ATE358143T1 - Wasserlösliche oder wasserdispergierbare fluorochemische silane um substrate öl- und wasserabstossend zu machen - Google Patents
Wasserlösliche oder wasserdispergierbare fluorochemische silane um substrate öl- und wasserabstossend zu machenInfo
- Publication number
- ATE358143T1 ATE358143T1 AT01200208T AT01200208T ATE358143T1 AT E358143 T1 ATE358143 T1 AT E358143T1 AT 01200208 T AT01200208 T AT 01200208T AT 01200208 T AT01200208 T AT 01200208T AT E358143 T1 ATE358143 T1 AT E358143T1
- Authority
- AT
- Austria
- Prior art keywords
- water
- group
- hydrolyzable
- value
- formula
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/46—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with organic materials
- C04B41/49—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Organo-clay compounds; Organo-silicates, i.e. ortho- or polysilicic acid esters ; Organo-phosphorus compounds; Organo-inorganic complexes
- C04B41/4905—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Organo-clay compounds; Organo-silicates, i.e. ortho- or polysilicic acid esters ; Organo-phosphorus compounds; Organo-inorganic complexes containing silicon
- C04B41/4922—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Organo-clay compounds; Organo-silicates, i.e. ortho- or polysilicic acid esters ; Organo-phosphorus compounds; Organo-inorganic complexes containing silicon applied to the substrate as monomers, i.e. as organosilanes RnSiX4-n, e.g. alkyltrialkoxysilane, dialkyldialkoxysilane
- C04B41/4933—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Organo-clay compounds; Organo-silicates, i.e. ortho- or polysilicic acid esters ; Organo-phosphorus compounds; Organo-inorganic complexes containing silicon applied to the substrate as monomers, i.e. as organosilanes RnSiX4-n, e.g. alkyltrialkoxysilane, dialkyldialkoxysilane containing halogens, i.e. organohalogen silanes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/28—Surface treatment of glass, not in the form of fibres or filaments, by coating with organic material
- C03C17/30—Surface treatment of glass, not in the form of fibres or filaments, by coating with organic material with silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/82—Coating or impregnation with organic materials
- C04B41/84—Compounds having one or more carbon-to-metal of carbon-to-silicon linkages
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D5/00—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures
- B05D5/08—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures to obtain an anti-friction or anti-adhesive surface
- B05D5/083—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures to obtain an anti-friction or anti-adhesive surface involving the use of fluoropolymers
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Materials Applied To Surfaces To Minimize Adherence Of Mist Or Water (AREA)
- Silicon Polymers (AREA)
- Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP01200208A EP1225188B1 (de) | 2001-01-19 | 2001-01-19 | Wasserlösliche oder wasserdispergierbare fluorochemische Silane um Substrate Öl- und wasserabstossend zu machen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE358143T1 true ATE358143T1 (de) | 2007-04-15 |
Family
ID=31197767
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT01200208T ATE358143T1 (de) | 2001-01-19 | 2001-01-19 | Wasserlösliche oder wasserdispergierbare fluorochemische silane um substrate öl- und wasserabstossend zu machen |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US6977307B2 (de) |
| EP (1) | EP1225188B1 (de) |
| JP (1) | JP2004517990A (de) |
| CN (1) | CN100422224C (de) |
| AT (1) | ATE358143T1 (de) |
| BR (1) | BR0206374A (de) |
| DE (1) | DE60127527T2 (de) |
| ES (1) | ES2282186T3 (de) |
| MX (1) | MXPA03006077A (de) |
| WO (1) | WO2002057329A1 (de) |
Families Citing this family (50)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE60042561D1 (de) | 1999-10-27 | 2009-08-27 | 3M Innovative Properties Co | Fluorochemische sulfonamide tenside |
| EP1225187B1 (de) * | 2001-01-19 | 2009-05-27 | 3M Innovative Properties Company | Fluorovinyloligomerkomponente mit Silangruppen, Flüssigzusammensetzungen daraus und Beschichtungsverfahren |
| JP4312606B2 (ja) * | 2002-03-12 | 2009-08-12 | 日本曹達株式会社 | 化学吸着膜製造方法及びそれに用いる化学吸着膜製造用溶液 |
| ATE346884T1 (de) * | 2002-06-03 | 2006-12-15 | 3M Innovative Properties Co | Fluor-silan-oligomerzusammensetzung |
| AU2003277598A1 (en) * | 2002-11-08 | 2004-06-07 | Daikin Industries, Ltd. | Treating agent for masonry |
| EP1493761A1 (de) * | 2003-07-02 | 2005-01-05 | 3M Innovative Properties Company | Fluorpolymer aus fluorhaltigen Kurzkettenacrylaten oder Methacrylaten und wasser- und ölabweisende Zusammensetzungen davon |
| US8722160B2 (en) * | 2003-10-31 | 2014-05-13 | Aeris Capital Sustainable Ip Ltd. | Inorganic/organic hybrid nanolaminate barrier film |
| US7321018B2 (en) * | 2003-12-23 | 2008-01-22 | 3M Innovative Properties Company | Compositions for aqueous delivery of fluorinated oligomeric silanes |
| US7247386B2 (en) | 2003-12-23 | 2007-07-24 | 3M Innovative Properties Company | Composition of an oligomeric fluorosilane and surface treatment of retroreflective sheet |
| US20050137266A1 (en) * | 2003-12-23 | 2005-06-23 | Naiyong Jing | Aqueous composition of an oligomeric fluorosilane and use thereof for surface treatment of optical elements |
| DE602004012324T2 (de) | 2003-12-31 | 2009-03-19 | 3M Innovative Properties Co., St. Paul | Wasser- und ölabweisende fluoracrylate |
| ITMI20040106A1 (it) * | 2004-01-27 | 2004-04-27 | Solvay Solexis Spa | Poliuretani |
| DE602004032231D1 (de) | 2004-09-02 | 2011-05-26 | 3M Innovative Properties Co | Verfahren zur Behandlung von porösem Stein, bei dem eine fluorchemische Zusammensetzung verwendet wird |
| US20060142530A1 (en) | 2004-12-28 | 2006-06-29 | Moore George G | Water- and oil-repellent fluorourethanes and fluoroureas |
| US7291688B2 (en) | 2004-12-28 | 2007-11-06 | 3M Innovative Properties Company | Fluoroacrylate-mercaptofunctional copolymers |
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| US20070014018A1 (en) * | 2004-12-30 | 2007-01-18 | Wheatley John A | Internal components of optical device comprising hardcoat |
| US7495118B2 (en) | 2004-12-30 | 2009-02-24 | 3M Innovative Properties Company | Compositions containing C4-swallow tail silanes |
| US7160850B2 (en) | 2004-12-30 | 2007-01-09 | 3M Innovative Properties Company | Compositions of monomeric surfactants |
| US7776983B2 (en) | 2004-12-30 | 2010-08-17 | 3M Innovative Properties Company | Fluorochemical polymeric surfactants |
| US7629298B2 (en) * | 2006-02-21 | 2009-12-08 | 3M Innovative Properties Company | Sandstone having a modified wettability and a method for modifying the surface energy of sandstone |
| US7615283B2 (en) | 2006-06-13 | 2009-11-10 | 3M Innovative Properties Company | Fluoro(meth)acrylate polymer composition suitable for low index layer of antireflective film |
| US20070285778A1 (en) * | 2006-06-13 | 2007-12-13 | Walker Christopher B | Optical films comprising high refractive index and antireflective coatings |
| US20070285779A1 (en) * | 2006-06-13 | 2007-12-13 | Walker Christopher B | Optical films comprising high refractive index and antireflective coatings |
| US8231973B2 (en) * | 2006-06-13 | 2012-07-31 | 3M Innovative Properties Company | Fluoro(meth)acrylate polymer composition suitable for low index layer of antireflective film |
| US7569715B2 (en) * | 2006-07-05 | 2009-08-04 | 3M Innovative Properties Company | Compositions containing silanes |
| US7728098B2 (en) | 2006-07-27 | 2010-06-01 | 3M Innovative Properties Company | Fluorochemical composition comprising fluorinated oligomeric silane |
| JP5385146B2 (ja) * | 2006-10-20 | 2014-01-08 | スリーエム イノベイティブ プロパティズ カンパニー | 易洗浄基材のための方法及びそれによる物品 |
| EP2949694A1 (de) | 2006-12-07 | 2015-12-02 | 3M Innovative Properties Company of 3M Center | Partikel mit einem fluorierten siloxan und verfahren zur herstellung und verwendung davon |
| US8080170B2 (en) * | 2007-10-01 | 2011-12-20 | 3M Innovative Properties Company | Cationic fluorinated ether silane compositions and related methods |
| WO2009045993A2 (en) | 2007-10-01 | 2009-04-09 | 3M Innovative Properties Company | Compositions comprising cationic fluorinated ether, silanes, and related methods |
| WO2009073537A2 (en) | 2007-12-03 | 2009-06-11 | 3M Innovative Properties Company | Cationic polymeric fluorinated ether silane compositions and methods of use |
| JP2011505488A (ja) | 2007-12-03 | 2011-02-24 | スリーエム イノベイティブ プロパティズ カンパニー | カチオン性ポリマー系フッ素化エーテルシラン組成物及び使用方法 |
| US8058463B2 (en) * | 2007-12-04 | 2011-11-15 | E. I. Du Pont De Nemours And Compnay | Fluorosilanes |
| KR101529355B1 (ko) | 2007-12-12 | 2015-06-16 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | 폴리(알킬렌 옥사이드) 반복 단위를 갖는 퍼플루오로폴리에테르 중합체를 포함하는 하드코트 |
| TWI450043B (zh) | 2008-03-11 | 2014-08-21 | 3M Innovative Properties Co | 具備保護層之光工具 |
| EP2456823A4 (de) | 2009-07-21 | 2012-12-26 | 3M Innovative Properties Co | Härtbare zusammensetzung, verfahren zur beschichtung eines lichtwerkzeugs und beschichtetes lichtwerkzeug |
| US8420281B2 (en) | 2009-09-16 | 2013-04-16 | 3M Innovative Properties Company | Epoxy-functionalized perfluoropolyether polyurethanes |
| CN102686642B (zh) | 2009-09-16 | 2016-06-29 | 3M创新有限公司 | 氟化涂料和用其制作的底片 |
| EP2478034A1 (de) | 2009-09-16 | 2012-07-25 | 3M Innovative Properties Company | Fluorierte beschichtungen und damit hergestellte fotowerkzeuge |
| RU2577864C2 (ru) | 2010-04-01 | 2016-03-20 | Эвоник Дегусса Гмбх | Способная к отверждению смесь |
| JP6478988B2 (ja) | 2013-06-25 | 2019-03-06 | スリーエム イノベイティブ プロパティズ カンパニー | 湿気硬化性組成物、使用法、及び複合物品 |
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| CN105482099B (zh) * | 2015-12-24 | 2017-10-03 | 天津科技大学 | 无催化剂制备多硅氧烷全氟聚醚的方法 |
| JP6685513B2 (ja) | 2016-07-15 | 2020-04-28 | 日産自動車株式会社 | 防汚構造体前駆体、防汚構造体及び表面改質方法 |
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| CN114430757A (zh) * | 2019-09-27 | 2022-05-03 | 赢创运营有限公司 | 硅酮(甲基)丙烯酸酯、其制备方法及其在可固化组合物中的用途 |
| CN111019476A (zh) * | 2019-12-11 | 2020-04-17 | 中国地质大学（武汉） | 一种超疏水和光催化油漆及其制备方法 |
| US20230225319A1 (en) | 2020-04-17 | 2023-07-20 | Kraton Polymers Llc | Antimicrobial Spray Composition |
| DE202021001420U1 (de) | 2021-04-19 | 2021-07-20 | Kraton Polymers Research B.V. | Antimikrobielle Sprühzusammensetzung |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2803615A (en) | 1956-01-23 | 1957-08-20 | Minnesota Mining & Mfg | Fluorocarbon acrylate and methacrylate esters and polymers |
| US4085137A (en) | 1969-03-10 | 1978-04-18 | Minnesota Mining And Manufacturing Company | Poly(perfluoroalkylene oxide) derivatives |
| JPS60190727A (ja) | 1984-03-09 | 1985-09-28 | Daikin Ind Ltd | 含フツ素有機シラン化合物およびその製法と用途 |
| FR2573079B1 (fr) * | 1984-11-13 | 1987-08-14 | Atochem | Fluorosilanes et leur procede de preparation |
| JPS6263560A (ja) | 1985-09-16 | 1987-03-20 | Daikin Ind Ltd | （メタ）アクリル酸フルオロアルキルオリゴマ−及びその誘導体 |
| JPH0699655B2 (ja) | 1985-10-09 | 1994-12-07 | 大日本インキ化学工業株式会社 | 常温硬化性樹脂組成物 |
| JPH0684495B2 (ja) * | 1986-06-03 | 1994-10-26 | 旭硝子株式会社 | 表面改質剤 |
| JP2595678B2 (ja) | 1988-04-15 | 1997-04-02 | ダイキン工業株式会社 | 防汚塗料組成物及び被覆品 |
| FR2653772B1 (fr) | 1989-11-02 | 1992-01-17 | Atochem | Telomeres acryliques fluores et leur application au traitement hydrofuge et oleofuge de substrats divers. |
| US5276175A (en) | 1991-04-02 | 1994-01-04 | Minnesota Mining And Manufacturing Company | Isocyanate derivatives comprising flourochemical oligomers |
| US5292796A (en) | 1991-04-02 | 1994-03-08 | Minnesota Mining And Manufacturing Company | Urea-aldehyde condensates and melamine derivatives comprising fluorochemical oligomers |
| CA2071596A1 (en) | 1991-07-10 | 1993-01-11 | Frederick E. Behr | Perfluoroalkyl halides and derivatives |
| CA2090302A1 (en) | 1992-03-20 | 1993-09-21 | Larry D. Rich | Aqueous dispersable oil and water repellent silane masonry penetrants |
| US5349004A (en) * | 1992-09-18 | 1994-09-20 | Minnesota Mining And Manufacturing Company | Fluoroalkyl siloxane/vinyl copolymer dispersions and pressure-sensitive adhesives having improved solvent resistance prepared therefrom |
| US5274159A (en) * | 1993-02-18 | 1993-12-28 | Minnesota Mining And Manufacturing Company | Destructable fluorinated alkoxysilane surfactants and repellent coatings derived therefrom |
| US5498657A (en) * | 1993-08-27 | 1996-03-12 | Asahi Glass Company Ltd. | Fluorine-containing polymer composition |
| JPH0819839B2 (ja) | 1993-08-30 | 1996-02-28 | 株式会社大阪鋼管商会 | 上向きアンカー用落下防止先端スペーサ |
| US5550184A (en) * | 1994-03-04 | 1996-08-27 | E. I. Du Pont De Nemours & Company | Hydrolyzed silane emulsions and their use as surface coatings |
| US5442011A (en) | 1994-03-04 | 1995-08-15 | E. I. Du Pont De Nemours And Company | Polymeric fluorocarbon siloxanes, emulsions and surface coatings thereof |
| US5662887A (en) | 1994-12-01 | 1997-09-02 | Minnesota Mining And Manufacturing Company | Fluorocarbon containing coatings, compositions and methods of use |
| US6037429A (en) | 1995-06-16 | 2000-03-14 | 3M Innovative Properties Company | Water-soluble fluorochemical polymers for use in water and oil repellent masonry treatments |
| US5608003A (en) * | 1995-06-23 | 1997-03-04 | Minnesota Mining And Manufacturing Company | Aqueous fluorochemical compositions and abrasion-resistant coatings therefrom |
| US5998549A (en) | 1996-05-31 | 1999-12-07 | 3M Innovative Properties Company | Durable, low surface energy compounds and articles, apparatuses, and methods for using the same |
| US5760126A (en) * | 1996-12-20 | 1998-06-02 | Minnesota Mining And Manufacturing Company | Aqueous fluorochemical compositions and abrasion-resistant coatings therefrom |
| US6156860A (en) | 1997-02-18 | 2000-12-05 | Dainippon Ink And Chemicals, Inc. | Surface active agent containing fluorine and coating compositions using the same |
| WO1998049218A1 (en) | 1997-04-30 | 1998-11-05 | Daikin Industries, Ltd. | Fluoropolymer, process for preparing the same, and use thereof |
| US5980992A (en) | 1997-10-03 | 1999-11-09 | 3M Innovative Properties Company | Fluorochemical treatments to provide low-energy surfaces |
| WO1999029636A1 (en) | 1997-12-10 | 1999-06-17 | E.I. Du Pont De Nemours And Company | Fluorocarbon silane hydrolysate-containing aqueous emulsions, and materials coated therewith |
| JP4733798B2 (ja) | 1998-01-31 | 2011-07-27 | 凸版印刷株式会社 | 防汚剤、防汚層の形成方法、光学部材、反射防止光学部材、光学機能性部材及び表示装置 |
| JP3712031B2 (ja) | 1998-02-23 | 2005-11-02 | 信越化学工業株式会社 | 硬化性組成物 |
| JP2000169483A (ja) * | 1998-12-02 | 2000-06-20 | Daikin Ind Ltd | 親水・疎水の両基を有する表面処理剤 |
| US6649272B2 (en) * | 2001-11-08 | 2003-11-18 | 3M Innovative Properties Company | Coating composition comprising fluorochemical polyether silane polycondensate and use thereof |
-
2001
- 2001-01-19 AT AT01200208T patent/ATE358143T1/de not_active IP Right Cessation
- 2001-01-19 ES ES01200208T patent/ES2282186T3/es not_active Expired - Lifetime
- 2001-01-19 EP EP01200208A patent/EP1225188B1/de not_active Expired - Lifetime
- 2001-01-19 DE DE60127527T patent/DE60127527T2/de not_active Expired - Lifetime
-
2002
- 2002-01-17 MX MXPA03006077A patent/MXPA03006077A/es active IP Right Grant
- 2002-01-17 WO PCT/US2002/001675 patent/WO2002057329A1/en not_active Ceased
- 2002-01-17 US US10/053,001 patent/US6977307B2/en not_active Expired - Fee Related
- 2002-01-17 CN CNB028038517A patent/CN100422224C/zh not_active Expired - Fee Related
- 2002-01-17 JP JP2002558399A patent/JP2004517990A/ja not_active Withdrawn
- 2002-01-17 BR BR0206374-3A patent/BR0206374A/pt active Search and Examination
Also Published As
| Publication number | Publication date |
|---|---|
| EP1225188B1 (de) | 2007-03-28 |
| BR0206374A (pt) | 2003-12-23 |
| DE60127527T2 (de) | 2007-12-13 |
| JP2004517990A (ja) | 2004-06-17 |
| ES2282186T3 (es) | 2007-10-16 |
| US20030168783A1 (en) | 2003-09-11 |
| EP1225188A1 (de) | 2002-07-24 |
| CN100422224C (zh) | 2008-10-01 |
| US6977307B2 (en) | 2005-12-20 |
| DE60127527D1 (de) | 2007-05-10 |
| CN1487959A (zh) | 2004-04-07 |
| WO2002057329A1 (en) | 2002-07-25 |
| WO2002057329A8 (en) | 2003-11-06 |
| MXPA03006077A (es) | 2004-05-04 |
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