WO2012163894A3 - Verfahren zur herstellung von polyisocyanaten - Google Patents

Verfahren zur herstellung von polyisocyanaten Download PDF

Info

Publication number
WO2012163894A3
WO2012163894A3 PCT/EP2012/059993 EP2012059993W WO2012163894A3 WO 2012163894 A3 WO2012163894 A3 WO 2012163894A3 EP 2012059993 W EP2012059993 W EP 2012059993W WO 2012163894 A3 WO2012163894 A3 WO 2012163894A3
Authority
WO
WIPO (PCT)
Prior art keywords
polyisocyanates
diisocyanates
provides
stages
unutilizable
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2012/059993
Other languages
English (en)
French (fr)
Other versions
WO2012163894A2 (de
Inventor
Torsten Mattke
Matthias KLÖTZER
Robert Baumann
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to JP2014513151A priority Critical patent/JP2014524892A/ja
Priority to EP12726063.6A priority patent/EP2714649A2/de
Priority to CN201280027059.9A priority patent/CN103596920A/zh
Publication of WO2012163894A2 publication Critical patent/WO2012163894A2/de
Publication of WO2012163894A3 publication Critical patent/WO2012163894A3/de
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/18—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas
    • C07C273/1854—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety
    • C07C273/1863—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety from urea
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/06—Preparation of derivatives of isocyanic acid from or via ureas

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Gegenstand der Erfindung ist ein mehrstufiges Verfahren zur kontinuierlichen Herstellung von organischen Polyisocyanaten, vorzugsweise von Diisocyanaten, besonders bevorzugt von aliphatischen oder cycloaliphatischen Diisocyanaten, durch Umsetzung der entsprechenden organischen Polyamine mit Kohlensäurederivaten und Alkoholen in niedermolekulare monomere Polyurethane und deren Spaltung. Ein weiterer Gegenstand der Erfindung ist ein zugehöriges Herstellverfahren, bei dem an bestimmten Reaktionsstufen die hergestellten Polyisocyanate und unverwertbaren Rückstände abgetrennt und wiederverwendbare Neben- und Zwischenprodukte in Vorstufen zurückgeführt werden.
PCT/EP2012/059993 2011-05-30 2012-05-29 Verfahren zur herstellung von polyisocyanaten Ceased WO2012163894A2 (de)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP2014513151A JP2014524892A (ja) 2011-05-30 2012-05-29 ポリイソシアネートの製造法
EP12726063.6A EP2714649A2 (de) 2011-05-30 2012-05-29 Verfahren zur herstellung von polyisocyanaten
CN201280027059.9A CN103596920A (zh) 2011-05-30 2012-05-29 制备多异氰酸酯的方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP11168028 2011-05-30
EP11168028.6 2011-05-30

Publications (2)

Publication Number Publication Date
WO2012163894A2 WO2012163894A2 (de) 2012-12-06
WO2012163894A3 true WO2012163894A3 (de) 2013-07-18

Family

ID=46210222

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2012/059993 Ceased WO2012163894A2 (de) 2011-05-30 2012-05-29 Verfahren zur herstellung von polyisocyanaten

Country Status (4)

Country Link
EP (1) EP2714649A2 (de)
JP (1) JP2014524892A (de)
CN (1) CN103596920A (de)
WO (1) WO2012163894A2 (de)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8816126B2 (en) 2011-09-02 2014-08-26 Basf Se Process for preparing isocyanates
WO2016156188A1 (de) 2015-03-31 2016-10-06 Basf Se Verfahren zur herstellung von isocyanaten durch carbamatspaltung

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0028338B1 (de) * 1979-10-20 1984-01-18 BASF Aktiengesellschaft Verfahren zur Herstellung von aromatischen Di- und/oder Polyisocyanaten
EP0566925A2 (de) * 1992-04-21 1993-10-27 BASF Aktiengesellschaft Mehrstufiges Verfahren zur kontinuierlichen Herstellung von organischen Polyisocyanaten
WO1998054129A1 (en) * 1997-05-31 1998-12-03 Huntsman Ici Chemicals Llc Method for the preparation of organic isocyanates
WO2007082818A1 (de) * 2006-01-13 2007-07-26 Basf Se Verfahren zur herstellung von isocyanaten
WO2011015541A1 (de) * 2009-08-04 2011-02-10 Basf Se Verfahren zur herstellung von isocyanaten

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1359032A (en) * 1971-06-01 1974-07-03 Quimco Gmbh Process for preparing organic mono-and polyisocyanates
DE2917490A1 (de) 1979-04-30 1980-11-13 Basf Ag Verfahren zur herstellung von aliphatischen und cycloaliphatischen di- und polyurethanen
DE2943480A1 (de) 1979-10-27 1981-05-07 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von n,o-disubstituierten urethanen, sowie ihre verwendung als ausgangsmaterial zur herstellung von isocyanaten
DE3311514A1 (de) * 1983-03-30 1984-10-25 Basf Farben + Fasern Ag, 2000 Hamburg Herstellung von harnstoffkondensationprodukten und deren verwendung
DE3314788A1 (de) 1983-04-23 1984-10-25 Basf Ag, 6700 Ludwigshafen Mehrstufenverfahren zur herstellung von hexamethylendiisocyanat-1,6 und/oder isomeren aliphatischen diisocyanaten mit 6 kohlenstoffatomen im alkylenrest
US4883908A (en) * 1989-02-02 1989-11-28 Arco Chemical Technology, Inc. Process for the preparation of aromatic isocyanates from dialkyl ureas using an organic sulfonic acid promoter

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0028338B1 (de) * 1979-10-20 1984-01-18 BASF Aktiengesellschaft Verfahren zur Herstellung von aromatischen Di- und/oder Polyisocyanaten
EP0566925A2 (de) * 1992-04-21 1993-10-27 BASF Aktiengesellschaft Mehrstufiges Verfahren zur kontinuierlichen Herstellung von organischen Polyisocyanaten
WO1998054129A1 (en) * 1997-05-31 1998-12-03 Huntsman Ici Chemicals Llc Method for the preparation of organic isocyanates
WO2007082818A1 (de) * 2006-01-13 2007-07-26 Basf Se Verfahren zur herstellung von isocyanaten
WO2011015541A1 (de) * 2009-08-04 2011-02-10 Basf Se Verfahren zur herstellung von isocyanaten

Also Published As

Publication number Publication date
EP2714649A2 (de) 2014-04-09
CN103596920A (zh) 2014-02-19
WO2012163894A2 (de) 2012-12-06
JP2014524892A (ja) 2014-09-25

Similar Documents

Publication Publication Date Title
WO2010149544A3 (en) Process for the production of isocyanates, preferably diisocyanates and polyisocyanates with solvent recirculation
WO2008120645A1 (ja) カルバミン酸エステルおよび芳香族ヒドロキシ化合物を含む組成物を用いるイソシアネートの製造方法、ならびにカルバミン酸エステル移送用および貯蔵用組成物
WO2013060614A9 (de) Farbstabile härterzusammensetzungen enthaltend polyisocyanate (cyclo)aliphatischer diisocyanate
WO2011036062A3 (de) Verfahren zur herstellung von isocyanaten
MX364734B (es) Procesos de recuperación de caucho de briquetas envejecidas y briquetas envejecidas que contienen materia vegetal de plantas no hevea.
MX2013013144A (es) Metodo para la produccion de un dimero mdi.
SG150460A1 (en) Process for the preparation of polyols
WO2009066616A1 (ja) イソシアネートおよび芳香族ヒドロキシ化合物の製造方法
MX2012013922A (es) Procedimientos de baja energia para la recuperacion de alcohol.
ATE512130T1 (de) Verfahren zur herstellung von isocyanaten
WO2009080743A3 (en) Plants with increased yield (ko nue)
WO2013079481A3 (de) Verfahren zur herstellung von polyisocyanaten und deren verwendung
WO2011087316A3 (ko) 테트라졸 메탄설폰산 염의 제조방법 및 이에 사용되는 신규 화합물
WO2011004402A3 (en) Improved process for the preparation of ambrisentan and novel intermediates thereof
AU2012358475A8 (en) An inhalable medicament comprising tiotropium
WO2012137152A3 (fr) Procede de preparation de composes formamides
WO2012118780A3 (en) Preparation of peptide mixtures by protease catalysis designed to provide useful biological and physical properties
WO2012114357A8 (en) Process for preparing hyperbranched polyesters
WO2013011296A3 (en) Separation process
MX2018012194A (es) Proceso para preparar diisocianatos de xilileno (xdi).
WO2013064219A3 (de) Qualitätstest für polymerisationsfähige milchsäure und verfahren zu deren herstellung
WO2012163894A3 (de) Verfahren zur herstellung von polyisocyanaten
MX2015001807A (es) Proceso para la producción de espumas de polímeros que comprenden grupos imida.
WO2013127814A3 (de) Verfahren zur herstellung von polymerhartschäumen
WO2011102640A3 (en) Method for preparing sitagliptin and amine salt intermediates used therein

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 12726063

Country of ref document: EP

Kind code of ref document: A2

ENP Entry into the national phase

Ref document number: 2014513151

Country of ref document: JP

Kind code of ref document: A