WO2015019013A3 - Zéolithes à porosité hiérarchisée - Google Patents

Zéolithes à porosité hiérarchisée Download PDF

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Publication number
WO2015019013A3
WO2015019013A3 PCT/FR2014/052028 FR2014052028W WO2015019013A3 WO 2015019013 A3 WO2015019013 A3 WO 2015019013A3 FR 2014052028 W FR2014052028 W FR 2014052028W WO 2015019013 A3 WO2015019013 A3 WO 2015019013A3
Authority
WO
WIPO (PCT)
Prior art keywords
zeolites
hierarchical porosity
present
concerns
hierarchical
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/FR2014/052028
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English (en)
Other versions
WO2015019013A2 (fr
Inventor
Serge Nicolas
Karine LOPEZ
Cécile LUTZ
Ludivine Bouvier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Carbonisation et Charbons Actifs CECA SA
Original Assignee
Carbonisation et Charbons Actifs CECA SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to EP14790175.5A priority Critical patent/EP3030521A2/fr
Priority to CN201480017464.1A priority patent/CN105050954B/zh
Priority to AU2014304409A priority patent/AU2014304409B2/en
Priority to UAA201511893A priority patent/UA119749C2/uk
Priority to CA2909798A priority patent/CA2909798C/fr
Priority to SG11201508819WA priority patent/SG11201508819WA/en
Priority to EA201592092A priority patent/EA034181B1/ru
Priority to US14/889,353 priority patent/US10106429B2/en
Priority to KR1020157033502A priority patent/KR101800526B1/ko
Application filed by Carbonisation et Charbons Actifs CECA SA filed Critical Carbonisation et Charbons Actifs CECA SA
Priority to JP2016520731A priority patent/JP6183631B2/ja
Priority to BR112015027251-7A priority patent/BR112015027251B1/pt
Publication of WO2015019013A2 publication Critical patent/WO2015019013A2/fr
Publication of WO2015019013A3 publication Critical patent/WO2015019013A3/fr
Priority to ZA2015/08079A priority patent/ZA201508079B/en
Anticipated expiration legal-status Critical
Priority to US16/112,103 priority patent/US10773965B2/en
Ceased legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/14—Type A
    • C01B39/145—Type A using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/20—Faujasite type, e.g. type X or Y
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/20—Faujasite type, e.g. type X or Y
    • C01B39/22—Type X
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C01P2006/17—Pore diameter distribution

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

La présente invention concerne des zéolithes à porosité hiérarchisée de rapport molaire Si/AI compris entre 1 et 1,4, bornes incluses, dont le diamètre moyen en nombre est compris entre 0,1 μm et 20 μm, de cristallinité contrôlée et optimale, et présentant une mésoporosité telle que la surface externe mésoporeuse est comprise entre 40 m2. g-1 et 400 m2.g-1. La présente invention concerne également le procédé de préparation des dites zéolithes à porosité hiérarchisée.
PCT/FR2014/052028 2013-08-05 2014-08-04 Zéolithes à porosité hiérarchisée Ceased WO2015019013A2 (fr)

Priority Applications (13)

Application Number Priority Date Filing Date Title
KR1020157033502A KR101800526B1 (ko) 2013-08-05 2014-08-04 다단기공성을 갖는 제올라이트
AU2014304409A AU2014304409B2 (en) 2013-08-05 2014-08-04 Zeolites with hierarchical porosity
UAA201511893A UA119749C2 (uk) 2013-08-05 2014-08-04 Цеоліти із заданою пористістю
CA2909798A CA2909798C (fr) 2013-08-05 2014-08-04 Zeolithes a porosite hierarchisee
SG11201508819WA SG11201508819WA (en) 2013-08-05 2014-08-04 Zeolites with hierarchical porosity
EA201592092A EA034181B1 (ru) 2013-08-05 2014-08-04 Цеолиты с заданной пористостью
US14/889,353 US10106429B2 (en) 2013-08-05 2014-08-04 Method of making zeolites with hierarchical porosity
EP14790175.5A EP3030521A2 (fr) 2013-08-05 2014-08-04 Zéolithes à porosité hiérarchisée
JP2016520731A JP6183631B2 (ja) 2013-08-05 2014-08-04 階層的多孔性を備えるゼオライト
CN201480017464.1A CN105050954B (zh) 2013-08-05 2014-08-04 具有分级多孔性的沸石
BR112015027251-7A BR112015027251B1 (pt) 2013-08-05 2014-08-04 Zeólitas com porosidade hierarquizada e processo de preparação de uma zeólita
ZA2015/08079A ZA201508079B (en) 2013-08-05 2015-10-30 Zeolites with hierarchical porosity
US16/112,103 US10773965B2 (en) 2013-08-05 2018-08-24 Zeolites with hierarchical porosity

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR13.57762 2013-08-05
FR1357762A FR3009300B1 (fr) 2013-08-05 2013-08-05 Zeolithes a porosite hierarchisee

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US14/889,353 A-371-Of-International US10106429B2 (en) 2013-08-05 2014-08-04 Method of making zeolites with hierarchical porosity
US16/112,103 Continuation US10773965B2 (en) 2013-08-05 2018-08-24 Zeolites with hierarchical porosity

Publications (2)

Publication Number Publication Date
WO2015019013A2 WO2015019013A2 (fr) 2015-02-12
WO2015019013A3 true WO2015019013A3 (fr) 2015-04-09

Family

ID=50064712

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR2014/052028 Ceased WO2015019013A2 (fr) 2013-08-05 2014-08-04 Zéolithes à porosité hiérarchisée

Country Status (15)

Country Link
US (2) US10106429B2 (fr)
EP (1) EP3030521A2 (fr)
JP (1) JP6183631B2 (fr)
KR (1) KR101800526B1 (fr)
CN (1) CN105050954B (fr)
AU (1) AU2014304409B2 (fr)
BR (1) BR112015027251B1 (fr)
CA (1) CA2909798C (fr)
EA (1) EA034181B1 (fr)
FR (1) FR3009300B1 (fr)
SG (1) SG11201508819WA (fr)
TW (1) TWI544961B (fr)
UA (1) UA119749C2 (fr)
WO (1) WO2015019013A2 (fr)
ZA (1) ZA201508079B (fr)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3010071B1 (fr) * 2013-09-02 2015-08-21 Ceca Sa Zeolithes a porosite hierarchisee
FR3025789B1 (fr) * 2014-09-12 2018-04-20 Arkema France Agregats de nanocristaux de zeolithes
CN104477937A (zh) * 2014-12-05 2015-04-01 上海绿强新材料有限公司 介孔x型分子筛、基于该分子筛的吸附剂及其制备与应用
FR3032130B1 (fr) * 2015-02-02 2019-12-27 Arkema France Adsorbants zeolithiques de haute surface externe, leur procede de preparation et leurs utilisations
FR3032131B1 (fr) * 2015-02-02 2019-12-27 Arkema France Adsorbants zeolithiques de haute surface externe, leur procede de preparation et leurs utilisations
CN107814393B (zh) * 2017-12-04 2019-12-27 上海绿强新材料有限公司 一种快速晶化合成emt分子筛的方法
FR3076828A1 (fr) * 2018-01-15 2019-07-19 Arkema France Procede de preparation de zeolithes en continu au moyen d'ultrasons
US11007511B2 (en) * 2018-05-08 2021-05-18 Saudi Arabian Oil Company Methods for the synthesis of tunable mesoporous zeolites
WO2019215751A1 (fr) * 2018-05-11 2019-11-14 INDIAN INSTITUTE OF TECHNOLOGY MADRAS (IIT Madras) Cristal de zéolite ordonné et hiérarchiquement poreux et son procédé de préparation
US10995107B2 (en) * 2018-08-13 2021-05-04 Saudi Arabian Oil Company Organosilane templates and methods for the synthesis of mesoporous zeolites
KR101994765B1 (ko) 2018-09-21 2019-07-01 에스케이이노베이션 주식회사 계층화된 제올라이트 및 이의 제조방법
WO2020261795A1 (fr) * 2019-06-27 2020-12-30 公益財団法人地球環境産業技術研究機構 Corps composite de film de zéolite, son procédé de production et procédé de séparation de fluide
FR3112289B1 (fr) 2020-07-10 2022-07-22 Arkema France Purification de liquides aromatiques
US20230211327A1 (en) * 2020-08-28 2023-07-06 Tosoh Corporation Cha-type zeolite and method for producing the same
CN111960430B (zh) * 2020-09-01 2022-04-01 常州工学院 一种高结晶度多级孔lsx沸石分子筛的合成方法与应用
IT202000027390A1 (it) * 2020-11-16 2022-05-16 Getters Spa Antiviral composition comprising modified zeolites
CN113816765A (zh) * 2021-09-25 2021-12-21 深圳职业技术学院 沸石吸音材料及其制备方法和用途
FR3127844A1 (fr) 2021-10-01 2023-04-07 Arkema France Électrolyte solide
CN115974097B (zh) * 2023-02-17 2023-12-19 四川轻化工大学 一种分子筛及其在降低白酒中杂醛含量中的应用
FR3146137A1 (fr) 2023-02-28 2024-08-30 Arkema France Purification d’oxygène électrolytique
FR3146138A1 (fr) 2023-02-28 2024-08-30 Arkema France Purification d’hydrogène électrolytique

Citations (3)

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Publication number Priority date Publication date Assignee Title
EP0364352A1 (fr) * 1988-10-10 1990-04-18 Societe Nationale Elf Aquitaine Procédé de synthèse de zéolithes appartenant à la famille structurale de la faujasite, produits obtenus et leur application en adsorption et catalyse
CN103073020A (zh) * 2012-11-08 2013-05-01 大连理工大学 一种多级孔道沸石分子筛的制备方法和应用
CN103214003A (zh) * 2013-04-09 2013-07-24 华南理工大学 一种介孔y型沸石分子筛及其制备方法

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FR2602570B1 (fr) 1986-08-11 1988-12-02 Sgn Soc Gen Tech Nouvelle Dispositif pour la realisation d'un raccordement etanche et procede de raccordement utilisant ce dispositif
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Also Published As

Publication number Publication date
JP2016522156A (ja) 2016-07-28
UA119749C2 (uk) 2019-08-12
FR3009300A1 (fr) 2015-02-06
TWI544961B (zh) 2016-08-11
US20160137517A1 (en) 2016-05-19
AU2014304409B2 (en) 2017-03-09
WO2015019013A2 (fr) 2015-02-12
US10773965B2 (en) 2020-09-15
CA2909798A1 (fr) 2015-02-12
CN105050954B (zh) 2018-12-28
BR112015027251B1 (pt) 2021-12-07
EA201592092A1 (ru) 2016-06-30
KR101800526B1 (ko) 2017-11-22
SG11201508819WA (en) 2015-12-30
KR20160003076A (ko) 2016-01-08
CN105050954A (zh) 2015-11-11
FR3009300B1 (fr) 2022-11-25
AU2014304409A1 (en) 2015-11-12
CA2909798C (fr) 2018-01-09
US20180362354A1 (en) 2018-12-20
EP3030521A2 (fr) 2016-06-15
BR112015027251A2 (pt) 2017-07-25
ZA201508079B (en) 2017-01-25
US10106429B2 (en) 2018-10-23
EA034181B1 (ru) 2020-01-15
JP6183631B2 (ja) 2017-08-23
BR112015027251A8 (pt) 2018-02-06
TW201507776A (zh) 2015-03-01

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