ZA200401441B - Process for the production of detergent granules. - Google Patents

Process for the production of detergent granules. Download PDF

Info

Publication number: ZA200401441B
Authority: ZA; South Africa
Prior art keywords: weight; process according; liquid binder; detergent granules; aluminosilicate
Prior art date: 2001-10-25

Application number

ZA200401441A

Other languages

English (en)

Inventor

Johannes Hendrikus M Akkermans

Remy Antal Verburgh

Original Assignee

Unilever Plc

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2001-10-25

Filing date

2004-02-23

Publication date

2005-03-10

2004-02-23 Application filed by Unilever Plc filed Critical Unilever Plc

2005-03-10 Publication of ZA200401441B publication Critical patent/ZA200401441B/en

Links

238000000034 method Methods 0.000 title claims description 51
239000008187 granular material Substances 0.000 title claims description 37
239000003599 detergent Substances 0.000 title claims description 35
238000004519 manufacturing process Methods 0.000 title description 5
239000007788 liquid Substances 0.000 claims description 37
239000011230 binding agent Substances 0.000 claims description 34
HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 32
239000000203 mixture Substances 0.000 claims description 29
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 24
239000000843 powder Substances 0.000 claims description 24
229910000323 aluminium silicate Inorganic materials 0.000 claims description 23
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
150000003839 salts Chemical class 0.000 claims description 15
239000003945 anionic surfactant Substances 0.000 claims description 13
229910000029 sodium carbonate Inorganic materials 0.000 claims description 10
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 9
239000002736 nonionic surfactant Substances 0.000 claims description 8
239000000344 soap Substances 0.000 claims description 8
239000004094 surface-active agent Substances 0.000 claims description 6
239000002250 absorbent Substances 0.000 claims description 4
230000002745 absorbent Effects 0.000 claims description 4
239000000377 silicon dioxide Substances 0.000 claims description 4
229910017053 inorganic salt Inorganic materials 0.000 claims description 3
150000004760 silicates Chemical class 0.000 claims description 3
238000002360 preparation method Methods 0.000 claims description 2
239000000126 substance Substances 0.000 claims 3
239000000463 material Substances 0.000 description 16
239000010457 zeolite Substances 0.000 description 13
229910021536 Zeolite Inorganic materials 0.000 description 12
239000002245 particle Substances 0.000 description 12
239000007787 solid Substances 0.000 description 12
-1 alkali metal aluminosilicate Chemical class 0.000 description 11
239000003795 chemical substances by application Substances 0.000 description 10
235000017550 sodium carbonate Nutrition 0.000 description 9
239000012530 fluid Substances 0.000 description 7
238000005243 fluidization Methods 0.000 description 7
239000007789 gas Substances 0.000 description 6
238000001694 spray drying Methods 0.000 description 6
229910052783 alkali metal Inorganic materials 0.000 description 5
238000005469 granulation Methods 0.000 description 5
230000003179 granulation Effects 0.000 description 5
230000003472 neutralizing effect Effects 0.000 description 5
239000007921 spray Substances 0.000 description 5
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 4
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 4
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 4
125000004432 carbon atom Chemical group C* 0.000 description 4
238000009472 formulation Methods 0.000 description 4
239000007858 starting material Substances 0.000 description 4
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
150000001860 citric acid derivatives Chemical class 0.000 description 3
239000000945 filler Substances 0.000 description 3
238000011065 in-situ storage Methods 0.000 description 3
238000002156 mixing Methods 0.000 description 3
159000000000 sodium salts Chemical class 0.000 description 3
235000019832 sodium triphosphate Nutrition 0.000 description 3
BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 2
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
235000010724 Wisteria floribunda Nutrition 0.000 description 2
239000002253 acid Substances 0.000 description 2
229920006243 acrylic copolymer Polymers 0.000 description 2
239000004411 aluminium Substances 0.000 description 2
229910052782 aluminium Inorganic materials 0.000 description 2
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
239000007844 bleaching agent Substances 0.000 description 2
125000002091 cationic group Chemical group 0.000 description 2
150000003841 chloride salts Chemical class 0.000 description 2
150000001875 compounds Chemical class 0.000 description 2
235000014113 dietary fatty acids Nutrition 0.000 description 2
239000000194 fatty acid Substances 0.000 description 2
229930195729 fatty acid Natural products 0.000 description 2
230000004907 flux Effects 0.000 description 2
239000004615 ingredient Substances 0.000 description 2
238000006386 neutralization reaction Methods 0.000 description 2
229920000058 polyacrylate Polymers 0.000 description 2
229920005646 polycarboxylate Polymers 0.000 description 2
229920005996 polystyrene-poly(ethylene-butylene)-polystyrene Polymers 0.000 description 2
239000002994 raw material Substances 0.000 description 2
229910052708 sodium Inorganic materials 0.000 description 2
239000011734 sodium Substances 0.000 description 2
239000011780 sodium chloride Substances 0.000 description 2
229910052938 sodium sulfate Inorganic materials 0.000 description 2
235000011152 sodium sulphate Nutrition 0.000 description 2
KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 2
CIOXZGOUEYHNBF-UHFFFAOYSA-N (carboxymethoxy)succinic acid Chemical class OC(=O)COC(C(O)=O)CC(O)=O CIOXZGOUEYHNBF-UHFFFAOYSA-N 0.000 description 1
RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 description 1
CFPOJWPDQWJEMO-UHFFFAOYSA-N 2-(1,2-dicarboxyethoxy)butanedioic acid Chemical class OC(=O)CC(C(O)=O)OC(C(O)=O)CC(O)=O CFPOJWPDQWJEMO-UHFFFAOYSA-N 0.000 description 1
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
LVVZBNKWTVZSIU-UHFFFAOYSA-N 2-(carboxymethoxy)propanedioic acid Chemical class OC(=O)COC(C(O)=O)C(O)=O LVVZBNKWTVZSIU-UHFFFAOYSA-N 0.000 description 1
229910021532 Calcite Inorganic materials 0.000 description 1
OCUCCJIRFHNWBP-IYEMJOQQSA-L Copper gluconate Chemical class [Cu+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O OCUCCJIRFHNWBP-IYEMJOQQSA-L 0.000 description 1
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical group C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
239000005909 Kieselgur Substances 0.000 description 1
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
JYXGIOKAKDAARW-UHFFFAOYSA-N N-(2-hydroxyethyl)iminodiacetic acid Chemical class OCCN(CC(O)=O)CC(O)=O JYXGIOKAKDAARW-UHFFFAOYSA-N 0.000 description 1
229910019142 PO4 Inorganic materials 0.000 description 1
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
239000011358 absorbing material Substances 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
125000001931 aliphatic group Chemical group 0.000 description 1
239000003513 alkali Substances 0.000 description 1
229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
150000008041 alkali metal carbonates Chemical class 0.000 description 1
150000008044 alkali metal hydroxides Chemical class 0.000 description 1
229910000318 alkali metal phosphate Inorganic materials 0.000 description 1
229910052910 alkali metal silicate Inorganic materials 0.000 description 1
229910052936 alkali metal sulfate Inorganic materials 0.000 description 1
150000001340 alkali metals Chemical class 0.000 description 1
150000004996 alkyl benzenes Chemical group 0.000 description 1
125000000217 alkyl group Chemical group 0.000 description 1
JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 description 1
125000000129 anionic group Chemical group 0.000 description 1
238000013459 approach Methods 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
229910000019 calcium carbonate Inorganic materials 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
150000004649 carbonic acid derivatives Chemical class 0.000 description 1
239000003093 cationic surfactant Substances 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000004927 clay Substances 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
229920001577 copolymer Polymers 0.000 description 1
238000005520 cutting process Methods 0.000 description 1
238000011161 development Methods 0.000 description 1
XPPKVPWEQAFLFU-UHFFFAOYSA-J diphosphate(4-) Chemical compound [O-]P([O-])(=O)OP([O-])([O-])=O XPPKVPWEQAFLFU-UHFFFAOYSA-J 0.000 description 1
235000011180 diphosphates Nutrition 0.000 description 1
238000001035 drying Methods 0.000 description 1
239000004744 fabric Substances 0.000 description 1
150000004665 fatty acids Chemical class 0.000 description 1
238000009477 fluid bed granulation Methods 0.000 description 1
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
229910052816 inorganic phosphate Inorganic materials 0.000 description 1
238000011068 loading method Methods 0.000 description 1
HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 description 1
239000000391 magnesium silicate Substances 0.000 description 1
229910052919 magnesium silicate Inorganic materials 0.000 description 1
235000019792 magnesium silicate Nutrition 0.000 description 1
229910052943 magnesium sulfate Inorganic materials 0.000 description 1
CSNNHWWHGAXBCP-UHFFFAOYSA-L magnesium sulphate Substances [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 1
235000019341 magnesium sulphate Nutrition 0.000 description 1
VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
239000011976 maleic acid Substances 0.000 description 1
239000011159 matrix material Substances 0.000 description 1
229910052914 metal silicate Inorganic materials 0.000 description 1
238000003801 milling Methods 0.000 description 1
JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
150000007524 organic acids Chemical class 0.000 description 1
235000005985 organic acids Nutrition 0.000 description 1
150000004967 organic peroxy acids Chemical class 0.000 description 1
235000014366 other mixer Nutrition 0.000 description 1
239000002304 perfume Substances 0.000 description 1
125000000864 peroxy group Chemical group O(O*)* 0.000 description 1
235000020030 perry Nutrition 0.000 description 1
235000021317 phosphate Nutrition 0.000 description 1
150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
229920000642 polymer Polymers 0.000 description 1
229910052700 potassium Inorganic materials 0.000 description 1
239000011591 potassium Substances 0.000 description 1
239000002243 precursor Substances 0.000 description 1
238000012545 processing Methods 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
150000004671 saturated fatty acids Chemical class 0.000 description 1
235000003441 saturated fatty acids Nutrition 0.000 description 1
238000009818 secondary granulation Methods 0.000 description 1
229910052710 silicon Inorganic materials 0.000 description 1
239000010703 silicon Substances 0.000 description 1
239000011343 solid material Substances 0.000 description 1
239000000243 solution Substances 0.000 description 1
238000005507 spraying Methods 0.000 description 1
238000003756 stirring Methods 0.000 description 1
150000003890 succinate salts Chemical class 0.000 description 1
239000001384 succinic acid Substances 0.000 description 1
150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
238000012360 testing method Methods 0.000 description 1
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 1
RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
150000004670 unsaturated fatty acids Chemical class 0.000 description 1
235000021122 unsaturated fatty acids Nutrition 0.000 description 1
238000005406 washing Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
- C11D11/0088—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads the liquefied ingredients being sprayed or adsorbed onto solid particles
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/04—Carboxylic acids or salts thereof
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols

Landscapes

Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Detergent Compositions (AREA)

ZA200401441A 2001-10-25 2004-02-23 Process for the production of detergent granules. ZA200401441B (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
GBGB0125653.6A GB0125653D0 (en)	2001-10-25	2001-10-25	Process for the production of detergent granules

Publications (1)

Publication Number	Publication Date
ZA200401441B true ZA200401441B (en)	2005-03-10

Family

ID=9924530

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
ZA200401441A ZA200401441B (en)	2001-10-25	2004-02-23	Process for the production of detergent granules.

Country Status (12)

Country	Link
US (1)	US7018971B2 (de)
EP (1)	EP1438382B1 (de)
CN (1)	CN1280398C (de)
AR (1)	AR037022A1 (de)
AT (1)	ATE331022T1 (de)
BR (1)	BR0212752A (de)
DE (1)	DE60212676T2 (de)
GB (1)	GB0125653D0 (de)
MX (1)	MXPA04003585A (de)
RU (1)	RU2311451C2 (de)
WO (1)	WO2003035817A1 (de)
ZA (1)	ZA200401441B (de)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE102004016497B4 (de) *	2004-04-03	2007-04-26	Henkel Kgaa	Verfahren zur Herstellung von Granulaten und deren Einsatz in Wasch- und/oder Reinigungsmitteln
DE102007051093A1 (de) *	2007-10-24	2009-04-30	Henkel Ag & Co. Kgaa	Wasch- oder Reinigungsmittelcompounds und deren Herstellung
WO2011090957A2 (en) *	2010-01-21	2011-07-28	The Procter & Gamble Company	Process of preparing a particle
RU2747177C1 (ru) *	2020-07-30	2021-04-28	Общество с ограниченной ответственностью "Синергетик"	Способ получения концентрированного средства для стирки и его упаковка

Family Cites Families (33)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US4264464A (en) *	1977-10-06	1981-04-28	Colgate-Palmolive Company	High bulk density particulate heavy duty laundry detergent
JPS6169897A (ja)	1984-09-14	1986-04-10	花王株式会社	流動性の改良された高密度の粒状洗剤の製法
EP0229671B1 (de) *	1986-01-17	1991-03-13	Kao Corporation	Granuliertes Reinigungsmittel von hoher Dichte
US4721633A (en) *	1986-08-22	1988-01-26	Colgate-Palmolive Company	Process for manufacturing speckled detergent composition
GB8630991D0 (en)	1986-12-30	1987-02-04	Unilever Plc	Production of coloured detergent particles
GB2221695B (en)	1988-07-21	1992-02-12	Unilever Plc	Detergent compositions and process for preparing them
GB8822456D0 (en)	1988-09-23	1988-10-26	Unilever Plc	Detergent compositions & processes for preparing them
CA2001927C (en)	1988-11-03	1999-12-21	Graham Thomas Brown	Aluminosilicates and detergent compositions
GB8907187D0 (en)	1989-03-30	1989-05-10	Unilever Plc	Detergent compositions and process for preparing them
US5024782A (en) *	1989-06-16	1991-06-18	The Clorox Company	Zeolite agglomeration process and product
US5205958A (en) *	1989-06-16	1993-04-27	The Clorox Company	Zeolite agglomeration process and product
HU212980B (en) *	1990-09-28	1997-01-28	Procter & Gamble	Zeolite/layered silicate built detergent composition containing polyhydroxy fatty acid amides
JP3128170B2 (ja)	1992-09-30	2001-01-29	スズキ株式会社	幌付自動車の幌取付構造
EP0643129A1 (de)	1993-09-07	1995-03-15	The Procter & Gamble Company	Verfahren zur Herstellung von Waschmittelzusammensetzungen
WO1996025482A1 (en)	1995-02-13	1996-08-22	The Procter & Gamble Company	Process for producing detergent agglomerates in which particle size is controlled
US5925614A (en) *	1995-04-27	1999-07-20	The Procter & Gamble Company	Process for producing granular detergent components or compositions
BR9608445A (pt)	1995-04-27	1999-01-05	Procter & Gamble	Processo para a produção de componentes ou composições detergentes granulares
ES2167593T3 (es) *	1995-09-04	2002-05-16	Unilever Nv	Composiciones detergentes y proceso para prepararlas.
GB9526097D0 (en) *	1995-12-20	1996-02-21	Unilever Plc	Process
GB9604000D0 (en)	1996-02-26	1996-04-24	Unilever Plc	Production of anionic detergent particles
EP0922087A1 (de) *	1996-08-26	1999-06-16	The Procter & Gamble Company	Verfahren zur agglomeration zur herstellung von waschmitteln unter verwendung eines vorgemisches modifizierter polyamine
WO1998016615A1 (en)	1996-10-15	1998-04-23	The Procter & Gamble Company	Colored particulate compositions
GB9712580D0 (en)	1997-06-16	1997-08-20	Unilever Plc	Production of detergent granulates
GB9712587D0 (en)	1997-06-16	1997-08-20	Unilever Plc	Production of detergent granulates
GB9712583D0 (en)	1997-06-16	1997-08-20	Unilever Plc	Production of detergent granulates
JP2002507629A (ja) *	1997-07-14	2002-03-12	ザ、プロクター、エンド、ギャンブル、カンパニー	粒子サイズによって塊状化を制御することによる低密度の洗剤組成物の作製方法
CA2296304C (en) *	1997-07-15	2003-05-27	Scott William Capeci	Process for making high-active detergent agglomerates by multi-stage surfactant paste injection
AU8072098A (en)	1998-06-12	1999-12-30	Procter & Gamble Company, The	Cleaning compositions containing speckle particles
US6794354B1 (en) *	1998-09-18	2004-09-21	The Procter & Gamble Company	Continuous process for making detergent composition
EP1149155B1 (de)	1999-02-01	2005-04-27	The Procter & Gamble Company	Kationisches teilchen und verfahren zu seiner herstellung
GB9913546D0 (en)	1999-06-10	1999-08-11	Unilever Plc	Granular detergent component containing zeolite map and laundry detergent compositions containing it
DE19943470A1 (de) *	1999-09-11	2001-03-15	Clariant Gmbh	Kristallines Alkalischichtsilikat
WO2001040428A1 (en)	1999-11-30	2001-06-07	The Procter & Gamble Company	Process for making a detergent composition

2001
- 2001-10-25 GB GBGB0125653.6A patent/GB0125653D0/en not_active Ceased
2002
- 2002-10-23 US US10/278,409 patent/US7018971B2/en not_active Expired - Fee Related
- 2002-10-23 RU RU2004115742/13A patent/RU2311451C2/ru not_active IP Right Cessation
- 2002-10-23 AT AT02787504T patent/ATE331022T1/de not_active IP Right Cessation
- 2002-10-23 WO PCT/EP2002/011895 patent/WO2003035817A1/en not_active Ceased
- 2002-10-23 DE DE60212676T patent/DE60212676T2/de not_active Expired - Lifetime
- 2002-10-23 BR BR0212752-0A patent/BR0212752A/pt active Search and Examination
- 2002-10-23 MX MXPA04003585A patent/MXPA04003585A/es active IP Right Grant
- 2002-10-23 CN CNB028208714A patent/CN1280398C/zh not_active Expired - Fee Related
- 2002-10-23 EP EP02787504A patent/EP1438382B1/de not_active Expired - Lifetime
- 2002-10-25 AR ARP020104049A patent/AR037022A1/es unknown
2004
- 2004-02-23 ZA ZA200401441A patent/ZA200401441B/en unknown

Also Published As

Publication number	Publication date
ATE331022T1 (de)	2006-07-15
WO2003035817A1 (en)	2003-05-01
EP1438382B1 (de)	2006-06-21
CN1280398C (zh)	2006-10-18
RU2311451C2 (ru)	2007-11-27
MXPA04003585A (es)	2004-07-23
CN1575332A (zh)	2005-02-02
US20030100471A1 (en)	2003-05-29
AR037022A1 (es)	2004-10-20
US7018971B2 (en)	2006-03-28
RU2004115742A (ru)	2005-04-20
DE60212676D1 (de)	2006-08-03
GB0125653D0 (en)	2001-12-19
DE60212676T2 (de)	2006-11-09
EP1438382A1 (de)	2004-07-21
BR0212752A (pt)	2004-10-05

Publication	Publication Date	Title
US7053038B2 (en)	2006-05-30	Process for the production of detergent granules
US7018972B2 (en)	2006-03-28	Process for the production of detergent granules
EP0925354B1 (de)	2004-08-11	Verfahren zur herstellung von waschmitteln mit hohem schüttgewicht
EP1320578B1 (de)	2005-12-07	Herstellung von aniontensidgranulaten durch in-situ neutralisation
WO2000060041A1 (en)	2000-10-12	Detergent powder composition
US7018971B2 (en)	2006-03-28	Process for the production of detergent granules
US20020065207A1 (en)	2002-05-30	Production of anionic surfactant granules by in situ neutralisation
US20030060392A1 (en)	2003-03-27	Process for the production of detergent granules
EP0925353B1 (de)	2002-10-23	Verfahren zur herstellung von waschmittelzusammensetzungen mit hohem schüttgewicht
WO1998011193A1 (en)	1998-03-19	Process for preparing high bulk density detergent compositions
EP1332203B1 (de)	2004-11-24	Herstellung von aniontensidgranulaten durch in-situ neutralisation
ZA200402700B (en)	2005-06-29	Process for the production of detergent granules
GB2283756A (en)	1995-05-17	Particulate detergent composition
EP1436377A1 (de)	2004-07-14	Waschmittelzusammensetzungen
WO2005033258A1 (en)	2005-04-14	Process for making a detergent composition