WO2012004125A2 - Appareil de refroidissement et d'epuration d'air destine a une unite de distillation cryogenique d'air - Google Patents

Appareil de refroidissement et d'epuration d'air destine a une unite de distillation cryogenique d'air Download PDF

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Publication number
WO2012004125A2
WO2012004125A2 PCT/EP2011/060417 EP2011060417W WO2012004125A2 WO 2012004125 A2 WO2012004125 A2 WO 2012004125A2 EP 2011060417 W EP2011060417 W EP 2011060417W WO 2012004125 A2 WO2012004125 A2 WO 2012004125A2
Authority
WO
WIPO (PCT)
Prior art keywords
bottles
tower
building
air
cooling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2011/060417
Other languages
English (en)
French (fr)
Other versions
WO2012004125A3 (fr
Inventor
Patrice Cavagne
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Priority to US13/808,931 priority Critical patent/US20130152629A1/en
Priority to EP11726805.2A priority patent/EP2591299B1/de
Priority to CN201180033991.8A priority patent/CN103299146B/zh
Priority to CA2803147A priority patent/CA2803147C/fr
Priority to RU2013105495/06A priority patent/RU2557151C2/ru
Priority to UAA201300284A priority patent/UA107597C2/ru
Publication of WO2012004125A2 publication Critical patent/WO2012004125A2/fr
Anticipated expiration legal-status Critical
Publication of WO2012004125A3 publication Critical patent/WO2012004125A3/fr
Ceased legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04157Afterstage cooling and so-called "pre-cooling" of the feed air upstream the air purification unit and main heat exchange line
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04163Hot end purification of the feed air
    • F25J3/04169Hot end purification of the feed air by adsorption of the impurities
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04866Construction and layout of air fractionation equipments, e.g. valves, machines
    • F25J3/0489Modularity and arrangement of parts of the air fractionation unit, in particular of the cold box, e.g. pre-fabrication, assembling and erection, dimensions, horizontal layout "plot"
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00Processes or apparatus using other separation and/or other processing means
    • F25J2205/30Processes or apparatus using other separation and/or other processing means using a washing, e.g. "scrubbing" or bubble column for purification purposes
    • F25J2205/32Processes or apparatus using other separation and/or other processing means using a washing, e.g. "scrubbing" or bubble column for purification purposes as direct contact cooling tower to produce a cooled gas stream, e.g. direct contact after cooler [DCAC]
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00Processes or apparatus using other separation and/or other processing means
    • F25J2205/60Processes or apparatus using other separation and/or other processing means using adsorption on solid adsorbents, e.g. by temperature-swing adsorption [TSA] at the hot or cold end

Definitions

  • the present invention relates to an apparatus for cooling and purifying air for a cryogenic distillation unit for air.
  • a cryogenic distillation air separation apparatus In a cryogenic distillation air separation apparatus, the air is compressed in a compressor and then cooled by direct heat exchange with air in a cooling tower. The cooled air is then purified.
  • the purges in the air separation units mainly remove water and CO 2 from the air before entering the cryogenic distillation unit, placed in a cold box.
  • a set of valves and pipes allow the transit of the air to be purified and the impure nitrogen used for the regeneration of the purification bottles. This set of valves and pipes is placed "flat" on the ground and has a large footprint. The ratio of the height and length of the set is close to 1
  • One of the ways to reduce the width of this set is, through a different piping design, to extend this set.
  • the ratio between the height and the width of the set becomes much less than 1.
  • the air cooling tower by direct contact with water is installed between the two purification bottles.
  • an apparatus for cooling and purifying an air flow comprising a cooling tower by direct contact with water, two purification bottles, each having an axis vertical, a pipe for sending water to the cooling tower, a pipe for sending air to the cooling tower, the tower being disposed between the two bottles, a pipe for sending cooled air from the tower to the purification bottles and a set of valves and pipes for connecting the two bottles to the cooling tower, characterized in that the apparatus comprises a building, ⁇ together being located inside the building and both bottles and the tower being outside the building, the two bottles and the set being placed on either side of a wall of the building, the bottles being placed along the wall.
  • the center of the tower seen from above is situated on the median line between the centers of the two bottles seen from above;
  • the building also contains at least one compressor and / or at least one turbine and / or at least one distillation column;
  • the ratio between the dimension of the assembly in the vertical direction and the dimension in the horizontal direction is less than 1;
  • the wall constitutes the longest wall of the building, the building being of rectangular section;
  • the ratio of the length of the wall to the width of the building is greater than 2.
  • an air separation apparatus comprising a cooling and purification apparatus as described above.
  • the air separation apparatus may include a compressor in the building which is an air compressor connected to the cooling tower and / or a turbine in the building, which is an air turbine connected to the bottles and / or a distillation column in the building and connected to the purification bottles.
  • the apparatus comprises a cooling tower 1 by direct contact with water, two purification bottles 3A, 3B for purifying air in water and CO 2 and a building 5 containing at least one set of pipes 7 and valves to allow air from the tower 1 to be sent to the bottles 3A, 3B.
  • Some of the pipes of the assembly 7 pass through the wall 9 of the building 5.
  • the wall 9 is the longest wall of the building 5 which is of rectangular section. The ratio between the length of the wall 9 and the width of the building is preferably greater than 2.
  • the ratio between the dimension of the assembly 7 in the vertical direction and the dimension in the horizontal direction is less than 1.
  • the two bottles 3A, 3B and the tower are arranged along the wall 9 so that their centers seen from above form a straight line parallel to the wall.
  • the tower is arranged on the center line between the two bottles.
  • the tower 1 may be slightly closer to or further from the wall 9 than the two bottles 3A, 3B so that the centers of the tower and the two bottles form an obtuse angle triangle.
  • the building 5 may also contain a compressor and / or a turbine and / or a distillation column of the air separation apparatus of which the cooling and purification apparatus is part.
  • the air separation apparatus may comprise a compressor in the building 5 which is an air compressor connected to the cooling tower 1 and / or a turbine, in the building 5, which is an air turbine connected to the purification bottles 3A, 3B and / or a distillation column in the building 5 and connected to the purification bottles 3A, 3B.

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
PCT/EP2011/060417 2010-07-09 2011-06-22 Appareil de refroidissement et d'epuration d'air destine a une unite de distillation cryogenique d'air Ceased WO2012004125A2 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
US13/808,931 US20130152629A1 (en) 2010-07-09 2011-06-22 "Air cooling and purification apparatus intended for a cryogenic air distillation unit"
EP11726805.2A EP2591299B1 (de) 2010-07-09 2011-06-22 Lüftkühlungs- und reinigungsgerät für eine kryogene luftzerlegungsanlage
CN201180033991.8A CN103299146B (zh) 2010-07-09 2011-06-22 用于低温空气蒸馏单元的空气冷却和净化设备
CA2803147A CA2803147C (fr) 2010-07-09 2011-06-22 Appareil de refroidissement et d'epuration d'air destine a une unite de distillation cryogenique d'air
RU2013105495/06A RU2557151C2 (ru) 2010-07-09 2011-06-22 Аппарат охлаждения и очистки воздуха для установки криогенной дистилляции воздуха
UAA201300284A UA107597C2 (uk) 2010-07-09 2011-06-22 Блок для охолодження і очищення повітря, передбачений для установки для кріогенної дистиляції повітря

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1055603A FR2962526B1 (fr) 2010-07-09 2010-07-09 Appareil de refroidissement et d'epuration d'air destine a une unite de distillation cryogenique d'air
FR1055603 2010-07-09

Publications (2)

Publication Number Publication Date
WO2012004125A2 true WO2012004125A2 (fr) 2012-01-12
WO2012004125A3 WO2012004125A3 (fr) 2013-10-10

Family

ID=43868145

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2011/060417 Ceased WO2012004125A2 (fr) 2010-07-09 2011-06-22 Appareil de refroidissement et d'epuration d'air destine a une unite de distillation cryogenique d'air

Country Status (8)

Country Link
US (1) US20130152629A1 (de)
EP (1) EP2591299B1 (de)
CN (1) CN103299146B (de)
CA (1) CA2803147C (de)
FR (1) FR2962526B1 (de)
RU (1) RU2557151C2 (de)
UA (1) UA107597C2 (de)
WO (1) WO2012004125A2 (de)

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1672301A1 (de) 2004-12-03 2006-06-21 Linde AG Vorrichtung zur Tieftemperaturzerlegung eines Gasgemischs, insbesondere von Luft

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3143412A (en) * 1960-11-28 1964-08-04 Dravo Corp Method of enriching the oxygen content of air supplied to blast furnaces
FR2695714B1 (fr) * 1992-09-16 1994-10-28 Maurice Grenier Installation de traitement cryogénique, notamment de distillation d'air.
FR2706025B1 (fr) * 1993-06-03 1995-07-28 Air Liquide Installation de distillation d'air.
FR2774752B1 (fr) * 1998-02-06 2000-06-16 Air Liquide Installation de distillation d'air et boite froide correspondante
DE10342788A1 (de) * 2003-09-15 2005-04-07 Linde Ag Coldbox
FR2929385A1 (fr) * 2008-03-28 2009-10-02 Air Liquide Appareil et procede de separation d'air par distillation cryogenique

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1672301A1 (de) 2004-12-03 2006-06-21 Linde AG Vorrichtung zur Tieftemperaturzerlegung eines Gasgemischs, insbesondere von Luft

Also Published As

Publication number Publication date
FR2962526A1 (fr) 2012-01-13
CA2803147C (fr) 2018-04-17
CA2803147A1 (fr) 2012-01-12
CN103299146A (zh) 2013-09-11
CN103299146B (zh) 2016-02-10
EP2591299B1 (de) 2018-10-17
WO2012004125A3 (fr) 2013-10-10
US20130152629A1 (en) 2013-06-20
EP2591299A2 (de) 2013-05-15
RU2013105495A (ru) 2014-08-20
UA107597C2 (uk) 2015-01-26
FR2962526B1 (fr) 2014-07-04
RU2557151C2 (ru) 2015-07-20

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