ATE323068T1 - Verfahren zur herstellung von cyclohexanonoxim - Google Patents

Verfahren zur herstellung von cyclohexanonoxim

Info

Publication number: ATE323068T1
Authority: AT; Austria
Prior art keywords: cyclohexanone oxime; synthesis zone; hydroxylammonium; sub; cyclohexanone
Prior art date: 2000-06-05

Application number

AT01938833T

Other languages

English (en)

Inventor

Marc Blaauw

Antonius Jacobus Franci Simons

Henk Oevering

Original Assignee

Dsm Ip Assets Bv

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2000-06-05

Filing date

2001-05-31

Publication date

2006-04-15

2001-05-31 Application filed by Dsm Ip Assets Bv filed Critical Dsm Ip Assets Bv

2006-04-15 Application granted granted Critical

2006-04-15 Publication of ATE323068T1 publication Critical patent/ATE323068T1/de

Links

VEZUQRBDRNJBJY-UHFFFAOYSA-N cyclohexanone oxime Chemical compound ON=C1CCCCC1 VEZUQRBDRNJBJY-UHFFFAOYSA-N 0.000 title abstract 16
238000004519 manufacturing process Methods 0.000 title abstract 2
230000015572 biosynthetic process Effects 0.000 abstract 7
238000003786 synthesis reaction Methods 0.000 abstract 7
RBLWMQWAHONKNC-UHFFFAOYSA-N hydroxyazanium Chemical compound O[NH3+] RBLWMQWAHONKNC-UHFFFAOYSA-N 0.000 abstract 5
JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract 4
239000003960 organic solvent Substances 0.000 abstract 2
229910002651 NO3 Inorganic materials 0.000 abstract 1
NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 abstract 1
229910019142 PO4 Inorganic materials 0.000 abstract 1
239000012431 aqueous reaction media Substances 0.000 abstract 1
238000010531 catalytic reduction reaction Methods 0.000 abstract 1
229910052739 hydrogen Inorganic materials 0.000 abstract 1
239000001257 hydrogen Substances 0.000 abstract 1
125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
238000000034 method Methods 0.000 abstract 1
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
239000010452 phosphate Substances 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1418—Preparation by catalytic reduction of nitrogen oxides or nitrates with hydrogen
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Inorganic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)

AT01938833T 2000-06-05 2001-05-31 Verfahren zur herstellung von cyclohexanonoxim ATE323068T1 (de)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
EP00201965		2000-06-05

Publications (1)

Publication Number	Publication Date
ATE323068T1 true ATE323068T1 (de)	2006-04-15

Family

ID=8171596

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
AT01938833T ATE323068T1 (de)	2000-06-05	2001-05-31	Verfahren zur herstellung von cyclohexanonoxim

Country Status (13)

Country	Link
US (1)	US7005547B2 (de)
EP (1)	EP1299353B1 (de)
JP (1)	JP2003535842A (de)
KR (1)	KR100763111B1 (de)
CN (1)	CN1203052C (de)
AT (1)	ATE323068T1 (de)
AU (1)	AU2001264409A1 (de)
BR (1)	BR0111455B1 (de)
DE (1)	DE60118745T2 (de)
MX (1)	MXPA02011960A (de)
MY (1)	MY136944A (de)
TW (1)	TW593232B (de)
WO (1)	WO2001094298A1 (de)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
KR100632758B1 (ko)	2001-01-31	2006-10-11	아사히 가세이 가부시키가이샤	시클로헥사논 옥심의 제조 방법
EP1318141A1 (de) *	2001-12-04	2003-06-11	Dsm Nv	Verfahren zur Behandlung eines Phosphat, Cyclohexanon, Cyclohexanonoxim enthaltenden wässrigen Mediums
EP1451149B1 (de) *	2001-12-04	2007-02-14	DSM IP Assets B.V.	Verfahren zur behandlung eines cyclohexanonoxim und cyclohexanon enthaltenden wässrigen mediums
EP1428792A1 (de) *	2002-12-11	2004-06-16	DSM IP Assets B.V.	Verfahren zur Mischung einer sauren Lösung enthaltend Hydroxylammonium und Phosphat mit Salpetersäure
CN104262223A (zh) *	2003-05-23	2015-01-07	帝斯曼知识产权资产管理有限公司	用于制备己内酰胺的连续方法
EP1901994B1 (de) *	2005-07-08	2010-01-27	DSM IP Assets B.V.	Verfahren zur kontinuierlichen produktion von hydroxylammonium
ITMI20060279A1 (it) *	2006-02-15	2007-08-16	Aser S R L	Procedimento per deacidificare oli e-o grassi
TW200829544A (en) *	2007-01-05	2008-07-16	China Petrochemical Dev Corp	Method for preparing cyclohexanone oxime
CN103420869B (zh) *	2012-05-23	2015-11-25	中国石油化工股份有限公司	一种环己烷氨氧化的方法
CN103896803A (zh) *	2012-12-28	2014-07-02	帝斯曼知识产权资产管理有限公司	蒸汽汽提hpo*萃取区流出的无机工艺液体以及冷凝热的利用

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
NL6513426A (de)	1965-10-16	1967-04-17
NL141502B (nl) *	1969-09-20	1974-03-15	Stamicarbon	Continue bereiding van cyclohexanonoxim.
US3862230A (en) *	1969-09-20	1975-01-21	Stamicarbon	Continuous preparation of cyclohexanone oxime
BE759914A (fr) *	1969-12-06	1971-06-04	Stamicarbon	Procede de recyclage pour la preparation et la traitement d'unesolutionde sel d'hydroxylammonium
BE759915A (fr) *	1969-12-06	1971-06-04	Stamicarbon	Procede de recyclage pour la preparation et le traitement d'unesolutionde sel d'hydroxylammonium
US3997607A (en) *	1974-04-26	1976-12-14	Stamicarbon B.V.	Recycling process for the preparation of cyclohexanone oxime
NL7907395A (nl) *	1979-10-05	1981-04-07	Stamicarbon	Kringloopproces voor de bereiding en verwerking van een hydroxylammoniumzoutoplossing.
US4994613A (en) *	1983-02-16	1991-02-19	Hoechst Celanese Corporation	Process for preparing 4-hydroxyacetophenone oxime with mother liquor recycle

2001
- 2001-05-31 DE DE60118745T patent/DE60118745T2/de not_active Expired - Fee Related
- 2001-05-31 KR KR1020027016548A patent/KR100763111B1/ko not_active Expired - Lifetime
- 2001-05-31 WO PCT/NL2001/000429 patent/WO2001094298A1/en not_active Ceased
- 2001-05-31 US US10/297,308 patent/US7005547B2/en not_active Expired - Fee Related
- 2001-05-31 EP EP01938833A patent/EP1299353B1/de not_active Expired - Lifetime
- 2001-05-31 CN CNB018137547A patent/CN1203052C/zh not_active Expired - Lifetime
- 2001-05-31 MX MXPA02011960A patent/MXPA02011960A/es unknown
- 2001-05-31 AT AT01938833T patent/ATE323068T1/de not_active IP Right Cessation
- 2001-05-31 AU AU2001264409A patent/AU2001264409A1/en not_active Abandoned
- 2001-05-31 BR BRPI0111455-7A patent/BR0111455B1/pt not_active IP Right Cessation
- 2001-05-31 JP JP2002501815A patent/JP2003535842A/ja active Pending
- 2001-06-05 MY MYPI20012629A patent/MY136944A/en unknown
- 2001-06-26 TW TW090115424A patent/TW593232B/zh not_active IP Right Cessation

Also Published As

Publication number	Publication date
EP1299353A1 (de)	2003-04-09
CN1203052C (zh)	2005-05-25
KR20030007872A (ko)	2003-01-23
DE60118745T2 (de)	2006-11-16
CN1446195A (zh)	2003-10-01
BR0111455A (pt)	2003-06-24
EP1299353B1 (de)	2006-04-12
WO2001094298A1 (en)	2001-12-13
MXPA02011960A (es)	2003-07-14
US20040116745A1 (en)	2004-06-17
KR100763111B1 (ko)	2007-10-04
DE60118745D1 (de)	2006-05-24
MY136944A (en)	2008-11-28
TW593232B (en)	2004-06-21
JP2003535842A (ja)	2003-12-02
US7005547B2 (en)	2006-02-28
BR0111455B1 (pt)	2012-07-24
AU2001264409A1 (en)	2001-12-17

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Legal Events

Date	Code	Title	Description
2006-10-15	RER	Ceased as to paragraph 5 lit. 3 law introducing patent treaties