ZA200201747B - Apparatus and methods for removing solvent residues. - Google Patents

Apparatus and methods for removing solvent residues. Download PDF

Info

Publication number: ZA200201747B
Authority: ZA; South Africa
Prior art keywords: solvent; biomass; extractor; transfer line; hot
Prior art date: 1999-09-06

Application number

ZA200201747A

Other languages

English (en)

Inventor

Stuart Corr

Paul Alan Dowdle

Robert Elliott Low

Frederick Thomas Murphy

James David Morrison

Original Assignee

Ineos Fluor Holdings Ltd

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1999-09-06

Filing date

2002-03-01

Publication date

2003-05-28

2002-03-01 Application filed by Ineos Fluor Holdings Ltd filed Critical Ineos Fluor Holdings Ltd

2003-05-28 Publication of ZA200201747B publication Critical patent/ZA200201747B/en

Links

239000002904 solvent Substances 0.000 title claims abstract description 97
238000000034 method Methods 0.000 title claims description 22
239000002028 Biomass Substances 0.000 claims abstract description 72
238000000605 extraction Methods 0.000 claims abstract description 33
238000012546 transfer Methods 0.000 claims abstract description 33
239000012530 fluid Substances 0.000 claims description 12
239000000284 extract Substances 0.000 claims description 9
238000009833 condensation Methods 0.000 claims description 5
230000005494 condensation Effects 0.000 claims description 5
230000000694 effects Effects 0.000 claims description 2
239000011877 solvent mixture Substances 0.000 claims description 2
238000002955 isolation Methods 0.000 description 8
239000000463 material Substances 0.000 description 8
LVGUZGTVOIAKKC-UHFFFAOYSA-N 1,1,1,2-tetrafluoroethane Chemical compound FCC(F)(F)F LVGUZGTVOIAKKC-UHFFFAOYSA-N 0.000 description 6
238000010438 heat treatment Methods 0.000 description 6
238000011084 recovery Methods 0.000 description 5
238000009834 vaporization Methods 0.000 description 5
238000010276 construction Methods 0.000 description 4
238000003795 desorption Methods 0.000 description 4
RWRIWBAIICGTTQ-UHFFFAOYSA-N difluoromethane Chemical compound FCF RWRIWBAIICGTTQ-UHFFFAOYSA-N 0.000 description 4
NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 description 4
239000007788 liquid Substances 0.000 description 4
239000013557 residual solvent Substances 0.000 description 4
230000005484 gravity Effects 0.000 description 3
150000005828 hydrofluoroalkanes Chemical class 0.000 description 3
MSSNHSVIGIHOJA-UHFFFAOYSA-N pentafluoropropane Chemical compound FC(F)CC(F)(F)F MSSNHSVIGIHOJA-UHFFFAOYSA-N 0.000 description 3
FYIRUPZTYPILDH-UHFFFAOYSA-N 1,1,1,2,3,3-hexafluoropropane Chemical compound FC(F)C(F)C(F)(F)F FYIRUPZTYPILDH-UHFFFAOYSA-N 0.000 description 2
NSGXIBWMJZWTPY-UHFFFAOYSA-N 1,1,1,3,3,3-hexafluoropropane Chemical compound FC(F)(F)CC(F)(F)F NSGXIBWMJZWTPY-UHFFFAOYSA-N 0.000 description 2
UJPMYEOUBPIPHQ-UHFFFAOYSA-N 1,1,1-trifluoroethane Chemical compound CC(F)(F)F UJPMYEOUBPIPHQ-UHFFFAOYSA-N 0.000 description 2
AWTOFSDLNREIFS-UHFFFAOYSA-N 1,1,2,2,3-pentafluoropropane Chemical compound FCC(F)(F)C(F)F AWTOFSDLNREIFS-UHFFFAOYSA-N 0.000 description 2
WXGNWUVNYMJENI-UHFFFAOYSA-N 1,1,2,2-tetrafluoroethane Chemical compound FC(F)C(F)F WXGNWUVNYMJENI-UHFFFAOYSA-N 0.000 description 2
NPNPZTNLOVBDOC-UHFFFAOYSA-N 1,1-difluoroethane Chemical compound CC(F)F NPNPZTNLOVBDOC-UHFFFAOYSA-N 0.000 description 2
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
241000196324 Embryophyta Species 0.000 description 2
YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 2
XPDWGBQVDMORPB-UHFFFAOYSA-N Fluoroform Chemical compound FC(F)F XPDWGBQVDMORPB-UHFFFAOYSA-N 0.000 description 2
239000013543 active substance Substances 0.000 description 2
230000003190 augmentative effect Effects 0.000 description 2
238000004140 cleaning Methods 0.000 description 2
239000000796 flavoring agent Substances 0.000 description 2
235000019634 flavors Nutrition 0.000 description 2
229910052731 fluorine Inorganic materials 0.000 description 2
239000011737 fluorine Substances 0.000 description 2
239000003205 fragrance Substances 0.000 description 2
239000007789 gas Substances 0.000 description 2
239000000203 mixture Substances 0.000 description 2
GTLACDSXYULKMZ-UHFFFAOYSA-N pentafluoroethane Chemical compound FC(F)C(F)(F)F GTLACDSXYULKMZ-UHFFFAOYSA-N 0.000 description 2
SUAMPXQALWYDBK-UHFFFAOYSA-N 1,1,1,2,2,3-hexafluoropropane Chemical compound FCC(F)(F)C(F)(F)F SUAMPXQALWYDBK-UHFFFAOYSA-N 0.000 description 1
ZDCWZRQSHBQRGN-UHFFFAOYSA-N 1,1,1,2,3-pentafluoropropane Chemical compound FCC(F)C(F)(F)F ZDCWZRQSHBQRGN-UHFFFAOYSA-N 0.000 description 1
WZLFPVPRZGTCKP-UHFFFAOYSA-N 1,1,1,3,3-pentafluorobutane Chemical compound CC(F)(F)CC(F)(F)F WZLFPVPRZGTCKP-UHFFFAOYSA-N 0.000 description 1
MWDWMQNTNBHJEI-UHFFFAOYSA-N 1,1,2,3,3-pentafluoropropane Chemical compound FC(F)C(F)C(F)F MWDWMQNTNBHJEI-UHFFFAOYSA-N 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
240000007154 Coffea arabica Species 0.000 description 1
244000018436 Coriandrum sativum Species 0.000 description 1
235000002787 Coriandrum sativum Nutrition 0.000 description 1
244000304337 Cuminum cyminum Species 0.000 description 1
235000007129 Cuminum cyminum Nutrition 0.000 description 1
240000006927 Foeniculum vulgare Species 0.000 description 1
235000004204 Foeniculum vulgare Nutrition 0.000 description 1
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
240000007232 Illicium verum Species 0.000 description 1
235000008227 Illicium verum Nutrition 0.000 description 1
-1 R-227ea Chemical compound 0.000 description 1
235000016639 Syzygium aromaticum Nutrition 0.000 description 1
244000223014 Syzygium aromaticum Species 0.000 description 1
244000273928 Zingiber officinale Species 0.000 description 1
235000006886 Zingiber officinale Nutrition 0.000 description 1
239000004480 active ingredient Substances 0.000 description 1
230000002411 adverse Effects 0.000 description 1
238000013459 approach Methods 0.000 description 1
125000003118 aryl group Chemical group 0.000 description 1
230000004323 axial length Effects 0.000 description 1
230000000740 bleeding effect Effects 0.000 description 1
238000009835 boiling Methods 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
238000004113 cell culture Methods 0.000 description 1
238000001311 chemical methods and process Methods 0.000 description 1
235000016213 coffee Nutrition 0.000 description 1
235000013353 coffee beverage Nutrition 0.000 description 1
238000009264 composting Methods 0.000 description 1
230000001276 controlling effect Effects 0.000 description 1
238000013461 design Methods 0.000 description 1
230000006866 deterioration Effects 0.000 description 1
238000011161 development Methods 0.000 description 1
230000018109 developmental process Effects 0.000 description 1
235000013399 edible fruits Nutrition 0.000 description 1
238000005516 engineering process Methods 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
239000006052 feed supplement Substances 0.000 description 1
238000000855 fermentation Methods 0.000 description 1
230000004151 fermentation Effects 0.000 description 1
125000001153 fluoro group Chemical group F* 0.000 description 1
235000013305 food Nutrition 0.000 description 1
235000008397 ginger Nutrition 0.000 description 1
UKACHOXRXFQJFN-UHFFFAOYSA-N heptafluoropropane Chemical class FC(F)C(F)(F)C(F)(F)F UKACHOXRXFQJFN-UHFFFAOYSA-N 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
238000012432 intermediate storage Methods 0.000 description 1
238000002156 mixing Methods 0.000 description 1
238000011017 operating method Methods 0.000 description 1
235000015205 orange juice Nutrition 0.000 description 1
239000000575 pesticide Substances 0.000 description 1
239000002243 precursor Substances 0.000 description 1
238000012545 processing Methods 0.000 description 1
230000002035 prolonged effect Effects 0.000 description 1
238000005086 pumping Methods 0.000 description 1
238000005057 refrigeration Methods 0.000 description 1
230000001105 regulatory effect Effects 0.000 description 1
238000000926 separation method Methods 0.000 description 1
238000000638 solvent extraction Methods 0.000 description 1
241000894007 species Species 0.000 description 1
238000013020 steam cleaning Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/40—Extractive distillation
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/28—Evaporating with vapour compression
- B01D1/284—Special features relating to the compressed vapour
- B01D1/2846—The compressed vapour is not directed to the same apparatus from which the vapour was taken off
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets

Landscapes

Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Extraction Or Liquid Replacement (AREA)
Detergent Compositions (AREA)

ZA200201747A 1999-09-06 2002-03-01 Apparatus and methods for removing solvent residues. ZA200201747B (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
GBGB9920943.9A GB9920943D0 (en)	1999-09-06	1999-09-06	Apparatus and methods for removing solvent residues

Publications (1)

Publication Number	Publication Date
ZA200201747B true ZA200201747B (en)	2003-05-28

Family

ID=10860370

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
ZA200201747A ZA200201747B (en)	1999-09-06	2002-03-01	Apparatus and methods for removing solvent residues.

Country Status (16)

Country	Link
US (1)	US6676838B2 (de)
EP (1)	EP1214130B1 (de)
JP (1)	JP2003508207A (de)
KR (1)	KR20020033786A (de)
CN (1)	CN1198673C (de)
AT (1)	ATE271909T1 (de)
AU (1)	AU776678B2 (de)
BR (1)	BR0013807A (de)
CA (1)	CA2383594A1 (de)
DE (1)	DE60012547T2 (de)
GB (2)	GB9920943D0 (de)
IL (1)	IL148466A0 (de)
MX (1)	MXPA02002440A (de)
RU (1)	RU2223132C2 (de)
WO (1)	WO2001017645A1 (de)
ZA (1)	ZA200201747B (de)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB9920947D0 (en) *	1999-09-06	1999-11-10	Ici Ltd	A method and apparatus for recovering a solvent
US20070199687A1 (en) *	2004-03-11	2007-08-30	Behr Gmbh & Co. Kg	Stacked-Plate Heat Exchanger
KR100618559B1 (ko) *	2005-06-15	2006-09-01	주식회사 제일메디칼코퍼레이션	회전방지턱 및 무나사부를 구비한 치열교정용 스크류
RU2290012C1 (ru) *	2005-07-08	2006-12-27	Олег Иванович Квасенков	Способ производства экспандированного табака
US8048304B2 (en) *	2007-12-27	2011-11-01	Dynasep Llc	Solvent extraction and recovery
WO2011000094A1 (en) *	2009-07-02	2011-01-06	Bioexx Specialty Proteins Ltd.	Process for removing organic solvents from a biomass
KR101303617B1 (ko) *	2011-03-22	2013-09-11	강원대학교산학협력단	미세조류의 바이오디젤 지질 추출 공정 부산물의 사료화를 위한 클로로포름/메탄올 제거 전처리 장치 및 방법
US9169455B2 (en) *	2011-10-27	2015-10-27	Jerry Hamler	Process for extracting oil from plants and animal matter
US8859793B2 (en) *	2011-10-27	2014-10-14	Jerry Hamler	Process for extracting oil from plants and animal matter
CN102363085B (zh) *	2011-11-11	2014-08-20	惠州市众惠能源科技有限公司	中药的水提取药液的提取浓缩方法及其专用装置
CN103830931A (zh) *	2012-11-27	2014-06-04	张勇	一种全自动萃取-蒸发装置
CN104826358A (zh) *	2015-04-22	2015-08-12	江苏沙家浜化工设备有限公司	笼式动态强制提取罐
UA103010U (xx) *	2015-06-18	2015-11-25		Установка для обезжирювання жировмісного продукту
IL255268B (en)	2017-10-26	2019-01-31	Izun Pharmaceuticals Corp	Smoke capture system and method
US20190308116A1 (en) *	2018-04-10	2019-10-10	Craig Alan Brodersen	Solvent based cannabinoid extraction process with improved efficiency, safety, quality, which yields a homogenous and pasteurized product
RU2769144C1 (ru) *	2021-07-15	2022-03-28	Дмитрий Александрович Соловьев	Способ и установка (варианты) экстракции твердых веществ
WO2024173304A1 (en) *	2023-02-16	2024-08-22	Cargill, Incorporated	Oilseed extraction plant comprising an installation suitable for evaporating a solvent from a solvent-containing mixture

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
GB1476697A (en) *	1973-10-19	1977-06-16	Sussmeyer L	Automatic continuous method of and apparatus for instanta neous vacuum vaporisation for the recovery of used solvents
GB1557123A (en) *	1977-04-29	1979-12-05	Distillers Co Carbon Dioxide	Method and apparatus for reparing extracts of hops and other materials
US4349415A (en) *	1979-09-28	1982-09-14	Critical Fluid Systems, Inc.	Process for separating organic liquid solutes from their solvent mixtures
EP0061877A3 (de) *	1981-03-31	1985-08-07	Distillers Mg Limited	Verfahren und Anlage zur Gewinnung eines Hopfenextrakts
US4518502A (en) *	1981-11-04	1985-05-21	Maxwell Laboratories, Inc.	Method of extracting organic contaminants from process waters
DE3538745A1 (de) *	1985-10-31	1987-05-07	Extraktionstechnik Gmbh	Verfahren und anlage zur abwasserfreien feststoffextraktion mit organischen loesemitteln
US5516923A (en)	1992-04-27	1996-05-14	Agritech International	Extracting oil from oil bearing plant parts
JPH0617081A (ja) *	1992-06-29	1994-01-25	Ajinomoto Co Inc	油脂抽出装置内での抽出粕からの抽出溶剤除去法
CN1090597A (zh) *	1993-02-01	1994-08-10	食品科学公司	从谷物原料和谷物基料食品中浸出油的设备和方法
GB2288552A (en) *	1994-04-19	1995-10-25	Ici Plc	Solvent extraction process
RU2122417C1 (ru) *	1994-09-19	1998-11-27	Игорь Сергеевич Ежов	Способ получения изомеризованного экстракта хмеля
US5998640A (en) *	1996-02-13	1999-12-07	Haefele; Gary R.	Method for recovering oil from an oil-bearing solid material
US5707673A (en) *	1996-10-04	1998-01-13	Prewell Industries, L.L.C.	Process for extracting lipids and organics from animal and plant matter or organics-containing waste streams
US6855349B2 (en) *	1998-12-07	2005-02-15	Kemin Industries, Inc.	Method for simultaneous extraction of essential oils and antioxidants from Labiatae species and the extract products thereof

1999
- 1999-09-06 GB GBGB9920943.9A patent/GB9920943D0/en not_active Ceased
2000
- 2000-08-24 GB GB0020776A patent/GB2353727B/en not_active Expired - Fee Related
- 2000-09-01 KR KR1020027002981A patent/KR20020033786A/ko not_active Withdrawn
- 2000-09-01 WO PCT/GB2000/003345 patent/WO2001017645A1/en not_active Ceased
- 2000-09-01 CA CA002383594A patent/CA2383594A1/en not_active Abandoned
- 2000-09-01 CN CNB008150737A patent/CN1198673C/zh not_active Expired - Fee Related
- 2000-09-01 EP EP00956696A patent/EP1214130B1/de not_active Expired - Lifetime
- 2000-09-01 DE DE60012547T patent/DE60012547T2/de not_active Expired - Fee Related
- 2000-09-01 AT AT00956696T patent/ATE271909T1/de not_active IP Right Cessation
- 2000-09-01 RU RU2002108730/12A patent/RU2223132C2/ru not_active IP Right Cessation
- 2000-09-01 BR BR0013807-0A patent/BR0013807A/pt not_active IP Right Cessation
- 2000-09-01 AU AU68563/00A patent/AU776678B2/en not_active Ceased
- 2000-09-01 MX MXPA02002440A patent/MXPA02002440A/es unknown
- 2000-09-01 JP JP2001521427A patent/JP2003508207A/ja not_active Withdrawn
- 2000-09-01 IL IL14846600A patent/IL148466A0/xx unknown
2002
- 2002-02-27 US US10/083,977 patent/US6676838B2/en not_active Expired - Fee Related
- 2002-03-01 ZA ZA200201747A patent/ZA200201747B/en unknown

Also Published As

Publication number	Publication date
RU2223132C2 (ru)	2004-02-10
DE60012547D1 (de)	2004-09-02
EP1214130B1 (de)	2004-07-28
CN1384766A (zh)	2002-12-11
GB2353727B (en)	2001-12-12
GB0020776D0 (en)	2000-10-11
US6676838B2 (en)	2004-01-13
AU776678B2 (en)	2004-09-16
WO2001017645A1 (en)	2001-03-15
AU6856300A (en)	2001-04-10
DE60012547T2 (de)	2005-08-04
US20020195329A1 (en)	2002-12-26
KR20020033786A (ko)	2002-05-07
CN1198673C (zh)	2005-04-27
ATE271909T1 (de)	2004-08-15
BR0013807A (pt)	2002-05-21
EP1214130A1 (de)	2002-06-19
JP2003508207A (ja)	2003-03-04
MXPA02002440A (es)	2002-07-30
IL148466A0 (en)	2002-09-12
GB2353727A (en)	2001-03-07
CA2383594A1 (en)	2001-03-15
GB9920943D0 (en)	1999-11-10

Publication	Publication Date	Title
US6676838B2 (en)	2004-01-13	Apparatus and methods for removing solvent residues
US6589422B2 (en)	2003-07-08	Apparatus and method for extracting biomass
AU766475C (en)	2004-09-09	Apparatus and method for removing solvent residues
EP1210157B1 (de)	2006-08-23	Vorrichtung und verfahren zur verminderung von restlösungsmittelgehalten
EP1345665B1 (de)	2006-06-28	Apparat und methode zum extrahieren von biomasse