WO2026052205A1 - Procédé de production d'émulsions finement divisées - Google Patents

Procédé de production d'émulsions finement divisées

Info

Publication number
WO2026052205A1
WO2026052205A1 PCT/EP2024/074609 EP2024074609W WO2026052205A1 WO 2026052205 A1 WO2026052205 A1 WO 2026052205A1 EP 2024074609 W EP2024074609 W EP 2024074609W WO 2026052205 A1 WO2026052205 A1 WO 2026052205A1
Authority
WO
WIPO (PCT)
Prior art keywords
preparation
wa12411s
valve
alkyl
group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
PCT/EP2024/074609
Other languages
German (de)
English (en)
Inventor
Frank Sandmeyer
Sebastian Prost
Christian Thaller
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wacker Chemie AG
Original Assignee
Wacker Chemie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wacker Chemie AG filed Critical Wacker Chemie AG
Priority to PCT/EP2024/074609 priority Critical patent/WO2026052205A1/fr
Publication of WO2026052205A1 publication Critical patent/WO2026052205A1/fr
Pending legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/41Emulsifying
    • B01F23/413Homogenising a raw emulsion or making monodisperse or fine emulsions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/44Mixers in which the components are pressed through slits
    • B01F25/441Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits
    • B01F25/4413Mixers in which the components are pressed through slits characterised by the configuration of the surfaces forming the slits the slits being formed between opposed conical or cylindrical surfaces
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/40Static mixers
    • B01F25/44Mixers in which the components are pressed through slits
    • B01F25/442Mixers in which the components are pressed through slits characterised by the relative position of the surfaces during operation
    • B01F25/4423Mixers in which the components are pressed through slits characterised by the relative position of the surfaces during operation the surfaces being part of a valve construction, formed by opposed members in contact, e.g. automatic positioning caused by spring pressure
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/02Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2333/00Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
    • C08J2333/04Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters
    • C08J2333/06Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters of esters containing only carbon, hydrogen, and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2383/00Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers
    • C08J2383/04Polysiloxanes
    • C08J2383/06Polysiloxanes containing silicon bound to oxygen-containing groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

L'invention concerne un procédé robuste évolutif pour la production d'émulsions aqueuses finement divisées à partir de préparations contenant des polyorganosiloxanes et un ou plusieurs monomères organiques par homogénéisation à l'aide d'un homogénéisateur haute pression équipé d'une vanne d'homogénéisation, comprenant un siège de vanne plat (1) ayant une ouverture (A), un piston de vanne (2) et une bague d'impact (3), la bague d'impact (3) étant disposée sur le siège de vanne (1) et de manière symétrique en rotation autour de son ouverture (A) et un logement de vanne entourant le siège de vanne (1), le piston de vanne (2) et la bague d'impact (3), le piston de vanne ayant une conicité conique (2') qui fait saillie dans l'ouverture (A) du siège de vanne et le piston de vanne (2) et le siège de vanne (1) étant agencés de manière symétrique en rotation et de telle sorte qu'un étranglement radial soit développé entre eux et forme un espace d'homogénéisation (B), où l'homogénéisation a lieu sous pression, suivie du vieillissement de la préparation par stockage à une température de 15 à 28 °C pendant une période d'au moins 6 semaines et homogénéisation à nouveau.
PCT/EP2024/074609 2024-09-03 2024-09-03 Procédé de production d'émulsions finement divisées Pending WO2026052205A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PCT/EP2024/074609 WO2026052205A1 (fr) 2024-09-03 2024-09-03 Procédé de production d'émulsions finement divisées

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/EP2024/074609 WO2026052205A1 (fr) 2024-09-03 2024-09-03 Procédé de production d'émulsions finement divisées

Publications (1)

Publication Number Publication Date
WO2026052205A1 true WO2026052205A1 (fr) 2026-03-12

Family

ID=92672085

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2024/074609 Pending WO2026052205A1 (fr) 2024-09-03 2024-09-03 Procédé de production d'émulsions finement divisées

Country Status (1)

Country Link
WO (1) WO2026052205A1 (fr)

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5091002A (en) 1989-04-08 1992-02-25 Th. Goldschmidt Ag Preparation for the water-repellent impregnation of porous mineral building materials
US6305836B1 (en) 1999-07-09 2001-10-23 Apv North America, Inc. Force absorbing homogenization valve
EP1195190A1 (fr) 2000-10-05 2002-04-10 Bertoli S.r.l. Soupape d'homogénéisation
EP1256611A2 (fr) 2001-05-08 2002-11-13 JSR Corporation Dispersion aqueuse et produit revêtu
EP1964605A1 (fr) * 2007-02-28 2008-09-03 Shigeo Ando Soupape d'injection d'homogénéisateur haute pression et unité de soupape d'injection de celle-ci
US7674868B2 (en) 2005-01-05 2010-03-09 Wacker Chemie Ag Copolymers containing nanoparticles
US8944673B2 (en) * 2008-01-29 2015-02-03 Tetra Laval Holdings & Finance S.A. Homogenizer valve
US20180305576A1 (en) 2015-11-24 2018-10-25 Wacker Chemie Ag Organocopolymer dispersions
US20190241749A1 (en) 2018-02-06 2019-08-08 Nippon Paint Industrial Coatings Co., Ltd. Method for producing aqueous silicone resin emulsion for preparing coating composition
US20190375938A1 (en) 2017-01-20 2019-12-12 Shin-Etsu Chemical Co., Ltd. Aqueous silicone dispersion, coating film and cosmetic
WO2021126174A1 (fr) * 2019-12-18 2021-06-24 Wacker Chemie Ag Dispersions de copolymères organiques de silicone réactifs réticulables

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5091002A (en) 1989-04-08 1992-02-25 Th. Goldschmidt Ag Preparation for the water-repellent impregnation of porous mineral building materials
US6305836B1 (en) 1999-07-09 2001-10-23 Apv North America, Inc. Force absorbing homogenization valve
EP1195190A1 (fr) 2000-10-05 2002-04-10 Bertoli S.r.l. Soupape d'homogénéisation
EP1256611A2 (fr) 2001-05-08 2002-11-13 JSR Corporation Dispersion aqueuse et produit revêtu
US7674868B2 (en) 2005-01-05 2010-03-09 Wacker Chemie Ag Copolymers containing nanoparticles
EP1964605A1 (fr) * 2007-02-28 2008-09-03 Shigeo Ando Soupape d'injection d'homogénéisateur haute pression et unité de soupape d'injection de celle-ci
US8944673B2 (en) * 2008-01-29 2015-02-03 Tetra Laval Holdings & Finance S.A. Homogenizer valve
US20180305576A1 (en) 2015-11-24 2018-10-25 Wacker Chemie Ag Organocopolymer dispersions
US20190375938A1 (en) 2017-01-20 2019-12-12 Shin-Etsu Chemical Co., Ltd. Aqueous silicone dispersion, coating film and cosmetic
US20190241749A1 (en) 2018-02-06 2019-08-08 Nippon Paint Industrial Coatings Co., Ltd. Method for producing aqueous silicone resin emulsion for preparing coating composition
WO2021126174A1 (fr) * 2019-12-18 2021-06-24 Wacker Chemie Ag Dispersions de copolymères organiques de silicone réactifs réticulables

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