ATE130001T1 - Verfahren zur reinigung von glycidyl(meth)acrylat. - Google Patents

Verfahren zur reinigung von glycidyl(meth)acrylat.

Info

Publication number: ATE130001T1
Authority: AT; Austria
Prior art keywords: meth; acrylate; glycidyl; distillation; heteroazeotrope
Prior art date: 1989-12-22

Application number

AT91401562T

Other languages

English (en)

Inventor

Raymond Hess

Christian Lacroix

Original Assignee

Atochem Elf Sa

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1989-12-22

Filing date

1991-06-12

Publication date

1995-11-15

1991-06-12 Application filed by Atochem Elf Sa filed Critical Atochem Elf Sa

1995-11-15 Application granted granted Critical

1995-11-15 Publication of ATE130001T1 publication Critical patent/ATE130001T1/de

Links

NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 title abstract 6
238000000034 method Methods 0.000 title abstract 2
SGFJJNBUMXQSMU-PDBXOOCHSA-N oxiran-2-ylmethyl (9z,12z,15z)-octadeca-9,12,15-trienoate Chemical class CC\C=C/C\C=C/C\C=C/CCCCCCCC(=O)OCC1CO1 SGFJJNBUMXQSMU-PDBXOOCHSA-N 0.000 title 1
238000004821 distillation Methods 0.000 abstract 6
125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 abstract 5
239000012535 impurity Substances 0.000 abstract 4
239000002904 solvent Substances 0.000 abstract 4
238000009835 boiling Methods 0.000 abstract 2
BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 abstract 1
238000000746 purification Methods 0.000 abstract 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/36—Azeotropic distillation
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/16—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by esterified hydroxyl radicals
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/13—Spirits
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/22—Accessories

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Epoxy Compounds (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

AT91401562T 1989-12-22 1991-06-12 Verfahren zur reinigung von glycidyl(meth)acrylat. ATE130001T1 (de)

Applications Claiming Priority (5)

Application Number	Priority Date	Filing Date	Title
FR8917135A FR2656305B1 (fr)	1989-12-22	1989-12-22	Procede de purification du (meth)acrylate de glycidyle.
EP91401562A EP0519139B1 (de)	1989-12-22	1991-06-12	Verfahren zur Reinigung von Glycidyl(meth)acrylat
CA002044981A CA2044981C (fr)	1989-12-22	1991-06-19	Procede de purification du (meth)acrylate de glycidyle
JP3148840A JPH0717626B2 (ja)	1989-12-22	1991-06-20	アクリル（メタクリル）酸グリシジルの精製方法
US07/717,289 US5207874A (en)	1989-12-22	1991-06-20	Process for the purification of glycidyl (meth)acrylate

Publications (1)

Publication Number	Publication Date
ATE130001T1 true ATE130001T1 (de)	1995-11-15

Family

ID=39276152

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT91401562T ATE130001T1 (de)	1989-12-22	1991-06-12	Verfahren zur reinigung von glycidyl(meth)acrylat.

Country Status (10)

Country	Link
US (1)	US5207874A (de)
EP (1)	EP0519139B1 (de)
JP (1)	JPH0717626B2 (de)
AT (1)	ATE130001T1 (de)
CA (1)	CA2044981C (de)
DE (1)	DE69114486T2 (de)
DK (1)	DK0519139T3 (de)
ES (1)	ES2079597T3 (de)
FR (1)	FR2656305B1 (de)
GR (1)	GR3018812T3 (de)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE4140373A1 (de) *	1991-12-07	1993-06-09	Henkel Kgaa, 4000 Duesseldorf, De	Verbesserte trockenneutralisation olefinisch reaktiver organischer fluessigphasen
JP3922310B2 (ja) *	1995-08-25	2007-05-30	三菱瓦斯化学株式会社	アクリル酸またはメタクリル酸のグリシジルエステルの製造方法
US6024839A (en) *	1997-11-06	2000-02-15	Shell Oil Company	Hydroquinone to inhibit fouling of epichlorohydrin equipment
JP4698778B2 (ja) *	1999-06-03	2011-06-08	株式会社日本触媒	（メタ）アクリル酸（エステル）の精製方法
JP4558870B2 (ja) *	1999-11-08	2010-10-06	株式会社日本触媒	塔式処理方法および装置
AU2001100399B4 (en) *	2000-12-28	2002-03-21	H Lundbeck As	Process for the preparation of pure citalopram
JP2006151854A (ja) *	2004-11-29	2006-06-15	Mitsubishi Gas Chem Co Inc	メタクリル酸グリシジルの製造方法
JP5471221B2 (ja) *	2009-09-14	2014-04-16	三菱化学エンジニアリング株式会社	Ｎｍｐの蒸留装置
FR3012140B1 (fr)	2013-10-18	2016-08-26	Arkema France	Unite et procede pour la purification de methacrylate de methyle brut
CN105218487A (zh) *	2015-09-11	2016-01-06	中昊(大连)化工研究设计院有限公司	一种甲基丙烯酸缩水甘油酯的生产方法
TW202528037A (zh) *	2023-11-02	2025-07-16	美商帷幕公司	縮水甘油(甲基)丙烯酸酯材料及使用方法
CN119792967B (zh) *	2024-12-26	2025-12-30	同济大学	一种用钾钠合金干燥有机溶剂且可循环多次使用的溶剂干燥装置及方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2772296A (en) *		1956-11-27		Process for preparing epoxy esters
US3075999A (en) *		1963-01-29		Glycidyl esteks
US2537981A (en) *	1949-10-28	1951-01-16	American Cyanamid Co	Method of producing a glycidyl ester
US3142686A (en) *	1960-05-16	1964-07-28	Shell Oil Co	Process for preparing epoxy esters of alpha, alpha-dialkyl monocarboxylic acids
US3239433A (en) *	1962-05-31	1966-03-08	Phillips Petroleum Co	Addition of oxygen during methylvinyl-pyridine distillation to prevent polymerization
JPS5123215A (ja) *	1974-08-12	1976-02-24	Nippon Catalytic Chem Ind	Akurirusangurishijiru mataha metakurirusangurishijiruno seiseihoho
JPS6037103B2 (ja) *	1977-01-18	1985-08-24	日本油脂株式会社	不飽和有機酸グリシジルエステルの製造法
JPS5517307A (en) *	1978-07-21	1980-02-06	Mitsubishi Gas Chem Co Inc	Preparation of glycidyl ester of acrylic or methacrylic acid
SU1175931A1 (ru) *	1983-04-11	1985-08-30	Valentina A Stepanova	"cпocoб oчиctkи cыpцa-глицидилmetakpилata ot глицидoлa"
JPS6110571A (ja) *	1984-06-25	1986-01-18	Mitsui Toatsu Chem Inc	グリシド−ルの精製方法
JPH0832693B2 (ja) *	1987-04-13	1996-03-29	大阪有機化学工業株式会社	アクリル酸グリシジルまたはメタクリル酸グリシジルの精製方法

1989
- 1989-12-22 FR FR8917135A patent/FR2656305B1/fr not_active Expired - Lifetime
1991
- 1991-06-12 AT AT91401562T patent/ATE130001T1/de not_active IP Right Cessation
- 1991-06-12 DE DE69114486T patent/DE69114486T2/de not_active Expired - Fee Related
- 1991-06-12 ES ES91401562T patent/ES2079597T3/es not_active Expired - Lifetime
- 1991-06-12 DK DK91401562.3T patent/DK0519139T3/da active
- 1991-06-12 EP EP91401562A patent/EP0519139B1/de not_active Expired - Lifetime
- 1991-06-19 CA CA002044981A patent/CA2044981C/fr not_active Expired - Fee Related
- 1991-06-20 US US07/717,289 patent/US5207874A/en not_active Expired - Fee Related
- 1991-06-20 JP JP3148840A patent/JPH0717626B2/ja not_active Expired - Lifetime
1996
- 1996-01-30 GR GR960400200T patent/GR3018812T3/el unknown

Also Published As

Publication number	Publication date
GR3018812T3 (en)	1996-04-30
US5207874A (en)	1993-05-04
EP0519139A1 (de)	1992-12-23
DE69114486T2 (de)	1996-03-21
DK0519139T3 (da)	1996-02-12
JPH0717626B2 (ja)	1995-03-01
FR2656305A1 (fr)	1991-06-28
DE69114486D1 (de)	1995-12-14
EP0519139B1 (de)	1995-11-08
JPH051050A (ja)	1993-01-08
CA2044981A1 (fr)	1992-12-20
ES2079597T3 (es)	1996-01-16
FR2656305B1 (fr)	1992-04-10
CA2044981C (fr)	1999-05-04

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Legal Events

Date	Code	Title	Description
1996-05-15	UEP	Publication of translation of european patent specification
2001-03-15	REN	Ceased due to non-payment of the annual fee