embodiment, this is accomplished by loosening screws 74 slightly to allow the outer die structure 55 to move relative to the mounting plate 20. Shifting bolts 66 are then adjusted against the support portion of the outer die structure 55 to push the outer ring 50 to a desired position relative to the mandrel 30. Once the outer die structure 55 is properly positioned, the screws 74 are tightened to securely fix the outer die structure 55 to the mounting plate 20.

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Extrusion Moulding Of Plastics Or The Like (AREA)

Abstract

Cette filière destinée à l'extrusion de matériau biodégradable est pourvu d'un mandrin (30), d'un élément extérieur (40) placé près du mandrin, d'un orifice d'extrusion (5) se trouvant entre le mandrin et l'élément extérieur, d'un élément en communication avec au moins un élément définisseur de l'orifice d'extrusion, l'élément étant en mesure de produire un mouvement relatif entre l'élément extérieur et le mandrin, lequel mouvement relatif a une composante transverse au sens d'extrusion du matériau biodégradable passant par l'orifice d'extrusion, d'un dispositif régulateur de débit agissant sur le flux de matériau biodégradable passant par l'orifice d'extrusion ainsi que d'un dispositif positionnant relativement l'un à l'autre l'élément extérieur et le mandrin. L'invention concerne également un procédé amélioré d'extrusion de matériau biodégradable, le processus d'extrusion supposant un écoulement du matériau biodégradable dans une direction donnée à travers un orifice. L'amélioration apportée consiste à faire se déplacer le matériau biodégradable dans une direction ayant une composante transverse au sens d'écoulement lors de l'extrusion et à agir sur le débit du matériau biodégradable lors du passage par l'orifice d'extrusion. Cette régulation du débit repose sur le réglage de la pression amont du matériau biodégradable dans la filière d'extrusion ainsi que sur le réglage d'au moins une section transversale du circuit d'écoulement du matériau biodégradable à l'intérieur de la filière d'extrusion et sur la modification de la géométrie de l'orifice.
PCT/US1999/004774 1998-03-05 1999-03-04 Filiere d'extrusion pour materiau biodegradable a dispositif modificateur de l'orifice de la filiere et dispositif regulateur de debit Ceased WO1999044806A1 (fr)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CA002323157A CA2323157C (fr) 1998-03-05 1999-03-04 Filiere d'extrusion pour materiau biodegradable a dispositif modificateur de l'orifice de la filiere et dispositif regulateur de debit
EP99912276A EP1069982A1 (fr) 1998-03-05 1999-03-04 Filiere d'extrusion pour materiau biodegradable a dispositif modificateur de l'orifice de la filiere et dispositif regulateur de debit
AU30687/99A AU3068799A (en) 1998-03-05 1999-03-04 Extrusion die for biodegradable material with die orifice modifying device and flow control device
JP2000534387A JP2002514522A (ja) 1998-03-05 1999-03-04 ダイオリフィス調節装置および流量制御装置を有する生分解性材料用押出し成形ダイ

Applications Claiming Priority (14)

Application Number Priority Date Filing Date Title
US3560598A 1998-03-05 1998-03-05
US3541998A 1998-03-05 1998-03-05
US3541898A 1998-03-05 1998-03-05
US3541798A 1998-03-05 1998-03-05
US3556698A 1998-03-05 1998-03-05
US09/035,566 1998-03-05
US09/035,605 1998-03-05
US09/035,417 1998-03-05
US09/035,200 US6183672B1 (en) 1998-03-05 1998-03-05 Extrusion die for biodegradable material with die orifice modifying device and flow control device
US09/035,200 1998-03-05
US09/035,560 US6103151A (en) 1998-03-05 1998-03-05 Extrusion die for biodegradable material with flow control device
US09/035,560 1998-03-05
US09/035,419 1998-03-05
US09/035,418 1998-03-05

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WO1999044806A1 true WO1999044806A1 (fr) 1999-09-10

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EP (1) EP1069982A1 (fr)
JP (2) JP2002514522A (fr)
AU (1) AU3068799A (fr)
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WO (1) WO1999044806A1 (fr)

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US7264461B2 (en) 2005-10-14 2007-09-04 Frito-Lay North America, Inc. Externally adjustable insert for extrusion manifold

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JP2011052028A (ja) * 2003-11-05 2011-03-17 Nichirei Foods:Kk ポリフェノールおよび／またはビタミンｃを含有するアセロラ処理物

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JP2009179060A (ja) 2009-08-13
EP1069982A1 (fr) 2001-01-24
CA2323157C (fr) 2008-09-30

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