ATE289869T1 - Verfahren zur herstellung von zerbrechlichen sprügetrockneten agglomerierten trägern und olefinpolymerisierungträgerkatalysatoren dafür - Google Patents
Verfahren zur herstellung von zerbrechlichen sprügetrockneten agglomerierten trägern und olefinpolymerisierungträgerkatalysatoren dafürInfo
- Publication number
- ATE289869T1 ATE289869T1 AT99966451T AT99966451T ATE289869T1 AT E289869 T1 ATE289869 T1 AT E289869T1 AT 99966451 T AT99966451 T AT 99966451T AT 99966451 T AT99966451 T AT 99966451T AT E289869 T1 ATE289869 T1 AT E289869T1
- Authority
- AT
- Austria
- Prior art keywords
- particles
- agglomerates
- olefin polymerization
- sprit
- possess
- Prior art date
Links
- 150000001336 alkenes Chemical class 0.000 title abstract 2
- 239000003054 catalyst Substances 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 title abstract 2
- 238000006116 polymerization reaction Methods 0.000 title abstract 2
- 239000002245 particle Substances 0.000 abstract 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- 229910052809 inorganic oxide Inorganic materials 0.000 abstract 2
- 239000000741 silica gel Substances 0.000 abstract 2
- 229910002027 silica gel Inorganic materials 0.000 abstract 2
- 239000000470 constituent Substances 0.000 abstract 1
- 238000009837 dry grinding Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000002685 polymerization catalyst Substances 0.000 abstract 1
- 239000007921 spray Substances 0.000 abstract 1
- 238000001694 spray drying Methods 0.000 abstract 1
- 239000011800 void material Substances 0.000 abstract 1
- 238000001238 wet grinding Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F110/00—Homopolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F110/02—Ethene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F10/02—Ethene
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
- B01J37/0027—Powdering
- B01J37/0036—Grinding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
- B01J37/0027—Powdering
- B01J37/0045—Drying a slurry, e.g. spray drying
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Catalysts (AREA)
- Silicon Compounds (AREA)
- Polymerization Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/219,077 US6313061B1 (en) | 1998-12-22 | 1998-12-22 | Method of making frangible spray dried agglomerated supports and olefin polymerization catalysts supported thereon |
| PCT/US1999/030294 WO2000037176A1 (en) | 1998-12-22 | 1999-12-20 | Method of making frangible spray dried agglomerated supports and olefin polymerization catalysts supported thereon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE289869T1 true ATE289869T1 (de) | 2005-03-15 |
Family
ID=22817768
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT99966451T ATE289869T1 (de) | 1998-12-22 | 1999-12-20 | Verfahren zur herstellung von zerbrechlichen sprügetrockneten agglomerierten trägern und olefinpolymerisierungträgerkatalysatoren dafür |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US6313061B1 (de) |
| EP (1) | EP1144116B1 (de) |
| JP (1) | JP4767416B2 (de) |
| KR (1) | KR100560872B1 (de) |
| AT (1) | ATE289869T1 (de) |
| AU (1) | AU2198200A (de) |
| DE (1) | DE69924019T2 (de) |
| WO (1) | WO2000037176A1 (de) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU1330701A (en) * | 1999-10-07 | 2001-05-10 | Dow Chemical Company, The | Silica gel composition and method for making |
| EP1240943A1 (de) * | 2000-10-21 | 2002-09-18 | Degussa AG | Katalysatorträger |
| ATE389684T1 (de) * | 2001-10-09 | 2008-04-15 | Genzyme Corp | Verfahren zum reinigen und trocknen von polymerhydrogelen |
| US6600011B2 (en) * | 2001-10-09 | 2003-07-29 | Genzyme Corporation | Process for purification and drying of polymer hydrogels |
| WO2003102037A1 (en) * | 2002-06-03 | 2003-12-11 | Univation Technologies, Llc | Solid, particulated, spray dried, heterogenous catalyst composition |
| RU2005128272A (ru) * | 2003-02-24 | 2006-08-10 | Чайна Петролеум Энд Кемикал Корпорейшн (Cn) | Комплексный носитель катализаторов полимеризации пропилена, каталитический компонент и катализатор, включающий указанный компонент |
| US7341977B2 (en) * | 2003-06-20 | 2008-03-11 | Nanoscale Corporation | Method of sorbing sulfur compounds using nanocrystalline mesoporous metal oxides |
| DE102004006104A1 (de) * | 2004-02-06 | 2005-08-25 | Basell Polyolefine Gmbh | Verfahren zur Herstellung von geträgerten Katalysatoren für die Polymerisation |
| DE102004006113A1 (de) * | 2004-02-06 | 2005-08-25 | Basell Polyolefine Gmbh | Verfahren zur Herstellung von Trägern für Katalysatoren |
| WO2006010065A2 (en) * | 2004-07-09 | 2006-01-26 | E.I. Dupont De Nemours And Company | Catalysts for olefin polymerization or oligomerization |
| CN100369942C (zh) * | 2006-01-26 | 2008-02-20 | 吉林市吉清科技开发有限公司 | 气相流化床乙烯聚合催化剂微球形二氧化硅载体的制备方法及设备 |
| DE102006058800A1 (de) * | 2006-12-13 | 2008-06-19 | Wacker Chemie Ag | Verfahren zur Herstellung von Katalysatoren und deren Verwendung für die Gasphasenoxidation von Olefinen |
| US20090020411A1 (en) * | 2007-07-20 | 2009-01-22 | Holunga Dean M | Laser pyrolysis with in-flight particle manipulation for powder engineering |
| US20100252484A1 (en) * | 2007-12-20 | 2010-10-07 | Ranjit Kumar | Process for preparing high attrition resistant inorganic compositions and compositions prepared therefrom |
| JP5736633B2 (ja) * | 2008-04-18 | 2015-06-17 | 株式会社明電舎 | 触媒及びその製造方法 |
| SG11201707037TA (en) * | 2015-03-10 | 2017-09-28 | Univation Tech Llc | Spray dried catalyst compositions, methods for preparation and use in olefin polymerization processes |
| CN105036146B (zh) * | 2015-08-28 | 2017-04-12 | 北京理工大学 | 一种球形纳米硅酸锆粉体的制备方法 |
| US11267914B2 (en) | 2016-12-29 | 2022-03-08 | Chevron Phillips Chemical Company Lp | Methods of preparing a catalyst |
| US10654953B2 (en) * | 2016-12-29 | 2020-05-19 | Chevron Phillips Chemical Company Lp | Methods of preparing a catalyst |
| US20200369803A1 (en) | 2016-12-29 | 2020-11-26 | Chevron Phillips Chemical Company Lp | Methods of Preparing a Catalyst |
| CN114057912B (zh) * | 2020-07-31 | 2023-06-16 | 中国石油化工股份有限公司 | 一种载铬硅胶控制颗粒形态的干燥方法和制备方法 |
| CN114426590A (zh) * | 2020-09-28 | 2022-05-03 | 中国石油化工股份有限公司 | 一种茂金属催化剂与Ziegler-Natta催化剂的在线切换方法 |
| US11124586B1 (en) * | 2020-11-09 | 2021-09-21 | Chevron Phillips Chemical Company Lp | Particle size control of metallocene catalyst systems in loop slurry polymerization reactors |
| WO2022125581A2 (en) | 2020-12-08 | 2022-06-16 | Chevron Phillips Chemical Company Lp | Particle size control of supported chromium catalysts in loop slurry polymerization reactors |
| KR20250133456A (ko) | 2021-09-13 | 2025-09-05 | 셰브론 필립스 케미컬 컴퍼니 엘피 | 올레핀 중합에서 사용하기 위한 촉매 시스템 성분의 하이드로사이클론 개질 |
Family Cites Families (45)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2288873A (en) * | 1939-12-30 | 1942-07-07 | Standard Oil Co | Polymerization of olefins |
| US2470410A (en) * | 1946-04-09 | 1949-05-17 | Standard Oil Dev Co | Preparation of silica magnesia catalysts |
| US2529283A (en) * | 1946-06-20 | 1950-11-07 | Standard Oil Dev Co | Preparation of a silica-aluminamagnesia catalyst |
| US2532525A (en) * | 1947-07-25 | 1950-12-05 | Universal Oil Prod Co | Preparation of a hydrocarbon conversion catalyst |
| US2958648A (en) * | 1956-11-27 | 1960-11-01 | Nalco Chemical Co | Conversion of hydrocarbons with a synthetic silica-alumina-magnesia catalyst composite |
| US2988521A (en) * | 1957-11-19 | 1961-06-13 | American Cyanamid Co | Process for preparing a silicamagnesia catalyst |
| NL231551A (de) * | 1958-09-22 | |||
| US3607777A (en) | 1968-06-18 | 1971-09-21 | Grace W R & Co | Process for preparing microspheroidal desiccant silica gel |
| US3887494A (en) | 1970-11-12 | 1975-06-03 | Phillips Petroleum Co | Olefin polymerization catalyst |
| US3965042A (en) | 1973-12-07 | 1976-06-22 | W. R. Grace & Co. | Formation of alumina-containing particles with aluminum hydroxide binder |
| US4022714A (en) | 1975-07-17 | 1977-05-10 | W. R. Grace & Co. | Silica hydrosol bound cracking catalysts |
| FR2332234A1 (fr) | 1975-11-20 | 1977-06-17 | Rhone Poulenc Ind | Corps siliceux agglomeres |
| US4070286A (en) | 1976-06-15 | 1978-01-24 | E. I. Du Pont De Nemours And Company | Macroporous microspheroids and a process for their manufacture |
| NL7707961A (nl) | 1977-07-18 | 1979-01-22 | Stamicarbon | Werkwijze ter bereiding van poreus, zuiver siliciumdioxyde. |
| US4131542A (en) | 1977-07-19 | 1978-12-26 | E. I. Dupont De Nemours And Company | Spray dried silica for chromatography |
| US4257874A (en) | 1977-08-31 | 1981-03-24 | E. I. Du Pont De Nemours And Company | Petroleum refinery processes using catalyst of aluminosilicate sols and powders |
| EP0037182B2 (de) | 1980-03-24 | 1991-06-12 | Imperial Chemical Industries Plc | Herstellung eines getrockneten Übergangsmetallproduktes |
| US4548912A (en) | 1980-04-14 | 1985-10-22 | Ashland Oil, Inc. | Microspherical catalysts |
| US4317778A (en) * | 1980-12-29 | 1982-03-02 | Standard Oil Company (Sohio) | Preparation of maleic anhydride using fluidized catalysts |
| FR2558738B1 (fr) * | 1984-01-27 | 1987-11-13 | Inst Francais Du Petrole | Procede de fabrication de catalyseurs contenant du cuivre, du zinc et de l'aluminium, utilisables pour la production de methanol a partir de gaz de synthese |
| JPS61174103A (ja) | 1985-01-23 | 1986-08-05 | Shokubai Kasei Kogyo Kk | 金属酸化物からなる多孔質真球状微粒子粉末の製造法 |
| US4657880A (en) | 1985-03-18 | 1987-04-14 | Corning Glass Works | Preparation of high surface area agglomerates for catalyst support and preparation of monolithic support structures containing them |
| FR2584698B1 (fr) | 1985-07-15 | 1990-05-18 | Rhone Poulenc Spec Chim | Procede de preparation de particules de silice spheroidales |
| US4677084A (en) | 1985-11-27 | 1987-06-30 | E. I. Du Pont De Nemours And Company | Attrition resistant catalysts, catalyst precursors and catalyst supports and process for preparing same |
| US4948773A (en) | 1989-02-13 | 1990-08-14 | Research Association For Petroleum Alternatives Development | Amphora particulate catalyst-support and a method for the preparation of an amphora-type particulate catalyst-support |
| JPS6344943A (ja) * | 1986-04-11 | 1988-02-25 | Res Assoc Petroleum Alternat Dev<Rapad> | つぼ型触媒担体およびその製造方法 |
| JPH0725817B2 (ja) | 1986-04-23 | 1995-03-22 | 日本石油株式会社 | オレフイン重合用触媒 |
| US4902666A (en) | 1986-07-02 | 1990-02-20 | Chevron Research Company | Process for the manufacture of spheroidal bodies by selective agglomeration |
| JPH0699135B2 (ja) | 1989-02-20 | 1994-12-07 | 富士デヴィソン株式会社 | 球状シリカゲルの製造法 |
| US5128114A (en) | 1989-04-14 | 1992-07-07 | E. I. Du Pont De Nemours And Company | Silica microspheres, method of improving attrition resistance |
| US5352645A (en) | 1989-04-14 | 1994-10-04 | E. I. Du Pont De Nemours And Company | Silica microspheres, method of improving attrition resistance and use |
| US5108975A (en) | 1991-01-28 | 1992-04-28 | Phillips Petroleum Company | Composition and method of making high porosity, high strength compositions |
| DE4132230A1 (de) | 1991-09-27 | 1993-04-01 | Grace Gmbh | Verwendung von kugelfoermigem siliciumdioxid |
| DE4200248A1 (de) * | 1992-01-08 | 1993-07-15 | Basf Ag | Verfahren zur regenerierung von metalloxid-katalysatoren |
| GB9210265D0 (en) | 1992-05-13 | 1992-07-01 | Unilever Plc | Catalysts and catalyst supports |
| US5552361A (en) | 1993-11-04 | 1996-09-03 | W. R. Grace & Co.-Conn. | Aluminum phosphate composition with high pore volume and large pore diameter, process for its production and use thereof |
| US5403809A (en) | 1992-12-21 | 1995-04-04 | W. R. Grace & Co.-Conn. | Composite inorganic supports containing carbon for bioremediation |
| US5403799A (en) | 1992-12-21 | 1995-04-04 | W. R. Grace & Co.-Conn. | Process upset-resistant inorganic supports for bioremediation |
| US5302566A (en) | 1993-01-25 | 1994-04-12 | E. I. Du Pont De Nemours And Company | Process for preparing attrition resistant catalysts |
| US5604170A (en) | 1993-02-23 | 1997-02-18 | Nippon Oil Company, Limited | Solid catalyst components for olefin polemerization and use thereof |
| US5661097A (en) | 1994-08-12 | 1997-08-26 | The Dow Chemical Company | Supported olefin polymerization catalyst |
| GB9417059D0 (en) | 1994-08-24 | 1994-10-12 | Bp Chem Int Ltd | Oxide catalysts |
| US5714424A (en) | 1995-01-09 | 1998-02-03 | W. R. Grace & Co.-Conn. | Multi-component polyolefin catalysts |
| DE19516253A1 (de) | 1995-04-26 | 1996-10-31 | Grace Gmbh | Mattierungsmittel auf Basis von aggregiertem Siliciumdioxid mit verbesserter Effizienz |
| ATE164598T1 (de) | 1995-08-09 | 1998-04-15 | Basf Ag | Katalysatorsysteme vom typ der ziegler-natta- katalysatoren |
-
1998
- 1998-12-22 US US09/219,077 patent/US6313061B1/en not_active Expired - Lifetime
-
1999
- 1999-12-20 AT AT99966451T patent/ATE289869T1/de not_active IP Right Cessation
- 1999-12-20 KR KR1020017007868A patent/KR100560872B1/ko not_active Expired - Fee Related
- 1999-12-20 WO PCT/US1999/030294 patent/WO2000037176A1/en not_active Ceased
- 1999-12-20 DE DE69924019T patent/DE69924019T2/de not_active Expired - Lifetime
- 1999-12-20 AU AU21982/00A patent/AU2198200A/en not_active Abandoned
- 1999-12-20 EP EP99966451A patent/EP1144116B1/de not_active Expired - Lifetime
- 1999-12-20 JP JP2000589280A patent/JP4767416B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| KR100560872B1 (ko) | 2006-03-13 |
| DE69924019D1 (de) | 2005-04-07 |
| DE69924019T2 (de) | 2006-01-26 |
| EP1144116A1 (de) | 2001-10-17 |
| JP4767416B2 (ja) | 2011-09-07 |
| AU2198200A (en) | 2000-07-12 |
| KR20010099874A (ko) | 2001-11-09 |
| EP1144116B1 (de) | 2005-03-02 |
| WO2000037176A1 (en) | 2000-06-29 |
| US6313061B1 (en) | 2001-11-06 |
| JP2002532250A (ja) | 2002-10-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RER | Ceased as to paragraph 5 lit. 3 law introducing patent treaties |