ATE239691T1 - Verfahren und einrichtung zum herstellen von butylacetat und isobutylacetat - Google Patents
Verfahren und einrichtung zum herstellen von butylacetat und isobutylacetatInfo
- Publication number
- ATE239691T1 ATE239691T1 AT99915571T AT99915571T ATE239691T1 AT E239691 T1 ATE239691 T1 AT E239691T1 AT 99915571 T AT99915571 T AT 99915571T AT 99915571 T AT99915571 T AT 99915571T AT E239691 T1 ATE239691 T1 AT E239691T1
- Authority
- AT
- Austria
- Prior art keywords
- separation
- esterification
- acetic acid
- separated
- components
- Prior art date
Links
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 title abstract 3
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 title abstract 3
- GJRQTCIYDGXPES-UHFFFAOYSA-N iso-butyl acetate Natural products CC(C)COC(C)=O GJRQTCIYDGXPES-UHFFFAOYSA-N 0.000 title abstract 2
- FGKJLKRYENPLQH-UHFFFAOYSA-M isocaproate Chemical compound CC(C)CCC([O-])=O FGKJLKRYENPLQH-UHFFFAOYSA-M 0.000 title abstract 2
- OQAGVSWESNCJJT-UHFFFAOYSA-N isovaleric acid methyl ester Natural products COC(=O)CC(C)C OQAGVSWESNCJJT-UHFFFAOYSA-N 0.000 title abstract 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 9
- 238000000926 separation method Methods 0.000 abstract 6
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 abstract 4
- 230000032050 esterification Effects 0.000 abstract 4
- 238000005886 esterification reaction Methods 0.000 abstract 4
- 238000006243 chemical reaction Methods 0.000 abstract 3
- 239000012074 organic phase Substances 0.000 abstract 3
- 230000002378 acidificating effect Effects 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 2
- 229940043232 butyl acetate Drugs 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- 238000010992 reflux Methods 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- 229940035429 isobutyl alcohol Drugs 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CZ98901A CZ90198A3 (cs) | 1998-03-25 | 1998-03-25 | Způsob výroby izobutylacetátu a zařízení k provádění tohoto způsobu |
| CZ98902A CZ285559B6 (cs) | 1998-03-25 | 1998-03-25 | Způsob výroby butylacetátu a zařízení k provádění tohoto způsobu |
| PCT/EP1999/001583 WO1999048855A1 (en) | 1998-03-25 | 1999-03-11 | Process and apparatus for the production of butylacetate and isobutylacetate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE239691T1 true ATE239691T1 (de) | 2003-05-15 |
Family
ID=25746874
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT99915571T ATE239691T1 (de) | 1998-03-25 | 1999-03-11 | Verfahren und einrichtung zum herstellen von butylacetat und isobutylacetat |
Country Status (12)
| Country | Link |
|---|---|
| US (2) | US6458992B1 (de) |
| EP (1) | EP1066242B1 (de) |
| JP (1) | JP4418589B2 (de) |
| KR (1) | KR100563596B1 (de) |
| AT (1) | ATE239691T1 (de) |
| AU (1) | AU3410799A (de) |
| BR (1) | BR9909040B1 (de) |
| CA (1) | CA2325479C (de) |
| DE (1) | DE69907653T2 (de) |
| MY (1) | MY118647A (de) |
| TW (1) | TWI250148B (de) |
| WO (1) | WO1999048855A1 (de) |
Families Citing this family (40)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CZ292620B6 (cs) * | 1999-10-14 | 2003-11-12 | Sulzer Chemtech Ltd. | Způsob výroby etylacetátu a zařízení k provádění tohoto způsobu |
| TW575557B (en) * | 2001-12-05 | 2004-02-11 | Ind Tech Res Inst | Preparation method for carboxylate |
| US7199263B2 (en) * | 2004-08-18 | 2007-04-03 | Celanese International Corporation | Acetic anhydride and acetate ester co-production |
| TW200635892A (en) * | 2005-02-10 | 2006-10-16 | Sulzer Chemtech Ag | A method for the manufacture of carboxylic acid ester by means of a reactive distillation |
| EP1690849B1 (de) | 2005-02-10 | 2009-08-26 | Sulzer Chemtech AG | Verfahren zur Herstellung von Carbonsäureester mittels einer Reaktivdestillation |
| KR100707831B1 (ko) * | 2005-12-22 | 2007-04-13 | 한국에너지기술연구원 | 노말 부틸아세테이트를 제조하는 방법 및 그 제조 장치 |
| BRPI0707394A2 (pt) * | 2006-02-28 | 2011-05-03 | Shell Internationale Res Maartschappij B V | processo para destilação reativa |
| US20080044324A1 (en) * | 2006-08-16 | 2008-02-21 | Agency For Science, Technology And Research | Recirculating reactor |
| US9353042B2 (en) | 2010-08-20 | 2016-05-31 | Enerkem, Inc. | Production of acetates from acetic acid and alcohols |
| PT2012164573W (pt) | 2011-05-27 | 2014-10-08 | Reliance Ind Ltd | Procedimento para a preparação de um ácido carboxílico orgânico por hidrólise de um ester de ácido carboxílico orgânico |
| US8829207B2 (en) | 2011-06-24 | 2014-09-09 | Eastman Chemical Company | Production of cyclic acetals by reactive distillation |
| US9000229B2 (en) | 2011-06-24 | 2015-04-07 | Eastman Chemical Company | Production of hydroxy ether hydrocarbons by vapor phase hydrogenolysis of cyclic acetals and ketals |
| US9056313B2 (en) | 2011-06-24 | 2015-06-16 | Eastman Chemical Company | Catalysts for the production of hydroxy ether hydrocarbons by vapor phase hydrogenolysis of cyclic acetals and ketals |
| US8969598B2 (en) | 2011-06-24 | 2015-03-03 | Eastman Chemical Company | Production of cyclic acetals or ketals using liquid-phase acid catalysts |
| US9388105B2 (en) | 2011-06-24 | 2016-07-12 | Eastman Chemical Company | Production of hydroxy ether hydrocarbons by liquid phase hydrogenolysis of cyclic acetals or cyclic ketals |
| US8829206B2 (en) | 2011-06-24 | 2014-09-09 | Eastman Chemical Company | Production of cyclic acetals or ketals using solid acid catalysts |
| US8785697B2 (en) | 2011-06-24 | 2014-07-22 | Eastman Chemical Company | Nickel modified catalyst for the production of hydroxy ether hydrocarbons by vapor phase hydrogenolysis of cyclic acetals and ketals |
| CN104096523B (zh) * | 2014-07-25 | 2016-02-03 | 广西众昌树脂有限公司 | 聚酯反应设备 |
| KR20180019611A (ko) | 2015-06-23 | 2018-02-26 | 쉘 인터내셔날 리써취 마트샤피지 비.브이. | 폐수 처리를 위한 반응성 증류를 위한 장치 및 방법 |
| US11365357B2 (en) | 2019-05-24 | 2022-06-21 | Eastman Chemical Company | Cracking C8+ fraction of pyoil |
| CN113993977B (zh) | 2019-05-24 | 2024-09-13 | 伊士曼化工公司 | 进入气体裂化器中加工的液体流中混入少量热解油 |
| WO2020242921A1 (en) | 2019-05-24 | 2020-12-03 | Eastman Chemical Company | Recycle content cellulose ester |
| WO2020247192A1 (en) | 2019-05-24 | 2020-12-10 | Eastman Chemical Company | Recycle content cracked effluent |
| EP3976734A4 (de) | 2019-05-24 | 2023-03-15 | Eastman Chemical Company | Cracken einer c4-c7-fraktion von pyrolyseöl |
| KR102257110B1 (ko) * | 2019-07-23 | 2021-05-27 | 한국과학기술원 | 에너지 감축형 반응 증류에 의한 복수의 에스테르의 동시 제조 장치 및 방법 |
| US12338211B2 (en) | 2019-07-29 | 2025-06-24 | Eastman Chemical Company | Recycle content (C4)alkanal |
| US12534590B2 (en) | 2019-07-29 | 2026-01-27 | Eastman Chemical Company | Recycle content cyclobutane diol polyester |
| JP7690462B2 (ja) | 2019-08-30 | 2025-06-10 | シエル・インターナシヨナル・リサーチ・マートスハツペイ・ベー・ヴエー | 有機カーボネート生成プロセス |
| US11945998B2 (en) | 2019-10-31 | 2024-04-02 | Eastman Chemical Company | Processes and systems for making recycle content hydrocarbons |
| WO2021087057A1 (en) | 2019-10-31 | 2021-05-06 | Eastman Chemical Company | Pyrolysis method and system for recycled waste |
| US12528995B2 (en) | 2019-10-31 | 2026-01-20 | ExxonMobil Product Solutions Company | Pyrolysis method and system for recycled waste |
| US11319262B2 (en) | 2019-10-31 | 2022-05-03 | Eastman Chemical Company | Processes and systems for making recycle content hydrocarbons |
| EP4055001A4 (de) | 2019-11-07 | 2024-02-14 | Eastman Chemical Company | Gemischte ester und lösungsmittel mit recyceltem inhalt |
| EP4054996A4 (de) | 2019-11-07 | 2024-03-27 | Eastman Chemical Company | Oxoalkohole und oxoweichmacher mit recyceltem inhalt |
| KR20220093368A (ko) | 2019-11-07 | 2022-07-05 | 이스트만 케미칼 컴파니 | 재활용물 알파 올레핀 및 지방 알코올 |
| CN118851872A (zh) | 2019-11-07 | 2024-10-29 | 伊士曼化工公司 | 回收成分丙醇 |
| CN111298725B (zh) * | 2020-04-24 | 2024-12-24 | 弥勒市康和甘油酯有限公司 | 一种三乙酸甘油酯生产用酯化反应塔 |
| EP4141009A1 (de) * | 2021-08-30 | 2023-03-01 | Saltigo GmbH | Verfahren zur herstellung von mischungen enthaltend 2 (2 hydroxyethyl)-piperidinyl-carbamidsäure-sek.-butylester |
| US12195674B2 (en) | 2021-09-21 | 2025-01-14 | Eastman Chemical Company | Using spent caustic solution from pygas treatment to neutralize halogens from liquified waste plastic |
| CN115672245A (zh) * | 2022-10-10 | 2023-02-03 | 南通百川新材料有限公司 | 一种新型的乙酸正丁酯酯化生产设备及方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2364341A (en) * | 1941-04-24 | 1944-12-05 | Eastman Kodak Co | Distillation control |
| FR1399653A (fr) * | 1964-04-06 | 1965-05-21 | Melle Usines Sa | Procédé continu de préparation de dérivés fonctionnels d'alcools |
| US5235102A (en) * | 1990-11-20 | 1993-08-10 | Amoco Corporation | Catalytic distillation using rigid, cellular monoliths as catalyst-packing material |
| FR2684893A1 (fr) * | 1991-12-16 | 1993-06-18 | Inst Francais Du Petrole | Procede de distillation reactive catalytique et appareillage pour sa mise en óoeuvre. |
| KR960006546B1 (ko) * | 1993-07-28 | 1996-05-17 | 한국과학기술연구원 | 초산에스테르의 제조 방법 |
| CN1036648C (zh) | 1994-07-16 | 1997-12-10 | 广西大学 | 连续催化精馏生产醋酸正丁酯的方法及设备 |
| BE1014031A3 (fr) * | 1997-07-04 | 2003-03-04 | Basf Ag | La preparation d'esters. |
-
1999
- 1999-03-11 US US09/647,013 patent/US6458992B1/en not_active Expired - Lifetime
- 1999-03-11 AT AT99915571T patent/ATE239691T1/de active
- 1999-03-11 BR BRPI9909040-6A patent/BR9909040B1/pt not_active IP Right Cessation
- 1999-03-11 CA CA002325479A patent/CA2325479C/en not_active Expired - Fee Related
- 1999-03-11 WO PCT/EP1999/001583 patent/WO1999048855A1/en not_active Ceased
- 1999-03-11 DE DE69907653T patent/DE69907653T2/de not_active Expired - Lifetime
- 1999-03-11 JP JP2000537840A patent/JP4418589B2/ja not_active Expired - Fee Related
- 1999-03-11 EP EP99915571A patent/EP1066242B1/de not_active Expired - Lifetime
- 1999-03-11 KR KR1020007010525A patent/KR100563596B1/ko not_active Expired - Fee Related
- 1999-03-11 AU AU34107/99A patent/AU3410799A/en not_active Abandoned
- 1999-03-23 MY MYPI99001095A patent/MY118647A/en unknown
- 1999-03-30 TW TW088105170A patent/TWI250148B/zh not_active IP Right Cessation
-
2002
- 2002-07-15 US US10/196,298 patent/US7160524B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| AU3410799A (en) | 1999-10-18 |
| DE69907653T2 (de) | 2003-11-27 |
| CA2325479C (en) | 2008-01-15 |
| BR9909040A (pt) | 2000-12-05 |
| BR9909040B1 (pt) | 2010-11-16 |
| DE69907653D1 (de) | 2003-06-12 |
| KR100563596B1 (ko) | 2006-03-22 |
| EP1066242A1 (de) | 2001-01-10 |
| CA2325479A1 (en) | 1999-09-30 |
| MY118647A (en) | 2004-12-31 |
| TWI250148B (en) | 2006-03-01 |
| WO1999048855A1 (en) | 1999-09-30 |
| JP2002507588A (ja) | 2002-03-12 |
| US20020183545A1 (en) | 2002-12-05 |
| JP4418589B2 (ja) | 2010-02-17 |
| KR20010042126A (ko) | 2001-05-25 |
| US6458992B1 (en) | 2002-10-01 |
| US7160524B2 (en) | 2007-01-09 |
| EP1066242B1 (de) | 2003-05-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| UEP | Publication of translation of european patent specification |
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