ATE276201T1 - Verfahren zur entfernung von templat aus synthetischen zeolithen - Google Patents

Verfahren zur entfernung von templat aus synthetischen zeolithen

Info

Publication number
ATE276201T1
ATE276201T1 AT00203986T AT00203986T ATE276201T1 AT E276201 T1 ATE276201 T1 AT E276201T1 AT 00203986 T AT00203986 T AT 00203986T AT 00203986 T AT00203986 T AT 00203986T AT E276201 T1 ATE276201 T1 AT E276201T1
Authority
AT
Austria
Prior art keywords
removal
template
synthetic zeolites
zeolites
silicalite
Prior art date
Application number
AT00203986T
Other languages
English (en)
Inventor
Stefano Palmery
Fausto Genoni
Guido Spano'
Leonardo Dalloro
Alberto Cesana
Roberto Buzzoni
Original Assignee
Polimeri Europa Spa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Polimeri Europa Spa filed Critical Polimeri Europa Spa
Application granted granted Critical
Publication of ATE276201T1 publication Critical patent/ATE276201T1/de

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/03—Catalysts comprising molecular sieves not having base-exchange properties
    • B01J29/035—Microporous crystalline materials not having base exchange properties, such as silica polymorphs, e.g. silicalites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7034—MTW-type, e.g. ZSM-12, NU-13, TPZ-12 or Theta-3
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/02—Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/04—Preparation of lactams from or via oximes by Beckmann rearrangement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/40—Special temperature treatment, i.e. other than just for template removal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
AT00203986T 1999-11-19 2000-11-14 Verfahren zur entfernung von templat aus synthetischen zeolithen ATE276201T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IT1999MI002424A IT1314001B1 (it) 1999-11-19 1999-11-19 Metodo per la rimozione del templante da zeoliti sintetiche

Publications (1)

Publication Number Publication Date
ATE276201T1 true ATE276201T1 (de) 2004-10-15

Family

ID=11383990

Family Applications (1)

Application Number Title Priority Date Filing Date
AT00203986T ATE276201T1 (de) 1999-11-19 2000-11-14 Verfahren zur entfernung von templat aus synthetischen zeolithen

Country Status (11)

Country Link
US (1) US6645899B1 (de)
EP (1) EP1101735B1 (de)
JP (1) JP4738588B2 (de)
KR (1) KR100393438B1 (de)
AT (1) ATE276201T1 (de)
DE (1) DE60013733T2 (de)
DK (1) DK1101735T3 (de)
ES (1) ES2228404T3 (de)
IT (1) IT1314001B1 (de)
SG (1) SG93909A1 (de)
TW (1) TW527319B (de)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7098161B2 (en) * 2000-10-20 2006-08-29 Abb Lummus Global Inc. Method of treating zeolite
US6833127B2 (en) * 2000-12-22 2004-12-21 California Institute Of Technology Method of removing structure directing agents from molecular sieves
WO2003004444A1 (en) 2001-07-02 2003-01-16 Exxonmobil Chemical Patents Inc. Inhibiting catalyst coke formation in the manufacture of an olefin
US7271123B2 (en) 2002-03-20 2007-09-18 Exxonmobil Chemical Patents Inc. Molecular sieve catalyst composition, its making and use in conversion process
US6872680B2 (en) 2002-03-20 2005-03-29 Exxonmobil Chemical Patents Inc. Molecular sieve catalyst composition, its making and use in conversion processes
US7022844B2 (en) 2002-09-21 2006-04-04 Honeywell International Inc. Amide-based compounds, production, recovery, purification and uses thereof
ITMI20072342A1 (it) * 2007-12-14 2009-06-15 Polimeri Europa Spa Processo per preparare zeoliti ts-1
ES2596223T3 (es) * 2009-11-27 2017-01-05 Basf Se Proceso para la preparación de un catalizador de zeolita de titanio
US8772476B2 (en) 2011-10-28 2014-07-08 Honeywell International Inc. Gas and liquid phase catalytic Beckmann rearrangement of oximes to produce lactams
DE102012217923A1 (de) * 2012-10-01 2014-04-03 Evonik Degussa Gmbh Herstellung von Katalysatoren auf Basis von Bor-Zeolithen
CN105339343B (zh) 2013-03-08 2017-08-29 英国石油化学品有限公司 羰基化催化剂和方法

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1127311B (it) * 1979-12-21 1986-05-21 Anic Spa Materiale sintetico,cristallino,poroso costituito da ossidi di silicio e titanio,metodo per la sua preparazione e suoi usi
JPS6354358A (ja) * 1986-04-21 1988-03-08 Sumitomo Chem Co Ltd ε−カプロラクタムの製法
JPH0610181B2 (ja) * 1986-11-14 1994-02-09 モンテデイペ・ソチエタ・ペル・アツイオニ オキシム製造のための接触方法
US4916097A (en) * 1988-05-16 1990-04-10 Mobil Oil Corp. Method for activating zeolites containing organic cations
US5066630A (en) * 1989-06-30 1991-11-19 Sumitomo Chemical Company, Limited Method for removing nitrogen-containing organic compounds from crystalline metallosilicate
US5143879A (en) * 1991-07-18 1992-09-01 Mobil Oil Corporation Method to recover organic templates from freshly synthesized molecular sieves
US5425934A (en) * 1993-12-27 1995-06-20 Gas Research Institute Dealumination and selective removal of organic material from zeolites
US5599987A (en) * 1995-03-31 1997-02-04 Arco Chemical Technology, L.P. Integrated process for cyclohexanone oxime production
US5681789A (en) * 1996-02-12 1997-10-28 Arco Chemical Technology, L.P. Activation of as-synthesized titanium-containing zeolites
JP3482075B2 (ja) * 1996-02-29 2003-12-22 三菱重工業株式会社 メソポーラス無機高分子の製造方法
JP3524686B2 (ja) * 1996-03-01 2004-05-10 三菱重工業株式会社 ペンタシルゼオライトの製造方法
DE19624340A1 (de) * 1996-06-19 1998-01-08 Degussa Verfahren zur Herstellung von kristallinen mikro- und mesoporösen Metallsilicaten, verfahrensgemäß erhältliche Produkte und deren Verwendung
JPH1043599A (ja) * 1996-08-02 1998-02-17 Ube Ind Ltd 修飾メソポアモレキュラーシーブの製造法
CN1058513C (zh) * 1997-12-16 2000-11-15 中国石化兰州炼油化工总厂 一种快速高效分子筛模板剂的抽提方法
US5925330A (en) * 1998-02-13 1999-07-20 Mobil Oil Corporation Method of m41s functionalization of potentially catalytic heteroatom centers into as-synthesized m41s with concomitant surfactant extraction

Also Published As

Publication number Publication date
ES2228404T3 (es) 2005-04-16
DE60013733D1 (de) 2004-10-21
DE60013733T2 (de) 2005-09-29
KR100393438B1 (ko) 2003-08-02
US6645899B1 (en) 2003-11-11
KR20010070223A (ko) 2001-07-25
TW527319B (en) 2003-04-11
EP1101735B1 (de) 2004-09-15
ITMI992424A1 (it) 2001-05-19
DK1101735T3 (da) 2005-01-24
IT1314001B1 (it) 2002-12-03
ITMI992424A0 (it) 1999-11-19
EP1101735A1 (de) 2001-05-23
JP4738588B2 (ja) 2011-08-03
SG93909A1 (en) 2003-01-21
JP2001190961A (ja) 2001-07-17

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