ATE1894T1 - Verfahren zur herstellung von siliziumdioxidaerogel und seine verwendung. - Google Patents
Verfahren zur herstellung von siliziumdioxidaerogel und seine verwendung.Info
- Publication number
- ATE1894T1 ATE1894T1 AT80850055T AT80850055T ATE1894T1 AT E1894 T1 ATE1894 T1 AT E1894T1 AT 80850055 T AT80850055 T AT 80850055T AT 80850055 T AT80850055 T AT 80850055T AT E1894 T1 ATE1894 T1 AT E1894T1
- Authority
- AT
- Austria
- Prior art keywords
- aerogel
- alcohol
- autoclave
- alcogel
- preparation
- Prior art date
Links
- 239000004964 aerogel Substances 0.000 title abstract 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 235000012239 silicon dioxide Nutrition 0.000 title 1
- 239000000377 silicon dioxide Substances 0.000 title 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 238000002360 preparation method Methods 0.000 abstract 2
- 239000004965 Silica aerogel Substances 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/157—After-treatment of gels
- C01B33/158—Purification; Drying; Dehydrating
- C01B33/1585—Dehydration into aerogels
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE7903766A SE422045C (sv) | 1979-04-30 | 1979-04-30 | Sett att framstella silikaaerogel i form av ett vesentligen sprickfritt, foretredesvis transparent block samt anvendning av detsamma i solpaneler |
| EP80850055A EP0018955B1 (de) | 1979-04-30 | 1980-04-17 | Verfahren zur Herstellung von Siliziumdioxid-Aerogel und seine Verwendung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE1894T1 true ATE1894T1 (de) | 1982-12-15 |
Family
ID=20337932
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT80850055T ATE1894T1 (de) | 1979-04-30 | 1980-04-17 | Verfahren zur herstellung von siliziumdioxidaerogel und seine verwendung. |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4327065A (de) |
| EP (1) | EP0018955B1 (de) |
| AT (1) | ATE1894T1 (de) |
| DE (1) | DE3061197D1 (de) |
| SE (1) | SE422045C (de) |
Families Citing this family (59)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2507171A1 (fr) * | 1981-06-04 | 1982-12-10 | Zarzycki Jerzy | Aerogels de silice monolithiques, leur preparation et leur utilisation pour la preparation d'articles en verre de silice et de materiaux thermiquement isolants |
| US4717708A (en) * | 1983-12-27 | 1988-01-05 | Stauffer Chemical Company | Inorganic oxide aerogels and their preparation |
| NL8403667A (nl) * | 1984-12-03 | 1986-07-01 | Philips Nv | Werkwijze voor de vervaardiging van monolitische glaslichamen. |
| JPS6287409A (ja) * | 1985-09-09 | 1987-04-21 | Tama Kagaku Kogyo Kk | 合成シリカの製造方法 |
| DE3533805C2 (de) * | 1985-09-21 | 1996-02-29 | Basf Ag | Verfahren zur Herstellung von Isolierscheiben mit hoher Wärme- und/oder Schallisolierung |
| US4810415A (en) * | 1985-09-24 | 1989-03-07 | Dresser Industries, Inc. | Process for manufacturing ultra pure silica and resulting encapsulated products |
| DE3616133A1 (de) * | 1985-09-25 | 1987-11-19 | Merck Patent Gmbh | Kugelfoermige sio(pfeil abwaerts)2(pfeil abwaerts)-partikel |
| DE3614978A1 (de) * | 1986-05-02 | 1987-11-12 | Heinz Kunert | Wand- und/oder bruestungselement |
| JPH0796447B2 (ja) * | 1986-06-13 | 1995-10-18 | モ−ゼス レイク インダストリ−ズ インコ−ポレイテツド | 高純度シリカの製造方法 |
| US4776867A (en) * | 1986-08-15 | 1988-10-11 | Gte Laboratories Incorporated | Process for molding optical components of silicate glass to a near net shape optical precision |
| DE3702481A1 (de) * | 1987-01-28 | 1988-08-11 | Philips Patentverwaltung | Gasentladungslampe |
| US4765818A (en) * | 1987-02-24 | 1988-08-23 | Hoechst Celanese Corporation | Porous glass monoliths |
| US4940571A (en) * | 1988-04-01 | 1990-07-10 | Gte Laboratories Incorporated | Method of making large particle size, high purity dense silica |
| US4943425A (en) * | 1988-04-01 | 1990-07-24 | Gte Laboratories Incorporated | Method of making high purity dense silica of large particle size |
| DE3814968A1 (de) | 1988-05-03 | 1989-11-16 | Basf Ag | Daemmstoff der dichte 0,1 bis 0,4 g/cm(pfeil hoch)3(pfeil hoch) |
| GB8828634D0 (en) * | 1988-12-08 | 1989-01-11 | Glaverbel | Composite glazing panel |
| US5078919A (en) * | 1990-03-20 | 1992-01-07 | The United States Of America As Represented By The United States Department Of Energy | Composition containing aerogel substrate loaded with tritium |
| US5122305A (en) * | 1990-03-20 | 1992-06-16 | Ashley Carol S | Solid-state radiation-emitting compositions and devices |
| US5240647A (en) * | 1990-03-20 | 1993-08-31 | Ashley Carol S | Process for making solid-state radiation-emitting composition |
| US5137659A (en) * | 1990-03-20 | 1992-08-11 | The United States Of America As Represented By The United States Department Of Energy | Solid-state radiation-emitting compositions and devices |
| US5409683A (en) * | 1990-08-23 | 1995-04-25 | Regents Of The University Of California | Method for producing metal oxide aerogels |
| NO912006D0 (no) * | 1991-05-24 | 1991-05-24 | Sinvent As | Fremgangsmaate for fremstilling av et silika-aerogel-lignende materiale. |
| US5306555A (en) * | 1991-09-18 | 1994-04-26 | Battelle Memorial Institute | Aerogel matrix composites |
| US5360572A (en) * | 1991-11-29 | 1994-11-01 | The United States Of America As Represented By The Secretary Of The Air Force | Aerogel mesh getter |
| US5308533A (en) * | 1991-11-29 | 1994-05-03 | The United States Of America As Represented By The Secretary Of The Air Force | Aerogel mesh getter |
| DE4201306A1 (de) * | 1992-01-20 | 1993-07-22 | Basf Ag | Formteile oder platten aus silica-aerogelen |
| US6156223A (en) * | 1993-04-26 | 2000-12-05 | Armstrong World Industries, Inc. | Xerogels and their preparation |
| US5473826A (en) * | 1994-08-19 | 1995-12-12 | Yazaki Corporation | Process for drying sol-gel derived porous bodies at elevated subcritical temperatures and pressures |
| US5686031A (en) * | 1995-01-05 | 1997-11-11 | Regents Of The University Of California | Method for rapidly producing microporous and mesoporous materials |
| DE19506141A1 (de) | 1995-02-22 | 1996-08-29 | Hoechst Ag | Verwendung von Aerogelen in der Pharmazie, in der Kosmetik und im Pflanzenschutz |
| DE19507732A1 (de) * | 1995-03-07 | 1996-09-12 | Hoechst Ag | Transparentes Bauelement, enthaltend mindestens eine faserverstärkte Aerogelplatte und/oder -matte |
| FR2736342B1 (fr) * | 1995-07-07 | 1999-01-29 | Univ Claude Bernard Lyon | Procede pour la fabrication d'aerogels de silice monolithiques et aerogels de silice ainsi obtenus |
| DE19533851A1 (de) * | 1995-09-13 | 1997-03-20 | Hoechst Ag | Organofunktionalisierte Aerogele |
| US6090861A (en) * | 1998-12-28 | 2000-07-18 | General Ideas, Inc. | Process for high temperature production of organic aerogels |
| US6077876A (en) * | 1997-12-29 | 2000-06-20 | General Ideas, Inc. | Process for high temperature production of organic aerogels |
| KR100264157B1 (ko) * | 1998-03-17 | 2001-04-02 | 박호군 | 메탄의이산화탄소개질반응용니켈-알루미나에어로젤촉매및이의제조방법 |
| DE19847634C1 (de) * | 1998-10-15 | 2000-02-10 | Saskia Solar Und Energietechni | Wärmeisolationspaneel |
| US6586501B1 (en) | 1999-01-20 | 2003-07-01 | Cabot Corporation | Aggregates having attached polymer groups and polymer foams |
| US6258864B1 (en) | 1999-01-20 | 2001-07-10 | Cabot Corporation | Polymer foam containing chemically modified carbonaceous filler |
| US6168694B1 (en) | 1999-02-04 | 2001-01-02 | Chemat Technology, Inc. | Methods for and products of processing nanostructure nitride, carbonitride and oxycarbonitride electrode power materials by utilizing sol gel technology for supercapacitor applications |
| US6339034B1 (en) | 2000-01-24 | 2002-01-15 | Hc Chem Research & Service Corp. | Light-weight ceramic insulation |
| US7641954B2 (en) | 2003-10-03 | 2010-01-05 | Cabot Corporation | Insulated panel and glazing system comprising the same |
| US7621299B2 (en) | 2003-10-03 | 2009-11-24 | Cabot Corporation | Method and apparatus for filling a vessel with particulate matter |
| US20060019084A1 (en) * | 2004-07-23 | 2006-01-26 | Pearson Laurence T | Monolithic composition and method |
| PT103257B (pt) | 2005-04-05 | 2007-05-31 | Inst Superior Tecnico | Método de produção subcrítica de xerogéis e aerogéis monolíticos híbridos de sílica e látex modificado com grupos alcoxissilano |
| CN100537215C (zh) * | 2005-04-22 | 2009-09-09 | 海尔集团公司 | 一种宇航绝热板及其制备工艺 |
| US7444687B2 (en) * | 2005-08-29 | 2008-11-04 | 3M Innovative Properties Company | Hearing protective device that includes cellular earmuffs |
| US20070044206A1 (en) * | 2005-08-29 | 2007-03-01 | Sato Luciana M | Hearing protective earmuff device having frictionally engageable ear cups |
| US8114336B2 (en) * | 2007-03-16 | 2012-02-14 | Board Of Regents Of The University Of Texas System | Methods for increasing the strength and controlling the architecture and composition of ceramic articles |
| WO2009151604A1 (en) * | 2008-06-12 | 2009-12-17 | Yunzhi Yang | Methods for making ceramic articles, including ceramic scaffolds for bone repair |
| SE533051C2 (sv) * | 2009-01-08 | 2010-06-15 | Airglass Ab | Silikaaerogelkropp som transparent panel i energifönster |
| SE0950004A1 (sv) * | 2009-01-08 | 2010-06-15 | Airglass Ab | Silikaaerogelkropp som isolering i ett solfångarsystem |
| TW201239495A (en) * | 2011-03-25 | 2012-10-01 | Jtouch Corp | Electrochromic apparatus |
| WO2019044669A1 (ja) * | 2017-09-01 | 2019-03-07 | Agc株式会社 | 湿潤ゲル、キセロゲルの製造方法 |
| JP7565671B2 (ja) * | 2018-11-07 | 2024-10-11 | 三菱ケミカル株式会社 | シリカゾルの製造方法及びシリカゾル中の中間生成物の抑制方法 |
| US20210363812A1 (en) * | 2020-05-20 | 2021-11-25 | Union College | Aerogel Mosaic-based Window System |
| EP4490104A1 (de) | 2022-03-09 | 2025-01-15 | Cardinal CG Company | Feuchtes kieselsäuregel und aerogel |
| CN115433020B (zh) * | 2022-08-20 | 2023-04-28 | 浙江大学 | 一种二氧化硅气凝胶隔热材料的制备方法 |
| CN119750597A (zh) * | 2025-01-10 | 2025-04-04 | 烟台大学 | 一种利用电子束辐照技术加速合成二氧化硅气凝胶的方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE482176C (de) * | 1918-12-07 | 1929-09-09 | Silica Gel Corp | Verfahren zur Herstellung einer stark porigen, adsorbierenden Masse |
| US2093454A (en) * | 1934-10-01 | 1937-09-21 | Samuel S Kistler | Method of producing aerogels |
| US2249767A (en) * | 1937-07-03 | 1941-07-22 | Monsanto Chemicals | Method of making aerogels |
| US3165379A (en) * | 1962-03-14 | 1965-01-12 | Socony Mobil Oil Co Inc | Preparation of siliceous aerogels |
| JPS4018266Y1 (de) * | 1962-08-31 | 1965-06-28 | ||
| US3434912A (en) * | 1965-11-22 | 1969-03-25 | Standard Oil Co | Self-sustaining,thin,crack-free sheet of inorganic aerogel |
| FR1568817A (de) * | 1967-11-30 | 1969-05-30 | ||
| US3681017A (en) * | 1970-07-06 | 1972-08-01 | Grace W R & Co | Platelet silica,its production and uses |
| FR2332234A1 (fr) * | 1975-11-20 | 1977-06-17 | Rhone Poulenc Ind | Corps siliceux agglomeres |
| DE2649472A1 (de) * | 1976-10-29 | 1978-05-03 | Schoell Guenter | Lichtdurchlaessige waermedaemmung |
-
1979
- 1979-04-30 SE SE7903766A patent/SE422045C/sv not_active IP Right Cessation
-
1980
- 1980-04-17 DE DE8080850055T patent/DE3061197D1/de not_active Expired
- 1980-04-17 AT AT80850055T patent/ATE1894T1/de active
- 1980-04-17 EP EP80850055A patent/EP0018955B1/de not_active Expired
- 1980-04-22 US US06/142,812 patent/US4327065A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0018955B1 (de) | 1982-12-01 |
| SE7903766L (sv) | 1980-10-31 |
| SE422045C (sv) | 1985-03-18 |
| SE422045B (sv) | 1982-02-15 |
| EP0018955A1 (de) | 1980-11-12 |
| US4327065A (en) | 1982-04-27 |
| DE3061197D1 (en) | 1983-01-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ATE1894T1 (de) | Verfahren zur herstellung von siliziumdioxidaerogel und seine verwendung. | |
| ATE208739T1 (de) | Verfahren zur herstellung einer hochkonzentrierten kolloidalen kieselsäure- suspension und des dabei hergestellten produktes | |
| JPS56104732A (en) | Preparation of silica glass | |
| ATE222565T1 (de) | Verfahren zur herstellung von wässrigen lösungen von freiem hydroxylamin | |
| DE3772307D1 (de) | Verfahren zur reinigung von propandiol-1,3. | |
| DE3784907D1 (de) | Oligosaccharide, immunogene und impstoffe und verfahren zur herstellung dieser oligosaccharide, immunogene und impstoffe. | |
| ATE119135T1 (de) | Verfahren zur hydrothermalen herstellung von kaliumsilikatlösungen mit hohem si02:k20- molverhältnis. | |
| DE3861191D1 (de) | Verfahren zur herstellung von kristalliner l-arabinose. | |
| DE58905753D1 (de) | Verfahren zur herstellung von alkoholarmem bier. | |
| DE69020729D1 (de) | Dämmstoff aus mineralwolle für die röhrenwärmedämmung und verfahren zur herstellung. | |
| DE3778073D1 (de) | Verfahren zur herstellung von kohle- oder koksbriketts. | |
| ES2004461A6 (es) | Procedimiento perfeccionado para la produccion de anhidrido borico a partir de acido borico | |
| ATE14984T1 (de) | Verfahren zur herstellung eines biochemischen vakzins gegen salmonellenfieber. | |
| JPS55167143A (en) | Manufacture of optical glass | |
| ATE2073T1 (de) | Verfahren zur herstellung von reiner cyanursaeure. | |
| DE3372210D1 (en) | Method for preparing organo germanium propionic acid derivatives | |
| ATE6270T1 (de) | Verfahren zum aufwerten von hopfenbitterstoffen durch phototransformation und vorrichtung zur durchfuehrung dieses verfahrens. | |
| DE3470026D1 (en) | Process for making monolithic glass objects | |
| SU1549917A1 (ru) | Способ очистки диоксида кремни | |
| ES423260A1 (es) | Un procedimiento para separar el fluor de las soluciones deacido fosforico. | |
| SU136046A1 (ru) | Способ гидрофобизации поливинилспиртовых волокон | |
| JPS6483528A (en) | Production of glass | |
| KR890004984A (ko) | 열수 물유리의 제조 방법 | |
| Esquivias et al. | present study is to establish a systematic comparison between the | |
| 野上正行 et al. | Dehydration of glass prepared by gel process from Si (OC2H5) 4. |