ATE12088T1 - Verfahren zur herstellung von siliciumdioxid und dessen verwendung. - Google Patents

Verfahren zur herstellung von siliciumdioxid und dessen verwendung.

Info

Publication number: ATE12088T1
Authority: AT; Austria
Prior art keywords: solvent; water; resulting silica; hydrolysis; single phase
Prior art date: 1980-05-21

Application number

AT81103459T

Other languages

English (en)

Inventor

Max Paul Mcdaniel

Original Assignee

Phillips Petroleum Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1980-05-21

Filing date

1981-05-07

Publication date

1985-03-15

1981-05-07 Application filed by Phillips Petroleum Co filed Critical Phillips Petroleum Co

1985-03-15 Application granted granted Critical

1985-03-15 Publication of ATE12088T1 publication Critical patent/ATE12088T1/de

Links

VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title abstract 8
239000000377 silicon dioxide Substances 0.000 title abstract 4
238000004519 manufacturing process Methods 0.000 title abstract 2
238000000034 method Methods 0.000 title abstract 2
235000012239 silicon dioxide Nutrition 0.000 title 1
239000002904 solvent Substances 0.000 abstract 4
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 4
238000006460 hydrolysis reaction Methods 0.000 abstract 3
230000007062 hydrolysis Effects 0.000 abstract 2
239000011148 porous material Substances 0.000 abstract 2
239000004115 Sodium Silicate Substances 0.000 abstract 1
WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 abstract 1
239000000159 acid neutralizing agent Substances 0.000 abstract 1
229910001413 alkali metal ion Inorganic materials 0.000 abstract 1
239000002585 base Substances 0.000 abstract 1
239000003054 catalyst Substances 0.000 abstract 1
229910000423 chromium oxide Inorganic materials 0.000 abstract 1
150000002148 esters Chemical class 0.000 abstract 1
239000000945 filler Substances 0.000 abstract 1
239000004033 plastic Substances 0.000 abstract 1
229920003023 plastic Polymers 0.000 abstract 1
239000011541 reaction mixture Substances 0.000 abstract 1
-1 silicate ester Chemical class 0.000 abstract 1
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 abstract 1
229910052911 sodium silicate Inorganic materials 0.000 abstract 1
238000005406 washing Methods 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
- B01J21/08—Silica
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/16—Preparation of silica xerogels
- C01B33/163—Preparation of silica xerogels by hydrolysis of organosilicon compounds, e.g. ethyl orthosilicate

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Dispersion Chemistry (AREA)
Polymers & Plastics (AREA)
Medicinal Chemistry (AREA)
Engineering & Computer Science (AREA)
Materials Engineering (AREA)
Health & Medical Sciences (AREA)
Inorganic Chemistry (AREA)
Silicon Compounds (AREA)
Catalysts (AREA)
Silicon Polymers (AREA)
Silicates, Zeolites, And Molecular Sieves (AREA)
Polymerization Catalysts (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)

AT81103459T 1980-05-21 1981-05-07 Verfahren zur herstellung von siliciumdioxid und dessen verwendung. ATE12088T1 (de)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US06/151,847 US4301034A (en)	1980-05-21	1980-05-21	Silica from single phase controlled hydrolysis of silicate ester
EP81103459A EP0040362B1 (de)	1980-05-21	1981-05-07	Verfahren zur Herstellung von Siliciumdioxid und dessen Verwendung

Publications (1)

Publication Number	Publication Date
ATE12088T1 true ATE12088T1 (de)	1985-03-15

Family

ID=22540473

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT81103459T ATE12088T1 (de)	1980-05-21	1981-05-07	Verfahren zur herstellung von siliciumdioxid und dessen verwendung.

Country Status (11)

Country	Link
US (1)	US4301034A (de)
EP (1)	EP0040362B1 (de)
JP (1)	JPS577814A (de)
AT (1)	ATE12088T1 (de)
AU (1)	AU546722B2 (de)
CA (1)	CA1156208A (de)
DE (1)	DE3169233D1 (de)
ES (1)	ES8300305A1 (de)
GB (1)	GB2076384B (de)
NO (1)	NO160351C (de)
SG (1)	SG92585G (de)

Families Citing this family (43)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
CS208879B1 (en) *	1979-07-09	1981-10-30	Ivan Novak	Preparation method of silicic acid xerogel with high volumen of pores
US4454293A (en) *	1981-11-20	1984-06-12	Phillips Petroleum Company	Polymerization using partially hydrolyzed silicate treatment of catalyst support
US4419268A (en) *	1981-11-20	1983-12-06	Phillips Petroleum Company	Partially hydrolyzed silicate treatment of catalyst support
US4647442A (en) *	1983-12-19	1987-03-03	Mobil Oil Corporation	Crystalline silicophosphoaluminate from a two phase medium
US4543341A (en) *	1983-12-23	1985-09-24	Massachusetts Institute Of Technology	Synthesis and processing of monosized oxide powders
US4547557A (en) *	1984-07-09	1985-10-15	Phillips Petroleum Company	Silica-titania cogel from two-step hydrolysis
AU5071285A (en) *	1984-12-13	1986-06-19	South African Inventions Development Corp.	Production of complex metal hydroxide powders
JPH069660B2 (ja) *	1986-10-30	1994-02-09	株式会社中戸研究所	金属アルコキシドのゾルーゲル法触媒およびそれを用いたゾルーゲル法
GB8707526D0 (en) *	1987-03-30	1987-05-07	Unilever Plc	Amorphous silicas
EP0328715B1 (de) *	1988-02-19	1992-08-05	Tohru Yamamoto	Katalysator für das ein Metallalkoxid verwendendes Sol-Gel-Verfahren und das Oxid verwendende Sol-Gel-Verfahren
US4943425A (en) *	1988-04-01	1990-07-24	Gte Laboratories Incorporated	Method of making high purity dense silica of large particle size
US5158758A (en) *	1989-04-24	1992-10-27	International Minerals & Chemical Corp.	Production of silica having high specific surface area
US5073531A (en) *	1990-05-07	1991-12-17	Phillips Petroleum Company	Olefin polymerization catalysts and preparation method
GB9210265D0 (en) *	1992-05-13	1992-07-01	Unilever Plc	Catalysts and catalyst supports
DE4309660A1 (de) *	1993-03-25	1994-09-29	Studiengesellschaft Kohle Mbh	Selektive anorganische Katalysatoren in Form von molekularen Abdrücken in Hohlräumen
US5372983A (en) *	1993-05-24	1994-12-13	W. R. Grace & Co.-Conn.	Preparation of catalysts and supports
US5670438A (en) *	1993-10-27	1997-09-23	Phillips Petroleum Company	Catalyst compositions and catalytic processes
FR2736342B1 (fr) *	1995-07-07	1999-01-29	Univ Claude Bernard Lyon	Procede pour la fabrication d'aerogels de silice monolithiques et aerogels de silice ainsi obtenus
KR20000070007A (ko)	1997-01-08	2000-11-25	마이클 비. 키한	탄화수소 수지 제조용 촉매로서의 고체 산
DE60123878T2 (de) *	2000-06-28	2007-05-24	Japan Super Quartz Corp.	Synthetisches Quarzpulver, Verfahren zur Herstellung und synthetischer Quarztiegel
KR20050084221A (ko) *	2002-12-10	2005-08-26	바젤 폴리올레핀 게엠베하	지지된 크롬 촉매, 및 에틸렌의 단독중합체 및 공중합체의제조를 위한 이의 용도
CA2690537A1 (en) *	2007-06-04	2008-12-11	Alltech Associates, Inc.	Silica particles and methods of making and using the same
US8399580B2 (en)	2010-08-11	2013-03-19	Chevron Philips Chemical Company Lp	Additives to chromium catalyst mix tank
US8440772B2 (en)	2011-04-28	2013-05-14	Chevron Phillips Chemical Company Lp	Methods for terminating olefin polymerizations
US8487053B2 (en)	2011-11-30	2013-07-16	Chevron Phillips Chemical Company Lp	Methods for removing polymer skins from reactor walls
US8501882B2 (en)	2011-12-19	2013-08-06	Chevron Phillips Chemical Company Lp	Use of hydrogen and an organozinc compound for polymerization and polymer property control
US8703883B2 (en)	2012-02-20	2014-04-22	Chevron Phillips Chemical Company Lp	Systems and methods for real-time catalyst particle size control in a polymerization reactor
US10273315B2 (en)	2012-06-20	2019-04-30	Chevron Phillips Chemical Company Lp	Methods for terminating olefin polymerizations
US8916494B2 (en)	2012-08-27	2014-12-23	Chevron Phillips Chemical Company Lp	Vapor phase preparation of fluorided solid oxides
US8940842B2 (en)	2012-09-24	2015-01-27	Chevron Phillips Chemical Company Lp	Methods for controlling dual catalyst olefin polymerizations
US9708426B2 (en)	2015-06-01	2017-07-18	Chevron Phillips Chemical Company Lp	Liquid-solid sampling system for a loop slurry reactor
US10005861B2 (en)	2016-06-09	2018-06-26	Chevron Phillips Chemical Company Lp	Methods for increasing polymer production rates with halogenated hydrocarbon compounds
US10300460B1 (en)	2017-11-17	2019-05-28	Chevron Phillips Chemical Company L.P.	Aqueous methods for titanating a chromium/silica catalyst
US10259893B1 (en)	2018-02-20	2019-04-16	Chevron Phillips Chemical Company Lp	Reinforcement of a chromium/silica catalyst with silicate oligomers
US10774161B2 (en)	2019-01-31	2020-09-15	Chevron Phillips Chemical Company Lp	Systems and methods for polyethylene recovery with low volatile content
US11186656B2 (en)	2019-05-24	2021-11-30	Chevron Phillips Chemical Company Lp	Preparation of large pore silicas and uses thereof in chromium catalysts for olefin polymerization
US12077616B2 (en)	2021-12-15	2024-09-03	Chevron Phillips Chemical Company Lp	Production of polyethylene and ethylene oligomers from ethanol and the use of biomass and waste streams as feedstocks to produce the ethanol
US11845814B2 (en)	2022-02-01	2023-12-19	Chevron Phillips Chemical Company Lp	Ethylene polymerization processes and reactor systems for the production of multimodal polymers using combinations of a loop reactor and a fluidized bed reactor
US12466900B2 (en)	2022-04-19	2025-11-11	Chevron Phillips Chemical Company Lp	Loop slurry periodogram control to prevent reactor fouling and reactor shutdowns
CN115715969B (zh) *	2022-11-30	2025-08-12	华陆工程科技有限责任公司	高沸物处理方法
CN117089075A (zh) *	2023-07-20	2023-11-21	西北大学	一种催化硅酸酯水解的新方法
US20250066274A1 (en)	2023-08-22	2025-02-27	Chevron Phillips Chemical Company Lp	Integrated processes utilizing water electrolysis and oxidative dehydrogenation of ethane
CN119038492B (zh) *	2024-08-21	2025-04-11	东莞领航电子新材料有限公司	一种高纯度硅溶胶与氯化氢的制备方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3354095A (en) *	1964-07-23	1967-11-21	Owens Illinois Inc	Solid, substantially spherical, hard particles and preparation thereof
US3321276A (en) *	1965-10-23	1967-05-23	Owens Illinois Inc	Preparation of silica gel
US3442824A (en) *	1967-05-12	1969-05-06	Hempel S Marine Paints Inc	Polymeric compositions and protective coatings
FR1568817A (de) *	1967-11-30	1969-05-30
DE1963439A1 (de) *	1969-12-18	1971-06-24	Dynamit Nobel Ag	Verfahren zur Herstellung poroeser Kieselsaeure
US4006175A (en) *	1969-12-18	1977-02-01	Dynamit Nobel Aktiengesellschaft	Porous silicic acid and its production
US3709833A (en) *	1970-08-21	1973-01-09	Owens Illinois Inc	Process for preparing high purity silicon oxide porous beads doped with small quantities of other oxides
US3979215A (en) *	1972-05-25	1976-09-07	Zirconal Processes Limited	Refractory articles and methods of producing same
US4119569A (en) *	1973-05-24	1978-10-10	Phillips Petroleum Company	Olefin polymerization catalyst
US3948806A (en) *	1973-07-26	1976-04-06	Phillips Petroleum Company	Large pore silica and polymerization catalyst
JPS50140397A (de) *	1974-04-30	1975-11-11
JPS5134219A (de) *	1974-09-17	1976-03-23	Tokyo Shibaura Electric Co
DD114245A1 (de) *	1974-09-30	1975-07-20
US4188471A (en) *	1974-12-04	1980-02-12	Phillips Petroleum Company	Organochromium on titanium-impregnated base as olefin polymerization catalyst
JPS5223640A (en) *	1975-08-15	1977-02-22	Tokyo Electric Power Co Inc:The	Protective relay
US4206297A (en) *	1977-04-25	1980-06-03	Chemplex Company	Polymerization catalysts and methods
NL7707961A (nl) *	1977-07-18	1979-01-22	Stamicarbon	Werkwijze ter bereiding van poreus, zuiver siliciumdioxyde.

1980
- 1980-05-21 US US06/151,847 patent/US4301034A/en not_active Expired - Lifetime
1981
- 1981-03-24 CA CA000373701A patent/CA1156208A/en not_active Expired
- 1981-04-07 AU AU69167/81A patent/AU546722B2/en not_active Expired
- 1981-05-07 AT AT81103459T patent/ATE12088T1/de not_active IP Right Cessation
- 1981-05-07 DE DE8181103459T patent/DE3169233D1/de not_active Expired
- 1981-05-07 EP EP81103459A patent/EP0040362B1/de not_active Expired
- 1981-05-07 JP JP6886081A patent/JPS577814A/ja active Granted
- 1981-05-19 GB GB8115323A patent/GB2076384B/en not_active Expired
- 1981-05-20 NO NO811718A patent/NO160351C/no not_active IP Right Cessation
- 1981-05-20 ES ES502349A patent/ES8300305A1/es not_active Expired
1985
- 1985-12-03 SG SG925/85A patent/SG92585G/en unknown

Also Published As

Publication number	Publication date
JPS577814A (en)	1982-01-16
GB2076384B (en)	1984-12-05
DE3169233D1 (en)	1985-04-18
ES502349A0 (es)	1982-11-01
US4301034A (en)	1981-11-17
JPH0338207B2 (de)	1991-06-10
ES8300305A1 (es)	1982-11-01
NO160351C (no)	1989-04-12
CA1156208A (en)	1983-11-01
GB2076384A (en)	1981-12-02
NO160351B (no)	1989-01-02
SG92585G (en)	1986-07-25
EP0040362B1 (de)	1985-03-13
AU6916781A (en)	1981-11-26
EP0040362A1 (de)	1981-11-25
NO811718L (no)	1981-11-23
AU546722B2 (en)	1985-09-19

Legal Events

Date	Code	Title	Description
1985-07-15	UEP	Publication of translation of european patent specification
1998-02-15	REN	Ceased due to non-payment of the annual fee

Publication	Publication Date	Title
ATE12088T1 (de)	1985-03-15	Verfahren zur herstellung von siliciumdioxid und dessen verwendung.
ATE4303T1 (de)	1983-08-15	Verfahren zur herstellung von kieselsaeure mittels flammenhydrolyse.
DE3576172D1 (de)	1990-04-05	Verfahren zur reinigung des tollwutvirus.
AT346830B (de)	1978-11-27	Verfahren zur herstellung von p-benzochinon- diketalen
ATE8142T1 (de)	1984-07-15	Verfahren zur herstellung von isosorbid-5-nitrat.
ATE11525T1 (de)	1985-02-15	Verfahren zur herstellung von betahydroxybutans\|ure.
ATE60923T1 (de)	1991-03-15	Verfahren zur herstellung von pseudocumol oder von durol.
DE3577566D1 (de)	1990-06-13	Verfahren zur herstellung von poly(tetramethylenether)glykol.
ES8400727A1 (es)	1983-11-01	"metodo de producir un ester dialilico de acido tetrabromoftalico".
ATE12221T1 (de)	1985-04-15	Verfahren zur hestellung von einem glutaraldehydvorlaeufer.
ATE196758T1 (de)	2000-10-15	Verfahren zur herstellung von difluoromethan
ATE73423T1 (de)	1992-03-15	Verfahren zur herstellung von kieselsaeuren.
AT341533B (de)	1978-02-10	Verfahren zur herstellung von cyanursaure
AT346755B (de)	1978-11-27	Verfahren zur herstellung einer betonmischung zur erzielung eines betons hoher druckfestig- keit
ES8600336A1 (es)	1985-10-01	Procedimiento para preparar poli (vinilacetales)
ATA321674A (de)	1976-09-15	Verfahren zur herstellung von carbonsaureamiden durch wasseranlagerung an nitrile
ATA256175A (de)	1977-05-15	Verfahren zur herstellung von vinylchlorid durch thermische spaltung von 1,2 dichlorathan
GB1497992A (en)	1978-01-12	Production of carboxy-alkane-phosphonic acids and carboxy-alkyl-phosphinic acids
ATE10101T1 (de)	1984-11-15	Verfahren zur herstellung von alkylvanadaten.
ATE44969T1 (de)	1989-08-15	Herstellung von poly(arylenketonen).
ATE10486T1 (de)	1984-12-15	Verfahren zur herstellung von allylestern der tetrachlorphthalsaeure.
SU1840614A1 (ru)	2007-08-27	Способ получения жидких тиоколов
ATE41918T1 (de)	1989-04-15	Verfahren zur herstellung von trihydroxybenzolen.
JPS54112999A (en)	1979-09-04	Purification of polyether
ATA673076A (de)	1979-07-15	Verfahren zur herstellung von als ionen- austauscher verwendbaren aethern des polyhydroxymethylens