AT51203B - Process for the preparation of β-β-dianthraquinonylureas. - Google Patents
Process for the preparation of β-β-dianthraquinonylureas.Info
- Publication number
- AT51203B AT51203B AT51203DA AT51203B AT 51203 B AT51203 B AT 51203B AT 51203D A AT51203D A AT 51203DA AT 51203 B AT51203 B AT 51203B
- Authority
- AT
- Austria
- Prior art keywords
- dianthraquinonylureas
- preparation
- desc
- dianthraquinonylurea
- aminoanthraquinone
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 3
- 238000002360 preparation method Methods 0.000 title description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- LQNUZADURLCDLV-UHFFFAOYSA-N nitrobenzene Chemical compound [O-][N+](=O)C1=CC=CC=C1 LQNUZADURLCDLV-UHFFFAOYSA-N 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- XOGPDSATLSAZEK-UHFFFAOYSA-N 2-Aminoanthraquinone Chemical compound C1=CC=C2C(=O)C3=CC(N)=CC=C3C(=O)C2=C1 XOGPDSATLSAZEK-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- AOGYCOYQMAVAFD-UHFFFAOYSA-N chlorocarbonic acid Chemical compound OC(Cl)=O AOGYCOYQMAVAFD-UHFFFAOYSA-N 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
<Desc/Clms Page number 1>
Verfahren zur Herstellung von ss-ss-Dianthrachinonylharnstoffen.
In weiterer Ausbildung des Verfahrens des Stammpatentes Nr. 47522 wurde gefunden, dass, wenn man 2 Mol. ss-Aminoanthrachinon mit 1 Mol. Chlorkohlensäureäthyl- äther in einem hochsiedenden Lösungsmittel wie z. B. Naphtalin, erhitzt, man direkt den ss-ss-Dianthrachinonylharnstoff in glatter Weise in einer Operation erhält. Die Reaktion verläuft so, dass sich zunächst das in der deutschen Patentschrift Nr 16741 () beschriebene ss-Anthrachinonylurethan bildet, welches sich gemäss den Angaben der Stammpatentschrift Nr. 47522 mit einem weiteren Molekül -Aminoanthrachinon zum ss-ss-Dianthrachinonylharnstoff umsetzt.
EMI1.1
Verwendet man statt Naphtalin als Lösungsmittel Nitrobenzol, so muss entsprechend länger erhitzt werden.
**WARNUNG** Ende DESC Feld kannt Anfang CLMS uberlappen**.
<Desc / Clms Page number 1>
Process for the preparation of ss-ss-dianthraquinonylureas.
In a further development of the process of the parent patent no. 47522 it was found that if 2 mol. Ss-aminoanthraquinone with 1 mol. Chlorocarbonic acid ethyl ether in a high-boiling solvent such as. B. naphthalene heated, the ss-ss-dianthraquinonylurea is obtained directly in one operation in a smooth manner. The reaction proceeds in such a way that the ss-anthraquinonyl urea described in German patent specification No. 16741 () is initially formed, which, according to the information in parent patent specification No. 47522, reacts with another molecule -aminoanthraquinone to form ss-ss-dianthraquinonylurea.
EMI1.1
If nitrobenzene is used as a solvent instead of naphthalene, the heating must be correspondingly longer.
** WARNING ** End of DESC field may overlap beginning of CLMS **.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE47522X | 1909-02-01 | ||
| DE51203X | 1909-03-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AT51203B true AT51203B (en) | 1911-12-11 |
Family
ID=25749055
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT51203D AT51203B (en) | 1909-02-01 | 1910-02-07 | Process for the preparation of β-β-dianthraquinonylureas. |
Country Status (1)
| Country | Link |
|---|---|
| AT (1) | AT51203B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102006006301A1 (en) | 2006-02-10 | 2007-08-23 | Hiwin Technologies Corp. | Load-bearing elevator spindle attached to overhead frame hangs from locknut with rounded lower face |
-
1910
- 1910-02-07 AT AT51203D patent/AT51203B/en active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102006006301A1 (en) | 2006-02-10 | 2007-08-23 | Hiwin Technologies Corp. | Load-bearing elevator spindle attached to overhead frame hangs from locknut with rounded lower face |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| AT51203B (en) | Process for the preparation of β-β-dianthraquinonylureas. | |
| AT29202B (en) | Process for the preparation of pure double compounds of sulfoxylic acid salts with aldehydes. | |
| AT159191B (en) | Process for the preparation of a chlorocarbon compound of the formula C4Cl6. | |
| AT43639B (en) | Process for the preparation of β-methyladipic acid. | |
| AT30875B (en) | Process for the preparation of alizarin. | |
| AT39289B (en) | Process for the preparation of durable double compounds of aldehydes with reduction products of sulphurous acid. | |
| AT62490B (en) | Process for the preparation of acetaldehyde and its condensation and polymerization products from acetylene. | |
| AT143866B (en) | Process for the production of brewer's pitch. | |
| AT123880B (en) | Extrusion press for the production of soap bars with deposits. | |
| AT48248B (en) | Process for the production of combined photographic images. | |
| AT298438B (en) | Process for the production of aspartic acid | |
| AT48352B (en) | Process for the direct introduction of chlorine into anthraquinone. | |
| AT136012B (en) | Process for the preparation or regeneration of catalysts for the conversion of terpenes. | |
| AT131133B (en) | Method for the preparation of p-menthen- (3). | |
| AT25921B (en) | Process for producing a durable indigo paste which can be used directly in the fermentation vat. | |
| DE581956C (en) | Process for the production of condensation products from phenols and natural resins | |
| AT71166B (en) | Process for the preparation of 4-halogeno- and 4-alkyl-1-oxyanthraquinones and their substitution products. | |
| AT45767B (en) | Process for the preparation of antimony compounds which contain the antimony oxide wholly or partially bound to sulphurous acid or acetic acid. | |
| DE877305C (en) | Process for the preparation of 1,2-bis (alkylamino) cyclohexanes and its core substitution products | |
| AT49942B (en) | Process for the preparation of mixtures of aromatic nitro compounds from solvent naphtha. | |
| AT159377B (en) | Process for the preparation of descendants of 2-oxocycloparaffincarboxylic acids- (1). | |
| AT60761B (en) | Process for the preparation of β-γ-dimethylbutadiene. | |
| AT235826B (en) | Process for the production of organic peroxides | |
| AT50347B (en) | Process for the production of acetic anhydride. | |
| AT108545B (en) | Method for the preparation of codeinone. |