YU200090A - PROCEDURE FOR OBTAINING SODIUM SILICATE - Google Patents

PROCEDURE FOR OBTAINING SODIUM SILICATE

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Publication number
YU200090A
YU200090A YU200090A YU200090A YU200090A YU 200090 A YU200090 A YU 200090A YU 200090 A YU200090 A YU 200090A YU 200090 A YU200090 A YU 200090A YU 200090 A YU200090 A YU 200090A
Authority
YU
Yugoslavia
Prior art keywords
sodium silicate
temperature
sio2
molar ratio
powdered
Prior art date
Application number
YU200090A
Other languages
Serbo-Croatian (sh)
Original Assignee
Hoechst Aktiengesellschaft
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Aktiengesellschaft filed Critical Hoechst Aktiengesellschaft
Priority to SI9012000A priority Critical patent/SI9012000A/en
Priority to HRP-2000/90A priority patent/HRP921199B1/en
Publication of YU200090A publication Critical patent/YU200090A/en

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  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

POSTUPAK ZA DOBIJANJE NATRIJUM SILIKATA, amorfni natrijum silikat sa 0,3 do 6 mas. % vode i molskim odnosom izmedju SiO2 i Na2O (1,9 do 2,8) : 1 se dobija iz rastopa stakla sa najmanje 20% mas. čvrstih materija, što se rastopina stakla i natrijumhidroksida sa molskim odnosom SiO2 : NaO (2,0 do 2,8) : 1 tretira na temperaturi od 180В°C-240В°C i pritisku od 10-30 v. Tu rastopinu izložimo u zoni sušenja sa vazduhom na temperaturi 200-300В°C 10-20s, zatim na temperaturi 90-130В°C pri čemu nastaje praškasti amorfni natrijumsilikat sa sadržajem vode (dodate pri žarenju na 700В°C) 15 do 23 mas.% i nasipnom masom od 300 g/l. Praškasti natrijev silikat se dalje tretira u koso postavljenoj aparaturi za pomeranje čvrstih materija tj. u rotacionoj cevnoj peći kroz koju prolaze dimni gasovi na temperaturi u 250-500 В°C u vremenu od 1. 60 min. Temperatura spoljneg zida rotacione peći je oko 60В°C. Dobijeni amorfni natrijum silikat se drobi pomoću mehaničke drobilice na zrna od 0,1-12 mm.PROCESS FOR OBTAINING SODIUM SILICATE, amorphous sodium silicate with 0.3 to 6 wt. % of water and the molar ratio between SiO2 and Na2O (1.9 to 2.8): 1 is obtained from a glass melt with at least 20% by weight. solids, which are a solution of glass and sodium hydroxide with a molar ratio of SiO2: NaO (2.0 to 2.8): 1 is treated at a temperature of 180V ° C-240V ° C and a pressure of 10-30 C. This solution is exposed in an air-drying zone at a temperature of 200-300V ° C for 10-20 s, then at a temperature of 90-130V ° C, whereby powdered amorphous sodium silicate with a water content (added during annealing at 700V ° C) of 15 to 23 wt. % and bulk density of 300 g / l. Powdered sodium silicate is further treated in an obliquely placed apparatus for moving solids, i. in a rotary tube furnace through which flue gases pass at a temperature of 250-500 V ° C for a period of 1. 60 min. The temperature of the outer wall of the rotary kiln is about 60V ° C. The obtained amorphous sodium silicate is crushed by means of a mechanical crusher into grains of 0.1-12 mm.

YU200090A 1989-10-25 1990-10-24 PROCEDURE FOR OBTAINING SODIUM SILICATE YU200090A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
SI9012000A SI9012000A (en) 1989-10-25 1990-10-24 Method for preparation of sodium silicates
HRP-2000/90A HRP921199B1 (en) 1989-10-25 1992-11-06 A process for the preparation of natrium silicates

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE3935464 1989-10-25

Publications (1)

Publication Number Publication Date
YU200090A true YU200090A (en) 1994-09-09

Family

ID=47470738

Family Applications (2)

Application Number Title Priority Date Filing Date
YU200190A YU200190A (en) 1989-10-25 1990-10-02 PROCEDURE FOR OBTAINING SODIUM SILICATE
YU200090A YU200090A (en) 1989-10-25 1990-10-24 PROCEDURE FOR OBTAINING SODIUM SILICATE

Family Applications Before (1)

Application Number Title Priority Date Filing Date
YU200190A YU200190A (en) 1989-10-25 1990-10-02 PROCEDURE FOR OBTAINING SODIUM SILICATE

Country Status (1)

Country Link
YU (2) YU200190A (en)

Also Published As

Publication number Publication date
YU200190A (en) 1994-09-09

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