WO2009069220A1 - アンモニア合成用素ガスの製造方法および製造装置 - Google Patents

アンモニア合成用素ガスの製造方法および製造装置 Download PDF

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Publication number
WO2009069220A1
WO2009069220A1 PCT/JP2007/073109 JP2007073109W WO2009069220A1 WO 2009069220 A1 WO2009069220 A1 WO 2009069220A1 JP 2007073109 W JP2007073109 W JP 2007073109W WO 2009069220 A1 WO2009069220 A1 WO 2009069220A1
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WO
WIPO (PCT)
Prior art keywords
raw gas
ammonia synthesis
production
oxygen
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2007/073109
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English (en)
French (fr)
Inventor
Nobuhiro Yamada
Yoshinori Mashiko
Shuichi Funatsu
Yoshiyuki Watanabe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JGC Corp
Osaka Gas Co Ltd
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JGC Corp
Osaka Gas Co Ltd
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Publication date
Application filed by JGC Corp, Osaka Gas Co Ltd filed Critical JGC Corp
Priority to JP2009543623A priority Critical patent/JPWO2009069220A1/ja
Priority to PCT/JP2007/073109 priority patent/WO2009069220A1/ja
Priority to EP07832809A priority patent/EP2186778A4/en
Priority to US12/677,297 priority patent/US20100200812A1/en
Publication of WO2009069220A1 publication Critical patent/WO2009069220A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C01B3/32—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air
    • C01B3/34—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/382—Processes with two or more reaction steps, of which at least one is catalytic, e.g. steam reforming and partial oxidation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C01B3/025—Preparation or purification of gas mixtures for ammonia synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C01B3/32—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air
    • C01B3/34—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents
    • C01B3/38—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents using catalysts
    • C01B3/386—Catalytic partial combustion
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/02—Production of hydrogen; Production of gaseous mixtures containing hydrogen
    • C01B3/32—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air
    • C01B3/34—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents
    • C01B3/48—Production of hydrogen; Production of gaseous mixtures containing hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air by reaction of hydrocarbons with gasifying agents followed by reaction of water vapour with carbon monoxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0244—Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being an autothermal reforming step, e.g. secondary reforming processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02—Processes for making hydrogen or synthesis gas
    • C01B2203/0283—Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0415—Purification by absorption in liquids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0435—Catalytic purification
    • C01B2203/0445—Selective methanation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/047—Composition of the impurity the impurity being carbon monoxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0475—Composition of the impurity the impurity being carbon dioxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06—Integration with other chemical processes
    • C01B2203/068—Ammonia synthesis

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Hydrogen, Water And Hydrids (AREA)

Abstract

  　このアンモニア合成用素ガスの製造方法では、管３からの軽質炭化水素と、管６からのスチームと、酸素富化空気供給源７からの酸素濃度４０～６０体積％の酸素富化空気を加熱して１段改質反応器５に導入し、水蒸気改質反応と空気部分酸化反応を同時に行う。ついで、シフト反応器１２、脱炭酸器１４、メタン化反応器１６に通して、一酸化炭素、二酸化炭素を除去し、水素と窒素とのモル比がほぼ３：１のアンモニア合成に適した素ガスを得る。
PCT/JP2007/073109 2007-11-29 2007-11-29 アンモニア合成用素ガスの製造方法および製造装置 Ceased WO2009069220A1 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP2009543623A JPWO2009069220A1 (ja) 2007-11-29 2007-11-29 アンモニア合成用素ガスの製造方法および製造装置
PCT/JP2007/073109 WO2009069220A1 (ja) 2007-11-29 2007-11-29 アンモニア合成用素ガスの製造方法および製造装置
EP07832809A EP2186778A4 (en) 2007-11-29 2007-11-29 PROCESS AND APPARATUS FOR PRODUCING RAW GAS FOR THE SYNTHESIS OF AMMONIA
US12/677,297 US20100200812A1 (en) 2007-11-29 2007-11-29 Production method for raw gas for ammonia synthesis and production apparatus therefor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/JP2007/073109 WO2009069220A1 (ja) 2007-11-29 2007-11-29 アンモニア合成用素ガスの製造方法および製造装置

Publications (1)

Publication Number Publication Date
WO2009069220A1 true WO2009069220A1 (ja) 2009-06-04

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PCT/JP2007/073109 Ceased WO2009069220A1 (ja) 2007-11-29 2007-11-29 アンモニア合成用素ガスの製造方法および製造装置

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Country Link
US (1) US20100200812A1 (ja)
EP (1) EP2186778A4 (ja)
JP (1) JPWO2009069220A1 (ja)
WO (1) WO2009069220A1 (ja)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20140120023A1 (en) * 2012-10-31 2014-05-01 General Electric Company Methods and systems for ammonia production
WO2019043875A1 (ja) * 2017-08-31 2019-03-07 日揮株式会社 高窒素含有天然ガスを用いたアンモニアの製造方法
JP2022094908A (ja) * 2020-12-15 2022-06-27 エコナ パワー インコーポレイテッド 原料ガス反応器を用いて水素および窒素を生産する方法

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9140220B2 (en) 2011-06-30 2015-09-22 Lg Fuel Cell Systems Inc. Engine systems and methods of operating an engine
US9178235B2 (en) * 2009-09-04 2015-11-03 Lg Fuel Cell Systems, Inc. Reducing gas generators and methods for generating a reducing gas
US9118048B2 (en) 2009-09-04 2015-08-25 Lg Fuel Cell Systems Inc. Engine systems and methods of operating an engine
DE102010035885A1 (de) 2010-08-30 2012-03-01 Uhde Gmbh Verfahren zur Herstellung von Synthesegas aus kohlenwasserstoffhaltigen Einsatzgasen
EP2723676B1 (en) * 2011-06-23 2018-12-05 Stamicarbon B.V. acting under the name of MT Innovation Center Process for producing ammonia and urea
CA2875696C (en) 2012-06-27 2020-09-01 Grannus, Llc Polygeneration production of power and fertilizer through emissions capture
EP2801550A1 (en) * 2013-05-10 2014-11-12 Ammonia Casale S.A. A process for producing ammonia synthesis gas with high temperature shift and low steam-to-carbon ratio
US9968906B2 (en) * 2015-06-01 2018-05-15 The United States Of America, As Represented By The Secretary Of The Army Reforming with oxygen-enriched matter
GB201721126D0 (en) * 2017-12-18 2018-01-31 Johnson Matthey Plc Process for producing methanol and ammonia

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59195502A (ja) 1983-04-15 1984-11-06 Toyo Eng Corp アンモニア合成ガスの製造法
JPS6011587A (ja) * 1983-05-31 1985-01-21 ケイアールダブリュ　エネルギー　システムズ　インク アンモニア製造のためのガス化方法
JPS60186401A (ja) * 1984-01-30 1985-09-21 フルオー・コーポレイシヨン 合成ガスの自熱製造方法及び該方法で使用される反応装置
US4792441A (en) 1988-01-19 1988-12-20 Air Products And Chemicals, Inc. Ammonia synthesis
JPH04310501A (ja) * 1991-04-03 1992-11-02 Mw Kellogg Co 自己熱式スチーム改質プロセス
US5202057A (en) 1988-09-14 1993-04-13 Air Products And Chemicals, Inc. Production of ammonia synthesis gas
JP2007320779A (ja) * 2006-05-30 2007-12-13 Jgc Corp アンモニア合成用素ガスの製造方法および製造装置

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US4409196A (en) * 1979-04-24 1983-10-11 Foster Wheeler Energy Corporation Synthesis gas for ammonia production
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ITMI20011553A1 (it) * 2001-07-20 2003-01-20 Snam Progetti Processo per la sintesi di ammoniaca
US6911161B2 (en) * 2002-07-02 2005-06-28 Conocophillips Company Stabilized nickel-containing catalysts and process for production of syngas
EP1698588A1 (en) * 2005-03-04 2006-09-06 Ammonia Casale S.A. Ammonia synthesis process
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Patent Citations (7)

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Publication number Priority date Publication date Assignee Title
JPS59195502A (ja) 1983-04-15 1984-11-06 Toyo Eng Corp アンモニア合成ガスの製造法
JPS6011587A (ja) * 1983-05-31 1985-01-21 ケイアールダブリュ　エネルギー　システムズ　インク アンモニア製造のためのガス化方法
JPS60186401A (ja) * 1984-01-30 1985-09-21 フルオー・コーポレイシヨン 合成ガスの自熱製造方法及び該方法で使用される反応装置
US4792441A (en) 1988-01-19 1988-12-20 Air Products And Chemicals, Inc. Ammonia synthesis
US5202057A (en) 1988-09-14 1993-04-13 Air Products And Chemicals, Inc. Production of ammonia synthesis gas
JPH04310501A (ja) * 1991-04-03 1992-11-02 Mw Kellogg Co 自己熱式スチーム改質プロセス
JP2007320779A (ja) * 2006-05-30 2007-12-13 Jgc Corp アンモニア合成用素ガスの製造方法および製造装置

Non-Patent Citations (1)

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Title
See also references of EP2186778A4 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20140120023A1 (en) * 2012-10-31 2014-05-01 General Electric Company Methods and systems for ammonia production
WO2019043875A1 (ja) * 2017-08-31 2019-03-07 日揮株式会社 高窒素含有天然ガスを用いたアンモニアの製造方法
JP2022094908A (ja) * 2020-12-15 2022-06-27 エコナ パワー インコーポレイテッド 原料ガス反応器を用いて水素および窒素を生産する方法

Also Published As

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EP2186778A4 (en) 2011-08-17
US20100200812A1 (en) 2010-08-12
EP2186778A1 (en) 2010-05-19
JPWO2009069220A1 (ja) 2011-04-07

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