ATE340154T1 - Kontinuierliches verfahren zur herstellung von polytrimethylenetherglykol - Google Patents

Kontinuierliches verfahren zur herstellung von polytrimethylenetherglykol

Info

Publication number
ATE340154T1
ATE340154T1 AT00986476T AT00986476T ATE340154T1 AT E340154 T1 ATE340154 T1 AT E340154T1 AT 00986476 T AT00986476 T AT 00986476T AT 00986476 T AT00986476 T AT 00986476T AT E340154 T1 ATE340154 T1 AT E340154T1
Authority
AT
Austria
Prior art keywords
ether glycol
continuous process
polytrimethylene ether
producing polytrimethylene
gas
Prior art date
Application number
AT00986476T
Other languages
English (en)
Inventor
Hari B Sunkara
Ernest Keith Marchildon
Howard Chung-Ho Ng
Leo E Manzer
Original Assignee
Du Pont
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Du Pont filed Critical Du Pont
Application granted granted Critical
Publication of ATE340154T1 publication Critical patent/ATE340154T1/de

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/34Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/002Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/007Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor in the presence of catalytically active bodies, e.g. porous plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/245Stationary reactors without moving elements inside placed in series
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0453Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01Preparation of ethers
    • C07C41/09Preparation of ethers by dehydration of compounds containing hydroxy groups
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00115Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002Chemical plants
    • B01J2219/00027Process aspects
    • B01J2219/00033Continuous processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00164Controlling or regulating processes controlling the flow
    • B01J2219/00166Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00182Controlling or regulating processes controlling the level of reactants in the reactor vessel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Dispersion Chemistry (AREA)
  • Polyethers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
AT00986476T 1999-12-17 2000-12-15 Kontinuierliches verfahren zur herstellung von polytrimethylenetherglykol ATE340154T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US17212699P 1999-12-17 1999-12-17

Publications (1)

Publication Number Publication Date
ATE340154T1 true ATE340154T1 (de) 2006-10-15

Family

ID=22626474

Family Applications (1)

Application Number Title Priority Date Filing Date
AT00986476T ATE340154T1 (de) 1999-12-17 2000-12-15 Kontinuierliches verfahren zur herstellung von polytrimethylenetherglykol

Country Status (11)

Country Link
US (2) US6720459B2 (de)
EP (1) EP1237835B1 (de)
JP (1) JP4638646B2 (de)
KR (1) KR100677808B1 (de)
CN (1) CN1238317C (de)
AT (1) ATE340154T1 (de)
AU (1) AU2270901A (de)
CA (1) CA2389800C (de)
DE (1) DE60030880T2 (de)
MX (1) MXPA02005949A (de)
WO (1) WO2001044150A2 (de)

Families Citing this family (117)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2795735B1 (fr) 1999-07-01 2001-09-07 Univ Toulouse Derives citrullines de la fibrine et leur utilisation pour le diagnostic ou le traitement de la polyarthrite rhumatoide
US6949617B2 (en) * 2003-05-09 2005-09-27 Acushnet Company Golf balls comprising chiral diols or chiral cyclic ethers
EP1246861B1 (de) 1999-12-17 2006-05-17 E.I. Du Pont De Nemours And Company Herstellung von polytrimethylene ether glycol und copolymere davon
KR100677808B1 (ko) * 1999-12-17 2007-02-05 이 아이 듀폰 디 네모아 앤드 캄파니 폴리트리메틸렌 에테르 글리콜의 연속 제조 방법
US6599625B2 (en) 2001-10-31 2003-07-29 E. I. Du Pont De Nemours And Company Polyether ester elastomer comprising polytrimethylene ether ester soft segment and trimethylene ester hard segment
US6562457B1 (en) 2001-10-31 2003-05-13 E. I. Du Pont De Nemours And Company Polyether ester elastomer comprising polytrimethylene ether ester soft segment and tetramethylene ester hard segment
US6590065B1 (en) * 2001-12-10 2003-07-08 E. I. Du Pont De Nemours And Company Polytrimethylene ether ester amide and use thereof
US6905765B2 (en) * 2002-08-09 2005-06-14 E.I. Du Pont De Nemours And Company Polyether ester elastomers comprising poly(trimethylene-ethylene ether) ester soft segment and alkylene ester hard segment
US6852823B2 (en) 2002-08-09 2005-02-08 E. I. Du Pont De Nemours And Company Polyurethane and polyurethane-urea elastomers from polytrimethylene ether glycol
US6979492B2 (en) * 2002-08-09 2005-12-27 E. I. Du Pont De Nemours And Company Thermoplastic elastomer comprising poly(trimethylene-ethylene ether) soft segment and polyamide hard segment
US20040030095A1 (en) 2002-08-09 2004-02-12 Sunkara Hari B. Poly(trimethylene-ethylene ether) glycols
US6608168B1 (en) * 2002-08-09 2003-08-19 E. I. Du Pont De Nemours And Company Polytrimethylene ether esters
US6946539B2 (en) * 2002-08-09 2005-09-20 E. I. Du Pont De Nemours And Company Polyurethane and polyurethane-urea comprised of poly(trimethylene-ethylene ether) glycol soft segment
US6875514B2 (en) * 2003-03-21 2005-04-05 E. I. Du Pont De Nemours And Company Coating composition containing polytrimethylene ether diol useful as a primer composition
US7268182B2 (en) * 2003-03-21 2007-09-11 E. I. Du Pont De Nemours & Company Polytrimethylene ether diol containing coating compositions
CN100473634C (zh) * 2003-05-06 2009-04-01 纳幕尔杜邦公司 从聚三亚甲基醚二醇聚合物中除去色体
CN100475761C (zh) * 2003-05-06 2009-04-08 纳幕尔杜邦公司 聚三亚甲基醚二醇的氢化
EP1620378B1 (de) 2003-05-06 2016-03-09 E. I. du Pont de Nemours and Company Hydrierung von biochemisch erhaltenem 1,3-propandiol
US7009082B2 (en) * 2003-05-06 2006-03-07 E.I. Du Pont De Nemours And Company Removal of color bodies from polytrimethylene ether glycol polymers
US20040225107A1 (en) * 2003-05-06 2004-11-11 Sunkara Hari Babu Polytrimethylene ether glycol with excellent quality from biochemically-derived 1,3-propanediol
US7745668B2 (en) * 2003-05-06 2010-06-29 E. I. Du Pont De Nemours And Company Processes for reducing color in polytrimethylene ether glycol polymers
US7084311B2 (en) * 2003-05-06 2006-08-01 E. I. Du Pont De Nemours And Company Hydrogenation of chemically derived 1,3-propanediol
US7323539B2 (en) * 2003-05-06 2008-01-29 E. I. Du Pont De Nemours And Company Polytrimethylene ether glycol and polytrimethylene ether ester with excellent quality
US7342142B2 (en) * 2003-05-06 2008-03-11 E.I. Du Pont De Nemours And Company Hydrogenation of polytrimethylene ether glycol
DE602004028359D1 (de) * 2003-05-06 2010-09-09 Du Pont Reinigung von biologisch produziertem 1,3-propandiol
WO2004099110A1 (ja) * 2003-05-08 2004-11-18 Mitsubishi Chemical Corporation 1,3−プロパンジオールの製造方法
US7144958B2 (en) * 2003-05-21 2006-12-05 E. I. Du Pont De Nemours And Company Articles prepared from compositions modified with organic fiber micropulp
US7179769B2 (en) * 2003-07-17 2007-02-20 E. I. Du Pont De Nemours And Company Poly (trimethylene-ethylene ether) glycol lube oils
US20080103217A1 (en) * 2006-10-31 2008-05-01 Hari Babu Sunkara Polyether ester elastomer composition
US7074969B2 (en) * 2004-06-18 2006-07-11 E.I. Du Pont De Nemours And Company Process for preparation of polytrimethylene ether glycols
US7422795B2 (en) * 2004-06-21 2008-09-09 E.I. Du Pont De Nemours And Company Polytrimethylene ether ester elastomer flexible films
KR20070032725A (ko) * 2004-06-29 2007-03-22 미쓰비시 가가꾸 가부시키가이샤 폴리에테르폴리올의 제조 방법
US20060189711A1 (en) * 2005-02-23 2006-08-24 Ng Howard C Silicon-containing polytrimethylene homo- or copolyether composition
US7629396B2 (en) 2005-02-23 2009-12-08 E.I. Du Pont De Nemours And Company Silicon-containing polytrimethylene homo- for copolyether composition
US7413677B2 (en) * 2005-02-25 2008-08-19 E. I. Du Pont De Nemours And Company Process for heat transfer utilizing a polytrimethylene homo- or copolyether glycol based heat transfer fluid
US7282159B2 (en) * 2005-02-25 2007-10-16 E.I. Dupont De Nemours And Company Process for heat transfer utilizing a polytrimethylene ether glycol or polytrimethylene ether ester glycol based heat transfer fluid
US7476344B2 (en) * 2005-02-25 2009-01-13 E.I. Du Pont De Nemours Electrical apparatuses containing polytrimethylene homo- or copolyether glycol based electrical insulation fluids
US7638591B2 (en) * 2005-04-08 2009-12-29 E. I. Du Pont De Nemours And Company Polyester elastomer and compositions thereof
US7244790B2 (en) * 2005-05-02 2007-07-17 E.I. Du Pont De Nemours And Company Thermoplastic elastomer blend, method of manufacture and use thereof
WO2006121111A1 (ja) * 2005-05-13 2006-11-16 Mitsubishi Chemical Corporation ポリエーテルポリオールの製造方法
US7157607B1 (en) * 2005-08-16 2007-01-02 E. I. Du Pont De Nemours And Company Manufacture of polytrimethylene ether glycol
US7161045B1 (en) 2005-08-16 2007-01-09 E. I. Du Pont De Nemours And Company Process for manufacture of polytrimethylene ether glycol
US8271682B2 (en) * 2005-09-16 2012-09-18 Sendori, Inc. Enhancements for domain name leasing marketplace
US7357985B2 (en) * 2005-09-19 2008-04-15 E.I. Du Pont De Nemours And Company High crimp bicomponent fibers
EP1940914B1 (de) * 2005-09-22 2009-05-13 E.I. Du Pont De Nemours And Company Herstellung von polytrimethylenetherglykol und copolymeren davon
US7405330B2 (en) * 2005-09-22 2008-07-29 E.I. Du Pont De Nemours And Company Preparation of polytrimethylene ether glycol and copolymers thereof
US7625941B2 (en) * 2005-09-22 2009-12-01 E.I. Du Pont De Nemours And Company Ionic liquids
US7544813B2 (en) * 2005-09-22 2009-06-09 E.I. Du Pont De Nemours And Company Ionic liquids
WO2007052697A1 (ja) * 2005-11-02 2007-05-10 Mitsubishi Chemical Corporation ポリアルキレンエーテルグリコール及びその製造方法
US20070129524A1 (en) * 2005-12-06 2007-06-07 Sunkara Hari B Thermoplastic polyurethanes comprising polytrimethylene ether soft segments
US7388115B2 (en) * 2006-01-20 2008-06-17 E. I. Du Pont De Nemours And Company Manufacture of polytrimethylene ether glycol
US7164046B1 (en) 2006-01-20 2007-01-16 E. I. Du Pont De Nemours And Company Manufacture of polytrimethylene ether glycol
US20070203371A1 (en) * 2006-01-23 2007-08-30 Sunkara Hari B Process for producing polytrimethylene ether glycol
US7888431B2 (en) * 2006-02-10 2011-02-15 E.I. Du Pont De Nemours & Co. Coating compositions having improved early hardness
JP5258756B2 (ja) * 2006-05-17 2013-08-07 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー パーソナルケア組成物
US20080039582A1 (en) * 2006-07-28 2008-02-14 Hari Babu Sunkara Polytrimethylene ether-based polyurethane ionomers
US20080175875A1 (en) * 2006-09-25 2008-07-24 Hari Babu Sunkara Cosmetic compositions
US7531593B2 (en) * 2006-10-31 2009-05-12 E.I. Du Pont De Nemours And Company Thermoplastic elastomer blend composition
US20080108845A1 (en) * 2006-11-07 2008-05-08 Hari Babu Sunkara Polytrimethylene ether glycol esters
US20080135662A1 (en) * 2006-12-06 2008-06-12 Chang Jing C Melt-spun elastoester multifilament yarns
US20090131625A1 (en) * 2007-11-21 2009-05-21 Kurian Joseph V Processes for making elastomeric polyester esters from post-consumer polyester
US7714174B2 (en) * 2007-03-27 2010-05-11 E. I. Du Pont De Nemours And Company Lower-color polytrimethylene ether glycol using hydride compounds
US20080242831A1 (en) * 2007-03-27 2008-10-02 Yanhui Niu Lower-color polytrimethylene ether glycol using zero-valent metals
CN101784645A (zh) * 2007-08-24 2010-07-21 纳幕尔杜邦公司 润滑油组合物
EP2181184A1 (de) * 2007-08-24 2010-05-05 E. I. du Pont de Nemours and Company Schmierölzusammensetzungen
KR20100043109A (ko) * 2007-08-24 2010-04-27 이 아이 듀폰 디 네모아 앤드 캄파니 윤활유 조성물
US8703681B2 (en) 2007-08-24 2014-04-22 E I Du Pont De Nemours And Company Lubrication oil compositions
US20090054282A1 (en) * 2007-08-24 2009-02-26 E.I. Dupont De Nemours And Company Lubrication oil compositions
WO2009059148A2 (en) * 2007-11-01 2009-05-07 E. I. Du Pont De Nemours And Company Preparation of polytrimethylene ether glycol or copolymers thereof
EP2215146A2 (de) * 2007-11-01 2010-08-11 E. I. du Pont de Nemours and Company Herstellung von polytrimethylenetherglykol oder copolymeren davon
US7919017B2 (en) * 2007-11-12 2011-04-05 E. I. Du Pont De Nemours And Company Electrical insulation fluids for use in electrical apparatus
EP2209825A1 (de) 2007-11-13 2010-07-28 E. I. du Pont de Nemours and Company Isocyanat-terminiertes polytrimethylenetherpolyol und verfahren zu seiner herstellung
US20090197779A1 (en) * 2008-01-31 2009-08-06 Scott Christopher Jackson Method for enhanced recovery of oil from oil reservoirs
ATE521676T1 (de) * 2008-04-22 2011-09-15 Du Pont Beschichtungszusammensetzung mit polytrimethylenetherdiol
US20110052920A1 (en) * 2008-06-18 2011-03-03 E.I. Du Pont De Nemours And Company Polyester and polytrimethylene ether diol based coating composition
US7910644B2 (en) * 2008-07-02 2011-03-22 E.I. Du Pont De Nemours & Company High film build coating composition containing polytrimethylene ether diol
US8349407B2 (en) 2008-07-02 2013-01-08 E I Du Pont De Nemours And Company High film build coating composition containing polytrimethylene ether diol
IL200995A0 (en) * 2008-10-01 2010-06-30 Bayer Materialscience Ag Polyether-based polyurethane formulations for the production of holographic media
JP5480276B2 (ja) 2008-10-06 2014-04-23 ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー エルエルシー 担体として酸性混合金属酸化物を含む低金属(ニッケル及びレニウム)触媒組成物
CN102239002B (zh) 2008-10-06 2013-10-30 联合碳化化学品及塑料技术公司 低金属负载的氧化铝载体的催化剂组合物和氨基化方法
EP2356095B2 (de) 2008-10-06 2017-09-27 Union Carbide Chemicals & Plastics Technology LLC Verfahren zur herstellung von cyclischen n-aminofunktionellen triaminen
JP5806116B2 (ja) 2008-10-06 2015-11-10 ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー エルエルシー 求核性化合物のトランスアルコキシル化
CN101412798B (zh) 2008-11-21 2011-08-10 优洁(亚洲)有限公司 软质聚氨酯低回弹泡沫及其制备方法
CA2739566A1 (en) * 2008-12-23 2010-07-01 E.I. Du Pont De Nemours And Company Process for the production of acrylic and methacrylic esters of poly(trimethylene ether) glycol
WO2010074803A1 (en) * 2008-12-23 2010-07-01 E. I. Du Pont De Nemours And Company Acrylic and methacrylic esters of poly(trimethylene ether) glycol
CN102264781A (zh) * 2008-12-23 2011-11-30 纳幕尔杜邦公司 聚(三亚甲基醚)二醇的(甲基)丙烯酸酯及其用途
US20110257330A1 (en) 2008-12-30 2011-10-20 E.I. Du Pont De Nemours And Company Waterborne coating composition containing polytrimethylene ether diol
US20100267994A1 (en) * 2009-04-16 2010-10-21 E. I. Du Pont De Nemours And Company Processes for preparing polytrimethylene glycol using ion exchange resins
KR20120047267A (ko) * 2009-07-22 2012-05-11 이 아이 듀폰 디 네모아 앤드 캄파니 폴리트라이메틸렌 에테르 글리콜 및 그의 코폴리머의 합성 방법
CN102471480A (zh) * 2009-07-22 2012-05-23 纳幕尔杜邦公司 用于合成聚醚二醇和聚酯二醇的方法
EP2459660A1 (de) * 2009-07-30 2012-06-06 E. I. du Pont de Nemours and Company Verfahren zur herstellung einer beschichtung mit einem gewünschten glanzwert
FR2950823B1 (fr) * 2009-10-06 2011-12-09 Inst Francais Du Petrole Reacteur a cocourant ascendant de gaz et de liquide faisant appel a un generateur de micro bulles
US20110112331A1 (en) * 2009-11-09 2011-05-12 E.I. Du Pont De Nemours And Company Method for phase separation of polytrimethylene ether glycol in salt solution
CN102667444A (zh) 2009-12-18 2012-09-12 纳幕尔杜邦公司 用于涂层测量的方法
TW201130913A (en) * 2009-12-21 2011-09-16 Du Pont Processes for producing polytrimethylene ether glycol and copolymers thereof
JP5837517B2 (ja) 2010-03-02 2015-12-24 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se ポリエーテルアルコールの製造方法
KR20130048214A (ko) * 2010-03-15 2013-05-09 이 아이 듀폰 디 네모아 앤드 캄파니 트라이메틸렌 글리콜 올리고머를 포함하는 항미생물 조성물 및 조성물의 사용 방법
US8436081B2 (en) 2010-08-31 2013-05-07 U.S. Coatings IP Co. LLC. High film build coating composition containing low molecular weight polytrimethylene ether glycol
US8372905B2 (en) 2010-08-31 2013-02-12 E I Du Pont De Nemours And Company Coating compositions containing low molecular weight polytrimethylene ether glycol
US8410205B2 (en) 2010-08-31 2013-04-02 E I Du Pont De Nemours And Company Matting agent composition containing low molecular weight polytrimethylene ether glycol
US20130289129A1 (en) 2010-11-10 2013-10-31 Us Coatings Ip Co Llc Radiation curable coating composition containing low molecular weight polytrimethylene ether glycol
TW201221548A (en) 2010-11-19 2012-06-01 Du Pont Branched poly (trimethylene ether) polyols
US8247526B2 (en) 2010-12-20 2012-08-21 E I Du Pont De Nemours And Company Process for the preparation of polyalkylene ether glycol
DE112011104474T5 (de) * 2010-12-21 2013-09-19 Kao Corp. Säulen-Kontaktanlage und Verfahren für ihren Betrieb
CN102620400B (zh) 2011-01-30 2013-12-11 昌硕科技(上海)有限公司 空调装置
TW201245277A (en) 2011-04-26 2012-11-16 Du Pont Processes for preparing polytrimethylene ether glycol
US9718968B2 (en) 2011-12-12 2017-08-01 Axalta Coating Systems Ip Co., Llc Waterborne coating composition containing bio-resourced polytrimethylene ether polyol
US10090425B2 (en) 2012-02-21 2018-10-02 California Institute Of Technology Axially-integrated epitaxially-grown tandem wire arrays
WO2013152132A1 (en) 2012-04-03 2013-10-10 The California Institute Of Technology Semiconductor structures for fuel generation
US8759559B2 (en) 2012-04-18 2014-06-24 E I Du Pont De Nemours And Company Processes for preparing polytrimethylene ether glycol esters
US9553223B2 (en) 2013-01-24 2017-01-24 California Institute Of Technology Method for alignment of microwires
WO2015084619A1 (en) 2013-12-02 2015-06-11 Dow Global Technologies Llc Preparation of high molecular weight, branched, acyclic polyalkyleneamines and mixtures thereof
EP3083637A4 (de) * 2013-12-19 2017-05-31 Archer Daniels Midland Co. Verbessertes glycolacylierungsverfahren
EP3663383B1 (de) 2018-12-05 2021-01-20 The Procter & Gamble Company Flüssige handgeschirrspülmittelzusammensetzung
WO2022076208A1 (en) * 2020-10-06 2022-04-14 Dow Global Technologies Llc Method of making an amphiphilic oxetane oligomer
JP6912681B1 (ja) * 2021-02-01 2021-08-04 株式会社日本触媒 第2級アルコールアルコキシレートの製造方法
WO2025186782A1 (en) 2024-03-08 2025-09-12 Toray Lycra Co. Ltd. Polyurethane resin composition and polyurethane elastic fiber

Family Cites Families (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2520733A (en) * 1946-08-26 1950-08-29 Shell Dev Polymers of trimethylene glycol
US2492955A (en) 1946-08-31 1950-01-03 Shell Dev Polyoxyalkylene compounds
US3027352A (en) 1958-02-28 1962-03-27 Celanese Corp Copolymers
US3023192A (en) 1958-05-29 1962-02-27 Du Pont Segmented copolyetherester elastomers
US3192184A (en) * 1959-03-19 1965-06-29 Du Pont Prepolymerization process
US3384623A (en) 1964-01-11 1968-05-21 Toyo Spinning Co Ltd Production of polyurethane elastomers
US3326985A (en) 1964-12-29 1967-06-20 Shell Oil Co Polytrimethylene glycol
US3526484A (en) * 1968-05-17 1970-09-01 Du Pont Polymer finishing apparatus
US3651014A (en) 1969-07-18 1972-03-21 Du Pont Segmented thermoplastic copolyester elastomers
US3626484A (en) * 1969-09-22 1971-12-07 Acf Ind Inc Brake rigging for railway freight cars
US3763109A (en) 1971-08-19 1973-10-02 Du Pont Segmented thermoplastic copolyesters
DE2818240A1 (de) 1978-04-26 1979-11-08 Hoechst Ag Thermoplastische formmassen auf basis von polyoxymethylenen
DE3016113A1 (de) 1980-04-25 1981-10-29 Bayer Ag, 5090 Leverkusen Verfahren zur aufarbeitung von polyetherpolyolen
US4970296A (en) * 1984-03-01 1990-11-13 Massachusetts Institute Of Technology Heterodimeric T lymphocyte receptor
JP2608939B2 (ja) 1988-10-26 1997-05-14 帝人株式会社 ポリエーテルエステルブロック共重合体
US4970295A (en) 1989-02-27 1990-11-13 Arco Chemical Technology, Inc. Preparation of oxetane polyether polyols using a bleaching earth catalyst
US4937314A (en) 1989-02-28 1990-06-26 E. I. Du Pont De Nemours And Company Copolyetherester elastomer with poly(1,3-propylene terephthalate) hard segment
JPH06503113A (ja) * 1990-11-27 1994-04-07 コモンウェルス・サイエンティフィック・アンド・インダストリアル・リサーチ・オーガナイゼーション ポリ(アルキレンオキシド)類
US5128185A (en) 1991-08-29 1992-07-07 E. I. Du Pont De Nemours And Company Copolyetherester elastomer with poly(1,3-propylenebibenzoate) hard segment
DE69333518T2 (de) 1992-10-21 2005-04-07 E.I. Du Pont De Nemours And Co., Wilmington Depolymerisation zu zyclischen Ethern unter Verwendung der Katalysatoren aus gewählten Metallverbindungen
DE4236039A1 (de) 1992-10-24 1994-04-28 Basf Ag Verfahren und Vorrichtung zur Herstellung von Polykondensaten
EP0614877B1 (de) * 1993-03-12 1997-08-20 Bayer Ag Verfahren zur kontinuierlichen Herstellung von Arylcarbonaten
ES2200778T3 (es) 1994-10-28 2004-03-16 E.I. Dupont De Nemours And Company Polimerizacion de eteres ciclicos usando catalizadores de compuestos metalicos seleccionados.
US5674974A (en) 1994-11-23 1997-10-07 E. I. Du Pont De Nemours And Company Continuous polymerization process for polyamides
US5731453A (en) * 1996-03-12 1998-03-24 Ube Industries, Ltd. Process for producing a diaryl carbonate
US5677415A (en) * 1996-03-28 1997-10-14 E. I. Du Pont De Nemours And Company Apparatus and process for a polycondensation reaction
US5659089A (en) 1996-05-22 1997-08-19 Arco Chemical Technology, L.P. Process for making poly(2-methyl-1,3-propanediol)
US5814282A (en) * 1997-01-15 1998-09-29 Lohe; Hans High surface intermeshing profile reactor
DE19706901A1 (de) * 1997-02-21 1998-08-27 Bayer Ag Verfahren zur Durchführung von Polykondensationsreaktionen
AUPO761697A0 (en) 1997-06-30 1997-07-24 Cardiac Crc Nominees Pty Limited Process for the purification of polyethers
US6235948B1 (en) 1998-08-18 2001-05-22 E. I. Du Pont De Nemours And Company Process for the purification of 1,3-propanediol
KR100677808B1 (ko) * 1999-12-17 2007-02-05 이 아이 듀폰 디 네모아 앤드 캄파니 폴리트리메틸렌 에테르 글리콜의 연속 제조 방법
EP1246861B1 (de) * 1999-12-17 2006-05-17 E.I. Du Pont De Nemours And Company Herstellung von polytrimethylene ether glycol und copolymere davon

Also Published As

Publication number Publication date
WO2001044150A2 (en) 2001-06-21
US6720459B2 (en) 2004-04-13
CA2389800A1 (en) 2001-06-21
DE60030880D1 (de) 2006-11-02
JP4638646B2 (ja) 2011-02-23
EP1237835B1 (de) 2006-09-20
US20020010374A1 (en) 2002-01-24
US20040152925A1 (en) 2004-08-05
CN1238317C (zh) 2006-01-25
AU2270901A (en) 2001-06-25
KR20020063212A (ko) 2002-08-01
JP2003517082A (ja) 2003-05-20
CA2389800C (en) 2011-12-06
EP1237835A2 (de) 2002-09-11
WO2001044150A3 (en) 2002-01-03
CN1411431A (zh) 2003-04-16
DE60030880T2 (de) 2007-04-26
MXPA02005949A (es) 2003-01-28
US7074968B2 (en) 2006-07-11
KR100677808B1 (ko) 2007-02-05

Similar Documents

Publication Publication Date Title
DE60030880D1 (de) Kontinuierliches verfahren zur herstellung von polytrimethylenetherglykol
EP0877009A4 (de) Verfahren zur herstellung von 1,1,1,3,3,-pentafluoropropanen
RO115517B1 (ro) Procedeu de obţinere a acidului acetic
DE68911280D1 (de) Flüssigphaseverfahren zur Herstellung von Methanol aus Synthesegas.
DE60019649D1 (de) Verfahren zur herstellung von 1,1,1,3,3-pentachlorpropan
PL327632A1 (en) Stereoselective ring-opening reactions
UA50730C2 (uk) Спосіб одержання 1-(тіометил)циклопропаноцтової кислоти та проміжних сполук для її одержання
MY126773A (en) Method for producing alkali methylates
ATE283833T1 (de) Verfahren zur herstellung von epichlorohydrin und zwischenprodukt davon
ATE272065T1 (de) Verfahren zur herstellung von alkoxysilanen
ATE234797T1 (de) Verfahren zur herstellung von difluoromethan
DE69938535D1 (de) Dampfphasenprozess zur Herstellung von Aluminid
DE59804527D1 (de) Verfahren zur herstellung von metallfreien guerbetalkoholen
RU2000125746A (ru) Способ получения полиэфирполиолов со слабым запахом
DE59901513D1 (de) Verfahren zur herstellung von polycarbonaten mit terminalen oh-gruppen
DE58903808D1 (de) Verfahren zur herstellung von 3,5-dimethyl-4-methoxypyridinderivaten sowie neues zwischenprodukt hierfuer.
DE69909921D1 (de) Verfahren zur herstellung von n-methyl-pyrrolidon
DE3260280D1 (en) Process for the preparation of isosorbid-5-nitrate
DE69824843D1 (de) Verfahren zur herstellung von modifizierten p-chiralen nucleotid-analoga
ATE279414T1 (de) Verfahren zur herstellung von reinem triethylendiamin (teda)
RU2002131713A (ru) Способ получения триэтилфосфата
GC0000005A (en) Process for the purification of an alkanolamine.
DE60209499D1 (de) Verfahren zur herstellung von nylon 6,6
ATE273263T1 (de) Verfahren zur kontinuierlichen herstellung von glutaraldehyd
ATE272061T1 (de) Friedel-craft verfahren zur herstellung von thioxanthonen

Legal Events

Date Code Title Description
RER Ceased as to paragraph 5 lit. 3 law introducing patent treaties