ATE169351T1 - Verfahren zur reinigung von zurückgewonnenen n- methylmorpholin-n-oxid-lösungen - Google Patents
Verfahren zur reinigung von zurückgewonnenen n- methylmorpholin-n-oxid-lösungenInfo
- Publication number
- ATE169351T1 ATE169351T1 AT95106176T AT95106176T ATE169351T1 AT E169351 T1 ATE169351 T1 AT E169351T1 AT 95106176 T AT95106176 T AT 95106176T AT 95106176 T AT95106176 T AT 95106176T AT E169351 T1 ATE169351 T1 AT E169351T1
- Authority
- AT
- Austria
- Prior art keywords
- methylmorpholine
- oxide
- solution
- oxidant
- aqueous
- Prior art date
Links
- LFTLOKWAGJYHHR-UHFFFAOYSA-N N-methylmorpholine N-oxide Chemical compound CN1(=O)CCOCC1 LFTLOKWAGJYHHR-UHFFFAOYSA-N 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 4
- 230000001590 oxidative effect Effects 0.000 abstract 5
- 239000000243 solution Substances 0.000 abstract 5
- 150000001412 amines Chemical class 0.000 abstract 4
- 239000007800 oxidant agent Substances 0.000 abstract 4
- SJRJJKPEHAURKC-UHFFFAOYSA-N N-Methylmorpholine Chemical compound CN1CCOCC1 SJRJJKPEHAURKC-UHFFFAOYSA-N 0.000 abstract 3
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 abstract 2
- 229920002678 cellulose Polymers 0.000 abstract 2
- 239000001913 cellulose Substances 0.000 abstract 2
- 238000007796 conventional method Methods 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 2
- 239000003456 ion exchange resin Substances 0.000 abstract 2
- 229920003303 ion-exchange polymer Polymers 0.000 abstract 2
- 238000009987 spinning Methods 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 229920003043 Cellulose fiber Polymers 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 230000015271 coagulation Effects 0.000 abstract 1
- 238000005345 coagulation Methods 0.000 abstract 1
- 238000004042 decolorization Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 239000011347 resin Substances 0.000 abstract 1
- 229920005989 resin Polymers 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F13/00—Recovery of starting material, waste material or solvents during the manufacture of artificial filaments or the like
- D01F13/02—Recovery of starting material, waste material or solvents during the manufacture of artificial filaments or the like of cellulose, cellulose derivatives or proteins
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/42—Treatment of water, waste water, or sewage by ion-exchange
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/72—Treatment of water, waste water, or sewage by oxidation
- C02F1/722—Oxidation by peroxides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D265/00—Heterocyclic compounds containing six-membered rings having one nitrogen atom and one oxygen atom as the only ring hetero atoms
- C07D265/28—1,4-Oxazines; Hydrogenated 1,4-oxazines
- C07D265/30—1,4-Oxazines; Hydrogenated 1,4-oxazines not condensed with other rings
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D1/00—Treatment of filament-forming or like material
- D01D1/10—Filtering or de-aerating the spinning solution or melt
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
- Y02P70/62—Manufacturing or production processes characterised by the final manufactured product related technologies for production or treatment of textile or flexible materials or products thereof, including footwear
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Mechanical Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR1019940008948A KR0125960B1 (ko) | 1994-04-27 | 1994-04-27 | 회수한 n-메틸몰포린 n-옥사이드 수용액의 탈색정제방법 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE169351T1 true ATE169351T1 (de) | 1998-08-15 |
Family
ID=19381829
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT95106176T ATE169351T1 (de) | 1994-04-27 | 1995-04-25 | Verfahren zur reinigung von zurückgewonnenen n- methylmorpholin-n-oxid-lösungen |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US5611932A (de) |
| EP (1) | EP0679739B1 (de) |
| KR (1) | KR0125960B1 (de) |
| AT (1) | ATE169351T1 (de) |
| DE (1) | DE69503826T2 (de) |
| ES (1) | ES2120656T3 (de) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2206990A1 (en) * | 1994-12-15 | 1996-06-20 | Akzo Nobel N.V. | Process for producing cellulosic moldings |
| AT404033B (de) * | 1996-07-02 | 1998-07-27 | Chemiefaser Lenzing Ag | Verfahren zur herstellung einer wässrigen lösung von n-methylmorpholin-n-oxid |
| DE19821176C2 (de) * | 1998-05-12 | 2001-02-08 | Ostthueringische Materialpruef | Verfahren zur Aufbereitung wäßriger N-Methylmorpholin-N-oxid-Lösungen |
| US6409883B1 (en) | 1999-04-16 | 2002-06-25 | Kimberly-Clark Worldwide, Inc. | Methods of making fiber bundles and fibrous structures |
| US6896809B2 (en) * | 2002-12-20 | 2005-05-24 | Providence Health System - Oregon | Methods for purifying chitosan |
| CA2855945C (en) * | 2011-10-12 | 2018-02-27 | United Laboratories International, Llc | Process for decontamination of hazardous sulfur compounds in sour water tanks |
| CN105921131A (zh) * | 2016-05-24 | 2016-09-07 | 马鞍山中创环保科技有限公司 | 一种银提取材料的制备方法 |
| CN109183199A (zh) * | 2018-11-22 | 2019-01-11 | 淮安天然丝纺织科技有限公司 | 一种nmmo溶剂回收浓缩方法 |
| CN110055626A (zh) * | 2019-04-23 | 2019-07-26 | 福建宏远集团有限公司 | 一种纺丝n-甲基吗啉-n氧化物溶液的回收方法 |
| CN113651773A (zh) * | 2021-09-23 | 2021-11-16 | 上海昶法新材料有限公司 | 一种氧化甲基吗啉的合成和提纯方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1427011A1 (ru) * | 1985-08-19 | 1988-09-30 | Предприятие П/Я А-3844 | Способ регенерации N-метилморфолин-N-оксида из технологических растворов при производстве гидратцеллюлозных волокон |
| DE3618352A1 (de) * | 1986-05-31 | 1987-12-03 | Huels Chemische Werke Ag | Verfahren zur herstellung von waessrigen n-methylmorpholin-n-oxid-loesungen |
| DD254199B5 (de) * | 1986-12-04 | 1994-01-05 | Thueringische Faser Ag Schwarz | Verfahren zur reinigung waessriger n-methylmorpholin-n-oxyd-loesungen |
| DD259863A1 (de) * | 1987-04-06 | 1988-09-07 | Schwarza Chemiefaser | Verfahren zur herstellung waessriger, reiner n-methylmorpholin-n-oxid-loesungen |
| DD274435B5 (de) * | 1988-08-02 | 1996-10-31 | Thueringisches Inst Textil | Verfahren zur Rueckgewinnung von N-Methylmorpholin-N-Oxid |
| AT392776B (de) * | 1989-10-16 | 1991-06-10 | Chemiefaser Lenzing Ag | Verfahren zur reinigung waesseriger loesungen von n-methylmorpholin-n-oxid |
| AT392915B (de) * | 1990-03-28 | 1991-07-10 | Chemiefaser Lenzing Ag | Verfahren zum abtrennen von wasser aus einer verduennten waesserigen loesung von n-methylmorpholin-n-oxid, n-methylmorpholin und/oder morpholin |
| AT395246B (de) * | 1990-07-16 | 1992-10-27 | Chemiefaser Lenzing Ag | Loesung von cellulose in wasser und n-methyl-morpholin-n-oxid |
| AT395608B (de) * | 1990-11-26 | 1993-02-25 | Chemiefaser Lenzing Ag | Verfahren zur reinigung von waesserigen n-methylmorpholin-n-oxid-loesungen |
| GB9125594D0 (en) * | 1991-12-02 | 1992-01-29 | Courtaulds Plc | Purifying solutions |
-
1994
- 1994-04-27 KR KR1019940008948A patent/KR0125960B1/ko not_active Expired - Lifetime
-
1995
- 1995-03-30 US US08/413,302 patent/US5611932A/en not_active Expired - Lifetime
- 1995-04-25 AT AT95106176T patent/ATE169351T1/de active
- 1995-04-25 EP EP95106176A patent/EP0679739B1/de not_active Expired - Lifetime
- 1995-04-25 DE DE69503826T patent/DE69503826T2/de not_active Expired - Lifetime
- 1995-04-25 ES ES95106176T patent/ES2120656T3/es not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0679739B1 (de) | 1998-08-05 |
| KR950029259A (ko) | 1995-11-22 |
| KR0125960B1 (ko) | 1997-12-24 |
| EP0679739A1 (de) | 1995-11-02 |
| ES2120656T3 (es) | 1998-11-01 |
| US5611932A (en) | 1997-03-18 |
| DE69503826T2 (de) | 1999-04-22 |
| DE69503826D1 (de) | 1998-09-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| UEP | Publication of translation of european patent specification |