WO2012102570A2 - Composition pour comprimé édulcorant et son procédé de préparation - Google Patents

Composition pour comprimé édulcorant et son procédé de préparation Download PDF

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Publication number
WO2012102570A2
WO2012102570A2 PCT/KR2012/000630 KR2012000630W WO2012102570A2 WO 2012102570 A2 WO2012102570 A2 WO 2012102570A2 KR 2012000630 W KR2012000630 W KR 2012000630W WO 2012102570 A2 WO2012102570 A2 WO 2012102570A2
Authority
WO
WIPO (PCT)
Prior art keywords
tablet
sweetener composition
parts
weight
rebaudioside
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/KR2012/000630
Other languages
English (en)
Korean (ko)
Other versions
WO2012102570A3 (fr
Inventor
이승우
임재민
임지웅
김종훈
손정덕
이정옥
오유나
박동현
김경락
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yang Ji Chemical Co Ltd
Original Assignee
Yang Ji Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yang Ji Chemical Co Ltd filed Critical Yang Ji Chemical Co Ltd
Publication of WO2012102570A2 publication Critical patent/WO2012102570A2/fr
Publication of WO2012102570A3 publication Critical patent/WO2012102570A3/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00—Shaping or working of foodstuffs characterised by the products
    • A23P10/20—Agglomerating; Granulating; Tabletting
    • A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture

Definitions

  • the present invention relates to a sugar substitute tablet type sweetener composition useful in the field of dietary supplements, and a method of manufacturing the same.
  • the composition of the present invention can be added to beverages and other foods commonly ingested in daily life such as coffee, tea and tea, and contains ribioside A as a sweetness component.
  • the present invention relates to a melt-compressing tablet-type sweetener composition whose hardness is suitably adjusted so as to quickly disintegrate and dissolve in drinking water, and a method for producing the same.
  • Sugar is the most widely used sweetener for sweet taste.
  • high calories and intrinsic properties of sugar cause diabetes, obesity, striatum and other diseases. Therefore, sugar is not suitable for ingestion by patients suffering from the above diseases. Therefore, various low-calorie functional sweeteners have been developed as sugar substitutes.
  • saccharin, aspartame, sucralose, stevioside and acesulfame are used as various food additives to date.
  • These functional sweeteners exhibit 180-600 times higher sweetness than sugar. Therefore, the sweetener can provide a sweet taste of sugar substitute in a small amount and at the same time has the advantage of preventing the rise of blood sugar and low calories. However, most of these functional sweeteners have a characteristic bitter taste, which has a disadvantage that the aftertaste is not refreshing.
  • compositions including various types of sugars such as xyl, palatinose, glucose, maltodextrin, oligosaccharides, or other additives such as fragrances, sodium chloride, etc.
  • sugars such as xyl, palatinose, glucose, maltodextrin, oligosaccharides, or other additives such as fragrances, sodium chloride, etc.
  • the functional sweetener may be browned when stored for a long time, and there is a problem in that storage property is degraded due to decomposition or deterioration by moisture.
  • the price of the added sugar is relatively high, the price competitiveness is also lowered.
  • sugar substitute sweeteners have been developed in most cases in granular or powdery compositions. However, when used by the general public, it is possible to take an aliquot more than necessary because of its morphological characteristics. Thus, a certain amount of sweetener is produced, with a sugar content of about a tablespoon of sugar, while providing a sufficient sweetness effect. There is a need for development as a suitable composition that can be represented.
  • the present invention has been made to solve the above problems, while maintaining a sweetness and taste similar to sugar, while showing a lower calorie than sugar, there is no concern about various diseases such as diabetes, obesity, stratification, and solubility. It is an object of the present invention to provide a sugar-refining tablet sweetener composition that has a short time, excellent shelf life and easy usage control.
  • an object of the present invention is to provide a method for producing a sugar-refining tablet sweetener composition.
  • the tablet-type sweetener composition of the present invention is characterized by including rebaudioside A in order to achieve the object as described above.
  • the tablet-type sweetener composition of the present invention is Xyl, Maltose, Malty, Manny, Palatinos, Erysri, Trehalose, Glucose, Solbi, Maltotextrin, Dextrose, Lactose, Oligo It may further comprise a sugar selected from the group consisting of saccharides, and combinations thereof.
  • the tablet-type sweetener composition of the present invention is microcrystalline cellulose, starch glycolate or frium, crospobic £ ⁇ ⁇ seabomer, carboxymethyl 3 ⁇ 4 sen? .9, vidon, hydroxypropyl cellulose It may further comprise a disintegrant selected from the group consisting of polyethylene oxide, povidone, calciginate, croscarmellose, sodium stearyl fumarate, and combinations thereof.
  • the amount of the disintegrant further included is preferably 8 to 80 parts by weight per 100 parts by weight of rebaudioside A.
  • the tablet-type sweetener composition of the present invention is a magnesium stearate, calcium stearate It may further comprise a lubricant selected from the group consisting of arate, zinc stearate, polyethylene glycol, glyceryl behanate, glyceryl palmitostearate, sodium lauryl sulfate, stearic acid, talc, and combinations thereof. have.
  • the amount of the additionally included lubricant is preferably 2 to 48 parts by weight per 100 parts by weight of rebaudioside A.
  • An edge of the disc portion may be larger than an edge of the curved portion.
  • the tablet-type sweetener composition of the present invention preferably has a disintegration rate of 1 to
  • the tablet-type sweetener composition of the present invention is preferably lower in calories per unit weight than sugar.
  • microcrystalline cellulose sodium starch glycolate, crospovidone, gelatin, starch, carbomer, carboxymethyl cellulose, copovidone, hydroxypropylcellose, polyethylene oxide, povidone, calcium alginate, cross Disintegrants selected from the group consisting of carmellose, sodium stearyl fumarate, and combinations thereof
  • glidants selected from the group consisting of: calcium stearate, zinc stearate, polyethylene glycol, glyceryl behenate, glyceryl palmitostearate, sodium lauryl sulfate, stearic acid, talc, and mixtures thereof Adding with, and
  • the tablet-type sweetener composition may include 100 parts by weight of rebaudioside A, 200 to 1000 parts by weight, 8 to 80 parts by weight of disintegrant, and 2 to 48 parts by weight of lubricant.
  • the tablet-type sweetener composition of the present invention has no sweet aftertaste and has a sweetness similar to sugar. And, while maintaining sweetness, it shows lower calories than sugar, so it is possible to mark 0 calories (less than 5 kcal per unit packaging). In addition, there is no concern about various diseases such as diabetes, obesity and tooth decay caused by excessive intake of sugar. In addition, it quickly disintegrates and dissolves in drinking water, thereby improving user convenience. Furthermore, due to the appropriate hardness, the shape can be maintained during production and distribution, and mass handling is possible. In addition, it has a low cost of raw materials due to less expensive ingredients, and has excellent storage properties due to the low possibility of browning and alteration.
  • 1 is a schematic view showing the form of a tablet.
  • Figure 2 is a photograph measuring the disintegration rate of the tablet.
  • the term 'dissolved compression molded' means a compression molded product that exhibits sufficient disintegration and solubility by drinking water and at the same time has an appropriate hardness.
  • the term 'appropriate hardness' means that the It means that the mold has sufficient hardness to prevent collapse.
  • the tablet-type sweetener composition provided in the present invention essentially contains rebaudioside A as a functional sweetener having a sugar content of about 350 to 450 times that of sugar. This rebaudioside A is responsible for the sweet taste expression in the tablet sweetener composition of the present invention.
  • Ribaudioside A is one of the components of the stevia natural extract, steviol glycoside. Other components of steviol glycosides include stevioside and rebaudioside C. However, rebaudioside A has the highest sugar content, less bitterness and sourness than other ingredients, and is the most delicious sweetener. to be.
  • various kinds of sugars for example, xyl, maltose, malty, manny, palatinose and erys It is preferable to further include one or two or more sugars selected from the group consisting of trehalose, glucose, sorbitol, maltodextrin, dextrose, lactose and oligosaccharides.
  • the amount of sugar added is preferably 200 to 1000 parts by weight per 100 parts by weight of the rebaudioside A. If the amount of added sugar is less than 200 parts by weight, there is a disadvantage in that the moldability is easily broken. On the contrary, if the content exceeds 1000 parts by weight, the tableting property and the fluidity are lowered during compression, and thus there is a problem that tableting surface is uneven or a tableting obstacle such as sticking phenomenon occurs.
  • the tablet-type sweetener composition of the present invention is a microcrystalline cellulose, starch sodium glycolate, crospovidone, gelatin, starch, carbomer, carboxymethyl cellulose, copovidone, hydroxy as disintegrant and binder. It is preferable to further include one or two or more disintegrants selected from propylcellulose, polyethylene oxide, povidone, calcium alginate, croscarmellose, sodium stearyl fumarate.
  • the amount of the disintegrant added is preferably 8 to 80 parts by weight per 100 parts by weight of the rebaudioside A. If the amount of the disintegrant added is less than 8 parts by weight, the adhesiveness of the sugar is increased, there is a disadvantage that the sticking phenomenon is attached to the punch (punch) surface. On the contrary, if the amount exceeds 80 parts by weight, the bonding strength is good, but the disintegration is delayed, resulting in a poor product quality.
  • the tablet-type sweetener composition of the present invention as a lubricant, magnesium stearate, kale stearate, zinc stearate, polyethylene glycol, glyceryl behenate, glyceryl palmitostearate, sodium lauryl sulfide It is preferable to further include one or more lubricants selected from pate, stearic acid and talc.
  • the amount of the lubricant added is 2 to 48 parts by weight per 100 parts by weight of the rebaudioside A. If the amount of the added lubricant is less than 2 parts by weight, there is a disadvantage in that the occurrence of sticking phenomenon increases. On the contrary, if the content exceeds 48 parts by weight, there is a problem in that the tabletability is lowered and a tableting disorder such as a tablet breaking occurs.
  • the sweetener composition is required to disintegrate quickly in drinking water.
  • the rate of disintegration of tablets generally depends greatly on the shape of the tablet. Therefore, the tablet-type sweetener composition of the present invention is particularly formed as a circular or elliptical disk portion, and a curved portion integrally formed on the upper and lower surfaces of the disk portion, as shown in FIG. And, it is preferable that the edge of the disc portion is made larger than the edge of the curved portion.
  • the tablet-type sweetener composition of the present invention is completely disintegrated within 20 seconds, preferably within 10 seconds in drinking water.
  • the method for preparing a tablet sweetener composition of the present invention preferably includes the following steps:
  • ⁇ 52> A group consisting of xili, maltose, malttle, manny, palatinose, erysri, trehalose, glucose, sorbetle, maltodextrin, textose, lactose, oligosaccharides, and mixtures thereof.
  • Sugars selected from;
  • microcrystalline cellulose sodium starch glycolate, crospovidone, gelatin, starch, carbomer, carboxymethyl cellulose, copovidone, hydroxypropylcellose, polyethylene oxide, povidone, calcium alginate, croscarmellose Disintegrants selected from the group consisting of os, sodium stearyl fumarate, and combinations thereof
  • the content ratio of each component constituting the tablet-type sweetener composition is 100 parts by weight of rebaudioside A, 200 to 1000 parts by weight, 8 to 80 parts by weight of disintegrant, and 2 to 48 parts by weight of lubricant. Particularly preferred is denial.
  • the tablet-type sweetener composition of the present invention may exhibit similar sweetness to sugar while using calories per unit weight lower than sugar by using Rebaudioside A and other sugars instead of sugar. And because of its rapid disintegration and solubility, it is very useful as a sweetener that can be added to beverages such as coffee, tea, and other foods.
  • the tablet-type sweetener composition of the present invention has the advantage that the possibility of raising the blood sugar, obesity or stratification due to the use of sugar is very low. And, with the appropriate hardness, mass production and distribution are possible. In addition, it has a tablet form has the advantage that the convenience of the user is significantly improved as the amount of use is easy to adjust.
  • rebaudioside A 20.0 g of rebaudioside A, 15.0 g of D-manny and 61.0 g of palatinose were sequentially added to the mixer.
  • 2.5 g of sodium starch glycolate was added thereto and mixed for 30 minutes.
  • 1.5 g of magnesium stearate was filtered through a 60 mesh sieve, added to a mixer, mixed for 5 minutes, and then compressed into tablet form of FIG. 1.
  • Example 2 a tablet-type sweetener tank of the present invention was prepared by varying the composition as shown in Table 1 below.
  • the disintegration rate of the tablet sweetener composition prepared by the method of Examples 1 to 7 was measured.
  • the disintegration temperature was 80 ° C., disintegrated in deionized water, and completely disintegrated within 10 seconds as shown in FIG. 2.
  • the hardness and the friability of the tablet-type sweetener compositions prepared by the methods of Examples 1 to 7 were measured. Hardness measurement is Schleuniger tablet hardness tester (Pharmatest, Germany) was used to measure the results of the actual values 0.5 to 2.5). In addition, the wear test was measured using a Roche wear tester (Pharmatest, Germany), and less than 0.1% by weight relative to the test weight is 0.5% by weight or less generally required in the technical field to which the present invention belongs Met the requirements of. Accordingly, the tablet-type sweetener composition of the present invention was found to be an excellent formulation without the risk of breakage during manufacture or transportation.
  • the similarity with sugar was converted to 100 points after scoring, with the most similar taste as 5 points and the least similar taste as 1 point by 5 point scale method.
  • all of the tablet-type sweetener compositions of the present invention were close to the sweetness of the sugar by more than 80% even by the amount of 1/50 of the sugar, it was confirmed that the same level of similarity.

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Medicinal Preparation (AREA)
  • Seasonings (AREA)

Abstract

La présente invention concerne une composition pour comprimé édulcorant contenant un édulcorant fonctionnel qui est un substitut du sucre, ainsi que son procédé de préparation. L'invention concerne, plus précisément, une composition pour comprimé édulcorant à faible teneur en calories et son procédé de préparation, ladite composition pour comprimé édulcorant à faible teneur en calories présentant un pouvoir sucrant équivalent à celui du sucre, un goût sucré très agréable et étant caractérisée par une vitesse de dissolution rapide et par une bonne stabilité.
PCT/KR2012/000630 2011-01-27 2012-01-27 Composition pour comprimé édulcorant et son procédé de préparation Ceased WO2012102570A2 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR10-2011-0008317 2011-01-27
KR1020110008317A KR20120093461A (ko) 2011-01-27 2011-01-27 정제형 감미료 조성물 및 그 제조방법

Publications (2)

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WO2012102570A2 true WO2012102570A2 (fr) 2012-08-02
WO2012102570A3 WO2012102570A3 (fr) 2012-11-29

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PCT/KR2012/000630 Ceased WO2012102570A2 (fr) 2011-01-27 2012-01-27 Composition pour comprimé édulcorant et son procédé de préparation

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WO (1) WO2012102570A2 (fr)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2687028T3 (es) * 2012-12-20 2018-10-23 Cargill, Incorporated Composición que comprende glicósido de esteviol y maltosa

Family Cites Families (3)

* Cited by examiner, † Cited by third party
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UA74141C2 (uk) * 1998-12-09 2005-11-15 Дж.Д. Сірл Енд Ко. Фармацевтична композиція на основі тонкоподрібненого еплеренону (варіанти), спосіб її одержання та спосіб лікування розладів, опосередкованих альдостероном (варіанти)
US8993027B2 (en) * 2005-11-23 2015-03-31 The Coca-Cola Company Natural high-potency tabletop sweetener compositions with improved temporal and/or flavor profile, methods for their formulation, and uses
CN101854814B (zh) * 2007-11-12 2013-07-31 三荣源有限公司 改善甜叶菊提取物甜味的方法

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WO2012102570A3 (fr) 2012-11-29
KR20120093461A (ko) 2012-08-23

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