WO2012013177A3 - Verfahren und apparatur zur abdampfung von halogenwasserstoff und wasser aus halogensauren biomassehydrolysaten - Google Patents

Verfahren und apparatur zur abdampfung von halogenwasserstoff und wasser aus halogensauren biomassehydrolysaten Download PDF

Info

Publication number
WO2012013177A3
WO2012013177A3 PCT/DE2011/001423 DE2011001423W WO2012013177A3 WO 2012013177 A3 WO2012013177 A3 WO 2012013177A3 DE 2011001423 W DE2011001423 W DE 2011001423W WO 2012013177 A3 WO2012013177 A3 WO 2012013177A3
Authority
WO
WIPO (PCT)
Prior art keywords
heat
transfer medium
continuously
water
hydrogen halide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/DE2011/001423
Other languages
English (en)
French (fr)
Other versions
WO2012013177A4 (de
WO2012013177A2 (de
Inventor
Frank Kose
Matthias Schmidt
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Green Sugar GmbH Produktinnovationen Aus Biomasse
Original Assignee
Green Sugar GmbH Produktinnovationen Aus Biomasse
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Green Sugar GmbH Produktinnovationen Aus Biomasse filed Critical Green Sugar GmbH Produktinnovationen Aus Biomasse
Priority to EP11770676.2A priority Critical patent/EP2661478A2/de
Priority to EA201490293A priority patent/EA024291B1/ru
Priority to US13/809,904 priority patent/US9254451B2/en
Priority to CN2011800444312A priority patent/CN103261373A/zh
Publication of WO2012013177A2 publication Critical patent/WO2012013177A2/de
Publication of WO2012013177A3 publication Critical patent/WO2012013177A3/de
Publication of WO2012013177A4 publication Critical patent/WO2012013177A4/de
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/14—Evaporating with heated gases or vapours or liquids in contact with the liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid Fuels And Fuel-Associated Substances (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

Die Erfindung umfasst ein Verfahren und eine Vorrichtung mit Hilfe derer Halogenwasserstoff und Wasser aus halogensauren Biomassehydrolysaten abgetrennt werden. Kern der Erfindung ist ein evakuierter Behälter (B1), der mit einem Wärmeträger kontinuierlich beschickt wird und der in einem Teil vollständig mit dem Wärmeträger ausgefüllt ist. In diesem Verdampfungsraum wird das Biomassehydrolysat ebenfalls kontinuierlich eingebracht. Es kommt im Behälter (B1) zu einer Übertragung der Wärme vom Wärmeträger auf das Hydrolysat, wobei Halogenwasserstoff und Wasser kontinuierlich abgedampft wird. Die verbleibenden Hydrolysatpartikel werden kontinuierlich mit dem abgekühlten Wärmeträger ausgetragen und kontinuierlich vom Wärmeträger abgetrennt. Die hier beschriebene Erfindung kann auch zur Behandlung für andere Mischungen bzw. Lösungen zum Zwecke der Abdampfung verwendet werden. Grundlegend ist in Bezug auf den eingesetzten Wärmeträger: Er ist chemisch inert gegenüber den eingetragenen Stoffen.
PCT/DE2011/001423 2010-07-14 2011-07-12 Verfahren und apparatur zur abdampfung von halogenwasserstoff und wasser aus halogensauren biomassehydrolysaten Ceased WO2012013177A2 (de)

Priority Applications (4)

Application Number Priority Date Filing Date Title
EP11770676.2A EP2661478A2 (de) 2010-07-14 2011-07-12 Verfahren und apparatur zur abdampfung von halogenwasserstoff und wasser aus halogensauren biomassehydrolysaten
EA201490293A EA024291B1 (ru) 2010-07-14 2011-07-12 Способ непрерывного выпаривания галогеноводородных кислот и воды из гидролизатов биомассы
US13/809,904 US9254451B2 (en) 2010-07-14 2011-07-12 Method and apparatus for evaporating hydrogen halide and water from biomass hydrolyzates containing halogen acid
CN2011800444312A CN103261373A (zh) 2010-07-14 2011-07-12 用于从含氢卤酸的生物质水解产物中蒸发出卤化氢和水的方法和装置

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE102010027174.8 2010-07-14
DE102010027174 2010-07-14
DE102011104723.2 2011-06-15
DE102011104723A DE102011104723A1 (de) 2010-07-14 2011-06-15 Verfahren und Apparatur zur Entfernung von Halogenwasserstoffsäuren und Wasser aus halogensauren Biomassehydrolysaten

Publications (3)

Publication Number Publication Date
WO2012013177A2 WO2012013177A2 (de) 2012-02-02
WO2012013177A3 true WO2012013177A3 (de) 2012-03-22
WO2012013177A4 WO2012013177A4 (de) 2012-07-19

Family

ID=44992430

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/DE2011/001423 Ceased WO2012013177A2 (de) 2010-07-14 2011-07-12 Verfahren und apparatur zur abdampfung von halogenwasserstoff und wasser aus halogensauren biomassehydrolysaten

Country Status (6)

Country Link
US (1) US9254451B2 (de)
EP (1) EP2661478A2 (de)
CN (1) CN103261373A (de)
DE (1) DE102011104723A1 (de)
EA (1) EA024291B1 (de)
WO (1) WO2012013177A2 (de)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9115467B2 (en) 2010-08-01 2015-08-25 Virdia, Inc. Methods and systems for solvent purification
US9476106B2 (en) 2010-06-28 2016-10-25 Virdia, Inc. Methods and systems for processing a sucrose crop and sugar mixtures

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE112015005318A5 (de) 2014-11-26 2017-10-12 Green Sugar Gmbh Produktinnovationen Aus Biomasse Verfahren zur Säureführung in Hydrolyseanlagen zur sauren Hydrolyse von pflanzlichen Biomassen mittels konzentrierter Salzsäure
CA2970034C (en) * 2014-12-18 2019-09-03 Avantium Knowledge Centre B.V. Process for the production of solid saccharides from an aqueous saccharide solution
AU2016353665B2 (en) * 2015-11-09 2020-09-10 Avantium Knowledge Centre B.V. Process for the production of a saccharide product from an aqueous solution
CN107153113A (zh) * 2016-03-04 2017-09-12 北京慧荣和科技有限公司 对流式voc定量加热挥发管和对流式voc定量加热挥发装置
WO2023021432A1 (de) 2021-08-17 2023-02-23 Frank Kose Verfahren zur hydrolyse von pflanzlichen biomassen unter verwendung von halogenwasserstoffsäure, im speziellen salzsäure

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR916382A (fr) * 1943-04-08 1946-12-04 Economisch Technologish Inst O Procédé pour la récupération d'acide chlorhydrique dans l'hydrolyse de matières végétales avec de l'acide chlorhydrique concentré
US4432805A (en) * 1979-12-18 1984-02-21 Oy Tampella Ab Method for continuous saccharification of cellulose of plant raw material
US6007636A (en) * 1999-01-04 1999-12-28 Lightner; Gene E. Method to recycle an aqueous acidic liquor used for depolymerization of cellulose
DE102008064325A1 (de) * 2008-12-20 2010-07-01 Green Sugar Gmbh Enzymatisches Nachbehandlungsverfahren von Biomassehydrolysaten, welche durch Behandlung mit wässrigen Halogenwasserstoffsäuren gewonnen wurden

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE362230C (de) * 1918-10-15 1922-10-25 Erik Haegglund Dr Verfahren zum Abscheiden fluechtiger Saeuren aus waessrigen Gemischen, insbesondere von Salzsaeure aus Loesungen der Holzverzuckerung
DE845779C (de) * 1950-03-14 1955-08-01 Bergin Ag Deutsche Verfahren zur Wiedergewinnung und Nutzbarmachung von Salzsaeure und Chlorwasserstoff aus durch Hydrolyse von cellulosehaltigem Material anfallenden sauren Zuckerloesungen
US4237110A (en) * 1979-04-30 1980-12-02 The Dow Chemical Company Process for separating and recovering concentrated hydrochloric acid from the crude product obtained from the acid hydrolysis of cellulose
AU2008224486B2 (en) * 2007-03-15 2011-10-20 Hcl Cleantech Ltd. A process for the recovery of HCl from a dilute solution thereof
DE102008022242A1 (de) * 2008-05-06 2009-11-12 Green Sugar Gmbh Apparatur zur Entfernung von Halogenwasserstoffsäuren aus Biomassehydrolysaten
US9512495B2 (en) * 2011-04-07 2016-12-06 Virdia, Inc. Lignocellulose conversion processes and products

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR916382A (fr) * 1943-04-08 1946-12-04 Economisch Technologish Inst O Procédé pour la récupération d'acide chlorhydrique dans l'hydrolyse de matières végétales avec de l'acide chlorhydrique concentré
US4432805A (en) * 1979-12-18 1984-02-21 Oy Tampella Ab Method for continuous saccharification of cellulose of plant raw material
US6007636A (en) * 1999-01-04 1999-12-28 Lightner; Gene E. Method to recycle an aqueous acidic liquor used for depolymerization of cellulose
DE102008064325A1 (de) * 2008-12-20 2010-07-01 Green Sugar Gmbh Enzymatisches Nachbehandlungsverfahren von Biomassehydrolysaten, welche durch Behandlung mit wässrigen Halogenwasserstoffsäuren gewonnen wurden

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9476106B2 (en) 2010-06-28 2016-10-25 Virdia, Inc. Methods and systems for processing a sucrose crop and sugar mixtures
US10760138B2 (en) 2010-06-28 2020-09-01 Virdia, Inc. Methods and systems for processing a sucrose crop and sugar mixtures
US9115467B2 (en) 2010-08-01 2015-08-25 Virdia, Inc. Methods and systems for solvent purification
US11242650B2 (en) 2010-08-01 2022-02-08 Virdia, Llc Methods and systems for solvent purification

Also Published As

Publication number Publication date
US20130168226A1 (en) 2013-07-04
US9254451B2 (en) 2016-02-09
EA024291B1 (ru) 2016-09-30
EP2661478A2 (de) 2013-11-13
EA201490293A1 (ru) 2014-05-30
DE102011104723A1 (de) 2012-03-22
CN103261373A (zh) 2013-08-21
WO2012013177A4 (de) 2012-07-19
WO2012013177A2 (de) 2012-02-02

Similar Documents

Publication Publication Date Title
JO3212B1 (ar) طريقة وجهاز لتوفير مياه ذات جودة ميكروبيولوجية وتبلور عالي لتبريد العمليات الصناعية وبتكلفة منخفضة، للمياه التي تأتي من خزانات مياه عمالقة
WO2008093787A1 (ja) 基板処理装置およびパーティクル付着防止方法
WO2009079636A3 (en) Methods and apparatuses for controlling contamination of substrates
TN2012000404A1 (en) Water treatment process
PE20131026A1 (es) Proceso para la recuperacion de compuestos oleaginosos a partir de biomasa
JP2013537035A5 (de)
WO2011104556A3 (en) Improved heat storage system
EA026677B9 (ru) Способ и система для накопления тепловой энергии
JP2017518798A5 (de)
BR112013014643A2 (pt) método de tratamento de água de torre de resfriamento e dispositivo de eletrólise para o tratamento de água
WO2008152749A1 (ja) 造水装置及び造水方法
WO2011072171A3 (en) System and method for removing volatile vapors from containers
TW200942491A (en) A process for removing aluminum and other metal chlorides from chlorosilanes
WO2011091950A3 (en) Process and plant for cooling sulfuric acid
WO2010043698A3 (en) Treatment of liquid wastes containing heavy metals
EA201490293A1 (ru) Способ и аппаратура для выпаривания галогеноводорода и воды из гидролизатов биомассы, содержащих галогенокислоту
MY193738A (en) Apparatus and process for treating chlorosilane-containing liquids
JP2010160231A5 (de)
EP4481769A3 (de) Partikelstrahlbehandlung
JP2016518242A5 (de)
SG157984A1 (en) Apparatus and method for improved desalination
WO2012122168A3 (en) Method and apparatus for accumulating, storing, and releasing thermal energy and humidity
MY180668A (en) Method and device for preparing high temperature water vapour rich in active particles using plasma
RU2010104251A (ru) Способ отгонки растворителя из пороховых элементов сферического пороха
WO2009007692A3 (en) Methods and apparatuses relating to cell culture media

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 11770676

Country of ref document: EP

Kind code of ref document: A2

WWE Wipo information: entry into national phase

Ref document number: 2011770676

Country of ref document: EP

WWE Wipo information: entry into national phase

Ref document number: 13809904

Country of ref document: US

WWE Wipo information: entry into national phase

Ref document number: 201490293

Country of ref document: EA