ATE252592T1 - Verfahren zur reinigung von 2-keto-l-gulonic säure - Google Patents

Verfahren zur reinigung von 2-keto-l-gulonic säure

Info

Publication number: ATE252592T1
Authority: AT; Austria
Prior art keywords: keto; gulonic acid; purifying; purification; ion exchange
Prior art date: 1999-08-02

Application number

AT00950892T

Other languages

English (en)

Inventor

Kevin M Moore

Original Assignee

Archer Daniels Midland Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1999-08-02

Filing date

2000-07-31

Publication date

2003-11-15

2000-07-31 Application filed by Archer Daniels Midland Co filed Critical Archer Daniels Midland Co

2003-11-15 Application granted granted Critical

2003-11-15 Publication of ATE252592T1 publication Critical patent/ATE252592T1/de

Links

VBUYCZFBVCCYFD-NUNKFHFFSA-N 2-dehydro-L-idonic acid Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)C(=O)C(O)=O VBUYCZFBVCCYFD-NUNKFHFFSA-N 0.000 title abstract 2
VBUYCZFBVCCYFD-UHFFFAOYSA-N D-arabino-2-Hexulosonic acid Natural products OCC(O)C(O)C(O)C(=O)C(O)=O VBUYCZFBVCCYFD-UHFFFAOYSA-N 0.000 title abstract 2
238000000034 method Methods 0.000 title abstract 2
NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 abstract 1
239000003456 ion exchange resin Substances 0.000 abstract 1
229920003303 ion-exchange polymer Polymers 0.000 abstract 1
238000004811 liquid chromatography Methods 0.000 abstract 1
238000000746 purification Methods 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H3/00—Compounds containing only hydrogen atoms and saccharide radicals having only carbon, hydrogen, and oxygen atoms
- C07H3/02—Monosaccharides

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Biochemistry (AREA)
Health & Medical Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Oil, Petroleum & Natural Gas (AREA)
Biotechnology (AREA)
General Health & Medical Sciences (AREA)
Genetics & Genomics (AREA)
Molecular Biology (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Preparation Of Compounds By Using Micro-Organisms (AREA)
Saccharide Compounds (AREA)

AT00950892T 1999-08-02 2000-07-31 Verfahren zur reinigung von 2-keto-l-gulonic säure ATE252592T1 (de)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US09/366,279 US6153791A (en)	1999-08-02	1999-08-02	Process for purifying 2-keto-L-gulonic acid
PCT/US2000/020830 WO2001009152A1 (en)	1999-08-02	2000-07-31	Process for purifying 2-keto-l-gulonic acid

Publications (1)

Publication Number	Publication Date
ATE252592T1 true ATE252592T1 (de)	2003-11-15

Family

ID=23442387

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT00950892T ATE252592T1 (de)	1999-08-02	2000-07-31	Verfahren zur reinigung von 2-keto-l-gulonic säure

Country Status (10)

Country	Link
US (1)	US6153791A (de)
EP (1)	EP1203003B8 (de)
JP (1)	JP2003506333A (de)
KR (1)	KR20020022789A (de)
CN (1)	CN1371384A (de)
AT (1)	ATE252592T1 (de)
AU (1)	AU777126B2 (de)
CA (1)	CA2388299A1 (de)
DE (1)	DE60006129T2 (de)
WO (1)	WO2001009152A1 (de)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE60113158T2 (de)	2000-12-22	2006-06-08	Eastman Chemical Co., Kingsport	Verfahren zur herstellung von ascorbinsäure in gegenwart eines sulfits
GB0119864D0 (en)	2001-08-15	2001-10-10	Cerestar Holding Bv	Process for the manufacture of 2-keto-L-gulonic acid
US6518454B1 (en)	2001-10-12	2003-02-11	Eastman Chemical Company	Preparation of esters of carboxylic acids
US6476239B1 (en)	2002-02-12	2002-11-05	Eastman Chemical Company	Process for the preparation of ascorbic acid
FI20020592A7 (fi) *	2002-03-27	2003-09-28	Danisco Sweeteners Oy	Menetelmä sokereiden, sokerialkoholien, hiilihydraattien ja niiden seosten erottamiseksi niitä sisältävistä liuoksista
US6872314B2 (en) *	2003-08-29	2005-03-29	Eastman Chemical Company	Dewatering process
WO2016164748A1 (en)	2015-04-08	2016-10-13	Invista North America S.A.R.L.	Materials and methods for the selective recovery of monovalent products from aqueous solutions using continuous ion exchange
US10343084B2 (en)	2015-04-10	2019-07-09	Invista North America S.A.R.L.	Process for separation of diamines and/or omega-aminoacids from a feed mixture
US12090420B2 (en)	2018-09-18	2024-09-17	Inv Nylon Chemicals Americas, Llc	Systems and methods for recovering amines and their derivatives from aqueous mixtures
CN111943993A (zh) *	2019-05-16	2020-11-17	帝斯曼知识产权资产管理有限公司	回收2-酮-l-古洛糖酸的改进方法
CN111943836A (zh) *	2019-05-16	2020-11-17	帝斯曼知识产权资产管理有限公司	回收2-酮-l-古洛糖酸的改进方法

Family Cites Families (63)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2223797A (en) *	1940-01-22	1940-12-03	Commercial Solvents Corp	Recovery of lactic acids from crude solutions thereof
US2421611A (en) *	1945-05-04	1947-06-03	Byron E Gray	Preparation of 2-keto gulonic acid and its salts
US2539472A (en) *	1949-07-15	1951-01-30	William P Ratchford	Process for the purification of certain water-soluble hydroxycarboxylic acids
US2650248A (en) *	1950-03-15	1953-08-25	Sharples Corp	Concentration of aqueous aconitic acid solutions
US2697724A (en) *	1950-03-15	1954-12-21	Sharples Corp	Ion exchange
US2664441A (en) *	1951-07-19	1953-12-29	Harry S Owens	Separation of organic acids
US2710880A (en) *	1953-05-07	1955-06-14	Edward M Filachione	Extraction of lactic acid
US3086928A (en) *	1958-08-09	1963-04-23	Benckiser Gmbh Joh A	Process of producing citric acid
US3234105A (en) *	1962-09-20	1966-02-08	Takeda Chemical Industries Ltd	Method for producing 2-keto-lgulonic acid
FR1463729A (fr) *	1965-02-24	1966-12-23	Rohm & Haas	Enrichissement et éventuellement séparation d'un composé organique par des techniques d'adsorption
US3780097A (en) *	1972-01-03	1973-12-18	Phillips Petroleum Co	Purification of alkalimetal salts of aromatic carboxylic acids
IL39710A (en) *	1972-06-19	1975-04-25	Imi Inst For Res & Dev	Recovery of acids from aqueous solutions by solvent extraction
US3907639A (en) *	1972-08-31	1975-09-23	Hoffmann La Roche	Method for producing 2-keto-L-gulonic acid
IT1020235B (it) *	1973-11-03	1977-12-20	Benckiser Gmbh Joh A	Processo per la preparazione di citrati alcalini o di ammonio
US3912592A (en) *	1974-05-06	1975-10-14	Hoffmann La Roche	Method for producing L-sorbosone
JPS55124735A (en) *	1979-03-22	1980-09-26	Mitsubishi Chem Ind Ltd	Purification of malic acid
US4250331A (en) *	1979-10-09	1981-02-10	E. I. Du Pont De Nemours And Company	Removal of organic acids from dilute aqueous solutions of salts of organic acids by supercritical fluids
US4282323A (en) *	1979-10-09	1981-08-04	E. I. Du Pont De Nemours And Company	Removal and concentration of lower molecular weight organic acids from dilute solutions
JPS5675451A (en) *	1979-11-21	1981-06-22	Koei Chem Co Ltd	Method for treating composition containing carboxylic acid
US4308398A (en) *	1980-08-04	1981-12-29	Miles Laboratories, Inc.	Elimination of reducing sugars present in trisodium citrate
US4334095A (en) *	1980-10-06	1982-06-08	Miles Laboratories, Inc.	Extraction of organic acids from aqueous solutions
US4444881A (en) *	1981-10-26	1984-04-24	Cpc International Inc.	Recovery of organic acids from a fermentation broth
US4405717A (en) *	1981-10-26	1983-09-20	Cpc International Inc.	Recovery of acetic acid from a fermentation broth
DE3334863A1 (de) *	1983-09-27	1985-04-11	Basf Ag, 6700 Ludwigshafen	Verfahren zur gewinnung von waessrigen glyoxylsaeureloesungen
US4705894A (en) *	1984-02-29	1987-11-10	Yuanfu Su	Process for recovery of organic acids from aqueous solutions
US4764276A (en) *	1984-07-30	1988-08-16	Advanced Separation Technologies Incorporated	Device for continuous contacting of fluids and solids
US4522726A (en) *	1984-07-30	1985-06-11	Progress Equities Incorporated	Advanced separation device and method
DE3434918A1 (de) *	1984-09-22	1986-04-03	Hüls AG, 4370 Marl	Verfahren zur gewinnung von l-aepfelsaeure
US4698303A (en) *	1985-02-15	1987-10-06	Engenics, Inc.	Production of lactic acid by continuous fermentation using an inexpensive raw material and a simplified method of lactic acid purification
US4879412A (en) *	1985-03-14	1989-11-07	Mitsui Toatsu Chemicals, Inc.	Purification process of methacrylic acid
US4808317A (en) *	1985-03-19	1989-02-28	Advanced Separation Technologies Incorporated	Process for continuous contacting of fluids and solids
US5041645A (en) *	1985-05-10	1991-08-20	Haarmann & Reimer Corp.	Method for the preparation and recovery of alkali metal citrates
JPS6230791A (ja) *	1985-08-02	1987-02-09	Showa Denko Kk	Ｌ−アスコルビン酸−２−リン酸エステルの精製法
US4933289A (en) *	1986-06-05	1990-06-12	Takeda Chemical Industries, Ltd.	Biologically pure cultures of Pseudomonas sorbosoxidans useful for producing 2-keto-L-gulonic acid
JPH0795957B2 (ja) *	1986-06-05	1995-10-18	武田薬品工業株式会社	２−ケト−ｌ−グロン酸の製造法
US4935359A (en) *	1987-02-07	1990-06-19	Institute Of Microbiology	Fermentation process
US4877735A (en) *	1987-06-19	1989-10-31	Takeda Chemical Industries, Ltd.	Process for producing 2-keto-L-gulonic acid
US5202476A (en) *	1988-04-29	1993-04-13	Takeda Chemical Industries, Ltd.	Purification of 2-keto-L-gulonic acid
FR2632302B1 (fr) *	1988-06-06	1991-02-22	Roquette Freres	Procede de recuperation d'acide citrique a partir d'une liqueur en contenant
DE3831070A1 (de) *	1988-09-13	1990-03-22	Basf Ag	Verfahren zur isolierung von 2-keto-polyhdroxy-c(pfeil abwaerts)6(pfeil abwaerts)-carbonsaeuren, insbesondere von 2-keto-l-gulonsaeure aus waessrigen fermentationsaustraegen
FR2636343B1 (de) *	1988-09-13	1994-11-25	Rhone Poulenc Sante
DE3831071A1 (de) *	1988-09-13	1990-03-15	Basf Ag	Verfahren zur isolierung von 2-keto-polyhydroxy-c(pfeil abwaerts)6(pfeil abwaerts)-carbonsaeuren, insbesondere von 2-keto-l-gulonsaeure aus waessrigen fermentationsaustraegen
DK173507B1 (da) *	1988-09-30	2001-01-15	Hoffmann La Roche	Fremgangsmåde til fremstilling af 2-keto-L-gulonsyre
IT1227895B (it) *	1988-12-22	1991-05-14	Donegani Guido Ist	Processo per il recupero di acido lattico da soluzioni che lo contengono
FR2648136B1 (fr) *	1989-06-12	1994-06-17	Rhone Poulenc Sante	Procede de preparation de l'acide ascorbique
US5069883A (en) *	1989-10-20	1991-12-03	Progress Water Technologies Corp.	Device for continuous contacting of liquids and solids
US5231225A (en) *	1989-12-11	1993-07-27	Innova S.A.	Concurrent production of citric acid and alkali citrates
US4994609A (en) *	1990-06-06	1991-02-19	Innova S.A.	Production of citric acid
US5210296A (en) *	1990-11-19	1993-05-11	E. I. Du Pont De Nemours And Company	Recovery of lactate esters and lactic acid from fermentation broth
US5194130A (en) *	1990-12-21	1993-03-16	Allied-Signal Inc.	Method to produce sodium citrate using electrodialysis
TW265331B (de) *	1991-03-14	1995-12-11	Reilly Ind Inc
JPH04320691A (ja) *	1991-04-22	1992-11-11	Sumitomo Chem Co Ltd	発酵有機酸の精製方法
US5132456A (en) *	1991-05-07	1992-07-21	The Regents Of The University Of California	Sorption of carboxylic acid from carboxylic salt solutions at PHS close to or above the pKa of the acid, with regeneration with an aqueous solution of ammonia or low-molecular-weight alkylamine
IT1247995B (it) *	1991-06-06	1995-01-05	Himont Inc	Processo per la produzione di soluzioni acquose di acido lattico purificate a partire da brodi di fermentazione.
RU2102481C1 (ru) *	1991-06-13	1998-01-20	Ф.Хоффманн-Ля Рош, Аг	Способ получения 2-кето-l-гулоновой кислоты или ее соли
DE4233431A1 (de) *	1992-10-05	1994-04-07	Basf Ag	Verfahren zur Hydrierung von Zitronensäure
US5237098A (en) *	1992-10-09	1993-08-17	Miles, Inc.	Production of citric acid and trisodium citrate from molasses
US5278339A (en) *	1993-03-01	1994-01-11	Eastman Kodak Company	Process for the recovery of cyclohexanedicarboxylic acids
US5510526A (en) *	1993-06-29	1996-04-23	Cargill, Incorporated	Lactic acid production, separation and/or recovery process
US5426219A (en) *	1993-07-26	1995-06-20	A.E. Staley Manufacturing Co.	Process for recovering organic acids
US5522995A (en) *	1995-02-28	1996-06-04	Cockrem; Michael C. M.	Process for recovering organic acids from aqueous salt solutions
AU7662296A (en) *	1995-10-10	1997-04-30	Reilly Industries, Inc.	Thermally-managed separation and dewatering processes for recovering acid products
JP3976832B2 (ja) *	1996-04-30	2007-09-19	ディーエスエムアイピーアセッツビー．ブイ．	２−ケト−ｌ−グロン酸の単離方法

1999
- 1999-08-02 US US09/366,279 patent/US6153791A/en not_active Expired - Fee Related
2000
- 2000-07-31 EP EP00950892A patent/EP1203003B8/de not_active Expired - Lifetime
- 2000-07-31 CN CN00811205A patent/CN1371384A/zh active Pending
- 2000-07-31 DE DE60006129T patent/DE60006129T2/de not_active Expired - Fee Related
- 2000-07-31 AT AT00950892T patent/ATE252592T1/de not_active IP Right Cessation
- 2000-07-31 JP JP2001513959A patent/JP2003506333A/ja not_active Withdrawn
- 2000-07-31 CA CA002388299A patent/CA2388299A1/en not_active Abandoned
- 2000-07-31 AU AU63924/00A patent/AU777126B2/en not_active Ceased
- 2000-07-31 WO PCT/US2000/020830 patent/WO2001009152A1/en not_active Ceased
- 2000-07-31 KR KR1020027001370A patent/KR20020022789A/ko not_active Withdrawn

Also Published As

Publication number	Publication date
US6153791A (en)	2000-11-28
EP1203003B1 (de)	2003-10-22
DE60006129T2 (de)	2004-07-29
EP1203003B8 (de)	2004-05-26
JP2003506333A (ja)	2003-02-18
AU6392400A (en)	2001-02-19
CN1371384A (zh)	2002-09-25
CA2388299A1 (en)	2001-02-08
WO2001009152A1 (en)	2001-02-08
EP1203003A1 (de)	2002-05-08
KR20020022789A (ko)	2002-03-27
DE60006129D1 (de)	2003-11-27
AU777126B2 (en)	2004-09-30

Legal Events

Date	Code	Title	Description
2004-04-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties

Publication	Publication Date	Title
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DE69818304D1 (de)	2003-10-23	Verfahren zur reduktion von oxiranyl-epothilonen zu olefinischen epothilonen
FR2666996B1 (fr)	1994-05-20	Methode de purification d'un aminoacide utilisant une resine echangeuse d'ions.
DE50100979D1 (de)	2003-12-24	Verbessertes Verfahren zur Hydroformylierung von Olefinen durch Reduzierung der Ameisensäurekonzentration
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DE69421751D1 (de)	1999-12-30	Verfahren zur Reinigung von Abwässern durch Oxidation auf einen Adsorbentträger
DE60006129D1 (de)	2003-11-27	Verfahren zur reinigung von 2-keto-l-gulonic säure
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