WO2004008127A3 - Vorrichtung und verfahren zur erzeugung einer definierten umgebung für partikelförmige proben - Google Patents

Vorrichtung und verfahren zur erzeugung einer definierten umgebung für partikelförmige proben Download PDF

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Publication number
WO2004008127A3
WO2004008127A3 PCT/EP2003/007606 EP0307606W WO2004008127A3 WO 2004008127 A3 WO2004008127 A3 WO 2004008127A3 EP 0307606 W EP0307606 W EP 0307606W WO 2004008127 A3 WO2004008127 A3 WO 2004008127A3
Authority
WO
WIPO (PCT)
Prior art keywords
gas
temperature
outlet end
generation
cooler
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2003/007606
Other languages
English (en)
French (fr)
Other versions
WO2004008127A2 (de
Inventor
Torsten Neuefeind
Reiner Kiefersauer
Holger Venzke
Martin Still
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Proteros Biostructures GmbH
Original Assignee
Proteros Biostructures GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Proteros Biostructures GmbH filed Critical Proteros Biostructures GmbH
Priority to AU2003246693A priority Critical patent/AU2003246693A1/en
Priority to JP2004520622A priority patent/JP3976150B2/ja
Priority to DE50301158T priority patent/DE50301158D1/de
Priority to EP03763844A priority patent/EP1502099B1/de
Priority to AT03763844T priority patent/ATE304172T1/de
Publication of WO2004008127A2 publication Critical patent/WO2004008127A2/de
Publication of WO2004008127A3 publication Critical patent/WO2004008127A3/de
Priority to US11/035,769 priority patent/US7281669B2/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/20—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
    • G01N23/20008—Constructional details of analysers, e.g. characterised by X-ray source, detector or optical system; Accessories therefor; Preparing specimens therefor
    • G01N23/20025—Sample holders or supports therefor
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/20—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/02—Devices for withdrawing samples
    • G01N1/22—Devices for withdrawing samples in the gaseous state

Landscapes

  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Peptides Or Proteins (AREA)

Abstract

Die vorliegende Erfindung schafft eine Vorrichtung zur Erzeugung einer definierten Umgebung für partikelförmige Proben, die ein Halteelement (22) mit einem Auflageende für eine partikelförmige Probe und eine Vorrichtung zum Erzeugen eines feuchten Gasstroms an einem Mündungsende (30) derselben, wobei das Mündungsende (30) auf das Auflageende gerichtet ist, aufweist. Die Vorrichtung zum Erzeugen des feuchten Gasstroms umfasst eine Einrichtung (44) zum Bereitstellen eines Gases, das eine erste Temperatur und eine erste relative Feuchte aufweist, so dass das Gas eine erste Taupunkttemperatur besitzt. Ferner ist ein Kühler (46) zum Abkühlen des Gases auf eine Kühlertemperatur unter Kondensation von Feuchtigkeit vorgesehen, um eine zweite Taupunkttemperatur des Gases, die der Kühlertemperatur entspricht, einzustellen. Eine Einrichtung (24,28) zum Leiten des Gases mit der zweiten Taupunkttemperatur zu dem Mündungsende (30) unter Verhinderung einer Kondensation von Feuchtigkeit aus dem Gas und eine Einrichtung zum Einstellen der relativen Feuchte des Gases an dem Mündungsende (30)durch Einstellen der Kühlertemperatur und der Temperatur des Gases an dem Mündungsende sind ferner vorgesehen.
PCT/EP2003/007606 2002-07-16 2003-07-14 Vorrichtung und verfahren zur erzeugung einer definierten umgebung für partikelförmige proben Ceased WO2004008127A2 (de)

Priority Applications (6)

Application Number Priority Date Filing Date Title
AU2003246693A AU2003246693A1 (en) 2002-07-16 2003-07-14 Device and method for generation of a defined environment for particulate samples
JP2004520622A JP3976150B2 (ja) 2002-07-16 2003-07-14 粒子状サンプルのための所定の環境を生成するための装置及び方法
DE50301158T DE50301158D1 (de) 2002-07-16 2003-07-14 Vorrichtung und verfahren zur erzeugung einer definierten umgebung für partikelförmige proben
EP03763844A EP1502099B1 (de) 2002-07-16 2003-07-14 Vorrichtung und verfahren zur erzeugung einer definierten umgebung für partikelförmige proben
AT03763844T ATE304172T1 (de) 2002-07-16 2003-07-14 Vorrichtung und verfahren zur erzeugung einer definierten umgebung für partikelförmige proben
US11/035,769 US7281669B2 (en) 2002-07-16 2005-01-13 Apparatus and method for generating a defined environment for particle-shaped samples

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10232172A DE10232172B4 (de) 2002-07-16 2002-07-16 Vorrichtung und Verfahren zur Erzeugung einer definierten Umgebung für partikelförmige Proben
DE10232172.8 2002-07-16

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US11/035,769 Continuation US7281669B2 (en) 2002-07-16 2005-01-13 Apparatus and method for generating a defined environment for particle-shaped samples

Publications (2)

Publication Number Publication Date
WO2004008127A2 WO2004008127A2 (de) 2004-01-22
WO2004008127A3 true WO2004008127A3 (de) 2004-03-18

Family

ID=30010045

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2003/007606 Ceased WO2004008127A2 (de) 2002-07-16 2003-07-14 Vorrichtung und verfahren zur erzeugung einer definierten umgebung für partikelförmige proben

Country Status (8)

Country Link
US (1) US7281669B2 (de)
EP (1) EP1502099B1 (de)
JP (1) JP3976150B2 (de)
AT (1) ATE304172T1 (de)
AU (1) AU2003246693A1 (de)
DE (2) DE10232172B4 (de)
ES (1) ES2249735T3 (de)
WO (1) WO2004008127A2 (de)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7325748B2 (en) * 2002-09-03 2008-02-05 Phillip F. Acker, Jr. Ventilation system with humidity responsive ventilation controller
DE10336110B4 (de) * 2003-08-06 2008-01-03 Proteros Biostructures Gmbh Vorrichtung und Verfahren zum Behandeln eines Proteinkristalls
US9863862B2 (en) * 2013-03-15 2018-01-09 Tsi Incorporated Method and system for significantly improving charge probabilities of nanometer aerosol particles
EP2848924B1 (de) * 2013-09-11 2016-08-24 Anton Paar GmbH Temperierkammer für kompaktes Röntgengerät
DE102013019435A1 (de) 2013-11-20 2015-05-21 Proteros Biostructures Gmbh Verfahren und Vorrichtung zur Behandlung einer biologischen Probe, insbesondere eines Proteinkristalls
JP6237264B2 (ja) * 2014-01-24 2017-11-29 東京エレクトロン株式会社 縦型熱処理装置、熱処理方法及び記憶媒体
WO2020105723A1 (ja) * 2018-11-23 2020-05-28 株式会社リガク 単結晶ｘ線構造解析試料の吸蔵装置及び吸蔵方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000023795A1 (en) * 1998-10-21 2000-04-27 Glaxo Group Limited Environmentally controllable sample holder for x-ray diffractometer (xrd)
US6355217B1 (en) * 1998-09-18 2002-03-12 Max-Planck-Gesellschaft, Zur Forderung Der Wissenschaften E.V. Holding device for particulate samples

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3532270A (en) * 1969-02-03 1970-10-06 Us Navy Partial pressure low level humidity generator
US5457983A (en) * 1994-08-23 1995-10-17 Tecnovir International Inc. Apparatus and method for producing a reference gas
DE19541238A1 (de) * 1995-11-06 1996-06-27 Andreas Dipl Phys Dr Hieke Anordnung zur hochgenauen Temperierung von frei zugänglichen und beweglichen Proben durch ein Gas, sowie Verfahren zur Erzeugung eines thermisch homogenen Gasstromes zur Durchführung der Temperierung
AT3403U1 (de) * 1998-09-25 2000-02-25 E & E Elektronik Gmbh Vorrichtung zur erzeugung einer definierten relativen luftfeuchte
JP3877954B2 (ja) * 2000-11-09 2007-02-07 エスアイアイ・ナノテクノロジー株式会社 自動湿度ステップ制御熱分析装置

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6355217B1 (en) * 1998-09-18 2002-03-12 Max-Planck-Gesellschaft, Zur Forderung Der Wissenschaften E.V. Holding device for particulate samples
WO2000023795A1 (en) * 1998-10-21 2000-04-27 Glaxo Group Limited Environmentally controllable sample holder for x-ray diffractometer (xrd)

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
KIEFERSAUER R ET AL: "A NOVEL FREE-MOUNTING SYSTEM FOR PROTEIN CRYSTALS: TRANSFORMATION AND IMPROVEMENT OF DIFFRACTION POWER BY ACCURATELY CONTROLLED HUMIDITY CHANGES", JOURNAL OF APPLIED CRYSTALLOGRAPHY, COPENHAGEN, DK, vol. 33, 2000, pages 1223 - 1230, XP009021980, ISSN: 0021-8898 *
KIEFERSAUER R ET AL: "PROTEIN-CRYSTAL DENSITY BY VOLUME MEASUREMENT AND AMINO-ACID ANALYSIS", JOURNAL OF APPLIED CRYSTALLOGRAPHY, COPENHAGEN, DK, vol. 29, no. 4, 1996, pages 311 - 317, XP000866399, ISSN: 0021-8898 *

Also Published As

Publication number Publication date
DE10232172A1 (de) 2004-02-12
JP2005538345A (ja) 2005-12-15
DE50301158D1 (de) 2005-10-13
JP3976150B2 (ja) 2007-09-12
EP1502099B1 (de) 2005-09-07
ES2249735T3 (es) 2006-04-01
WO2004008127A2 (de) 2004-01-22
AU2003246693A1 (en) 2004-02-02
ATE304172T1 (de) 2005-09-15
DE10232172B4 (de) 2005-03-10
US7281669B2 (en) 2007-10-16
EP1502099A2 (de) 2005-02-02
US20050183518A1 (en) 2005-08-25

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